Controlled synthesis of metal sulfide nanocrystals by thermal decomposition of single-source precursors

2013 ◽  
Vol 43 (12) ◽  
pp. 1601-1613
Author(s):  
BoHua DONG ◽  
QiangBin WANG ◽  
YeJun ZHANG
2010 ◽  
Vol 20 (32) ◽  
pp. 6612 ◽  
Author(s):  
Ilan Jen-La Plante ◽  
Tahani W. Zeid ◽  
Peidong Yang ◽  
Taleb Mokari

1999 ◽  
Vol 606 ◽  
Author(s):  
Mike R. Lazell ◽  
Paul O'brien ◽  
David J. Otway ◽  
Jin-Ho Park

AbstractSeveral single-source precursors including In(SOCNiBu2)3, In(S2CNMeHex)3 and Ga(S2CNMeR)3, (R = Et, Bu, Hex) have been prepared and used for the deposition of Group 13 metal sulfide thin films. The α and β-In2S3thin films on borosilicate glass and oc-Ga 2S3thin films on GaAs(111) single crystal substrates were prepared from the precursors by various chemical vapour deposition (CVD) techniques. These semicondcuting materials have been characterized by XRD, SEM, XPS and EDAX.


2010 ◽  
Vol 39 (6) ◽  
pp. 1460-1463 ◽  
Author(s):  
Karthik Ramasamy ◽  
Mohammad A. Malik ◽  
Paul O'Brien ◽  
James Raftery

2019 ◽  
Vol 59 ◽  
pp. 161-165 ◽  
Author(s):  
Johannes Z. Mbese ◽  
Peter A. Ajibade ◽  
Funeka Matebese ◽  
Mojeed A. Agoro

We present the rational synthesis of novel nanocrystals CuS (nc-CuS) by single source molecular precursor (SSMP) method. Among the present materials synthetic routes, the SSMP route is high efficient and comfortable way to construct nanostructured materials. Both CuS nanocrystals capped with hexadecylamine (HDA) and trioctylphosphine oxide (TOPO) have been synthesized by thermolysing bis (N-diisopropyldithiocarbamate)Cu (II) complex at 180 °C. Various physicochemical characterizations such as SEM images of nc-CuS exhibited uniform exfoliated surface morphologies with uniform continuous network of about 50 μm agglomerated particles. Our method could be broadly applicable for the preparation of other high quality yield metal sulfide nanostructures


2011 ◽  
Vol 21 (26) ◽  
pp. 9737 ◽  
Author(s):  
Masood Akhtar ◽  
Javeed Akhter ◽  
M. Azad Malik ◽  
Paul O'Brien ◽  
Floriana Tuna ◽  
...  

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