scholarly journals Synthesis of metal sulfide nanomaterials via thermal decomposition of single-source precursors

2010 ◽  
Vol 20 (32) ◽  
pp. 6612 ◽  
Author(s):  
Ilan Jen-La Plante ◽  
Tahani W. Zeid ◽  
Peidong Yang ◽  
Taleb Mokari
Keyword(s):  
Thermal Decomposition ◽  
Metal Sulfide ◽  
Single Source ◽  
Single Source Precursors

Group III Metal Sulfide Thin Films From Single-Source Precursors by Chemical Vapor Deposition (CVD) Techniques

1999 ◽  
Vol 606 ◽  
Author(s):  
Mike R. Lazell ◽  
Paul O'brien ◽  
David J. Otway ◽  
Jin-Ho Park
Keyword(s):  
Thin Films ◽  
Vapor Deposition ◽  
Vapour Deposition ◽  
Chemical Vapour ◽  
Metal Sulfide ◽  
Chemical Vapor ◽  
Single Source ◽  
Group 13 ◽  
Single Source Precursors ◽  
Group Iii

AbstractSeveral single-source precursors including In(SOCNiBu2)3, In(S2CNMeHex)3 and Ga(S2CNMeR)3, (R = Et, Bu, Hex) have been prepared and used for the deposition of Group 13 metal sulfide thin films. The α and β-In2S3thin films on borosilicate glass and oc-Ga 2S3thin films on GaAs(111) single crystal substrates were prepared from the precursors by various chemical vapour deposition (CVD) techniques. These semicondcuting materials have been characterized by XRD, SEM, XPS and EDAX.

Metal complexes of thiobiurets and dithiobiurets: Novel single source precursors for metal sulfide thin film nanostructures

2010 ◽  
Vol 39 (6) ◽  
pp. 1460-1463 ◽  
Author(s):  
Karthik Ramasamy ◽  
Mohammad A. Malik ◽  
Paul O'Brien ◽  
James Raftery
Keyword(s):  
Thin Film ◽  
Metal Complexes ◽  
Metal Sulfide ◽  
Single Source ◽  
Single Source Precursors ◽  
Thin Film Nanostructures

Optical and Structural Properties of TOPO/HDA Capped CuS Nanocrystals via Thermal Decomposition of Bis(N-Diisopropyldithiocarbamate)Cu(II) Complex

2019 ◽  
Vol 59 ◽  
pp. 161-165 ◽  
Author(s):  
Johannes Z. Mbese ◽  
Peter A. Ajibade ◽  
Funeka Matebese ◽  
Mojeed A. Agoro
Keyword(s):  
Thermal Decomposition ◽  
Metal Sulfide ◽  
Trioctylphosphine Oxide ◽  
Single Source ◽  
High Quality ◽  
Sem Images ◽  
Molecular Precursor ◽  
High Efficient ◽  
Synthetic Routes ◽  
Surface Morphologies

We present the rational synthesis of novel nanocrystals CuS (nc-CuS) by single source molecular precursor (SSMP) method. Among the present materials synthetic routes, the SSMP route is high efficient and comfortable way to construct nanostructured materials. Both CuS nanocrystals capped with hexadecylamine (HDA) and trioctylphosphine oxide (TOPO) have been synthesized by thermolysing bis (N-diisopropyldithiocarbamate)Cu (II) complex at 180 °C. Various physicochemical characterizations such as SEM images of nc-CuS exhibited uniform exfoliated surface morphologies with uniform continuous network of about 50 μm agglomerated particles. Our method could be broadly applicable for the preparation of other high quality yield metal sulfide nanostructures

scholarly journals Exothermal effects in the thermal decomposition of [IrCl6]2−-containing salts with [M(NH3)5Cl]2+ cations: [M(NH3)5Cl][IrCl6] (M = Co, Cr, Ru, Rh, Ir)

2018 ◽  
Vol 42 (3) ◽  
pp. 1762-1770 ◽  
Author(s):  
S. A. Martynova ◽  
P. E. Plyusnin ◽  
T. I. Asanova ◽  
I. P. Asanov ◽  
D. P. Pishchur ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Ligand Exchange ◽  
Endothermic Effect ◽  
Single Source ◽  
Single Source Precursors ◽  
Bimetallic Alloys

[M(NH3)5Cl][IrCl6], M = Co, Cr, Ru, Rh, and Ir, were proposed as single-source precursors for bimetallic alloys. Upon heating, compounds show endothermic effect which can be corresponded with Ir(iv) reduction and ligand exchange.

Synthesis, characterisation and thermal decomposition of tin(IV) dithiocarbamate derivatives – single source precursors for tin sulfide powders

Polyhedron ◽  
2004 ◽  
Vol 23 (12) ◽  
pp. 2103-2109 ◽  
Author(s):  
D.C. Menezes ◽  
G.M. de Lima ◽  
A.O. Porto ◽  
C.L. Donnici ◽  
J.D. Ardisson ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Tin Sulfide ◽  
Single Source ◽  
Single Source Precursors ◽  
Dithiocarbamate Derivatives
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