Synthesis of phase-pure SnS particles employing dithiocarbamate organotin(IV) complexes as single source precursors in thermal decomposition experiments

2010 ◽  
Vol 24 (9) ◽  
pp. 650-655 ◽  
Author(s):  
D. C. Menezes ◽  
G. M. de Lima ◽  
F. A. Carvalho ◽  
M. G. Coelho ◽  
A. O. Porto ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Single Source ◽  
Single Source Precursors ◽  
Phase Pure ◽  
Decomposition Experiments

Heterometallic trinuclear oxo-centered clusters as single-source precursors for synthesis of stoichiometric monodisperse transition metal ferrite nanocrystals

2020 ◽  
Vol 49 (45) ◽  
pp. 16348-16358
Author(s):  
Karla R. Sanchez-Lievanos ◽  
Mehrin Tariq ◽  
William W. Brennessel ◽  
Kathryn E. Knowles
Keyword(s):  
Transition Metal ◽  
Single Source ◽  
Single Source Precursors ◽  
Phase Pure

Solvothermal reactions of MIIFe2III(μ3-O)(μ2-O2CR)6(H2O)3 (R = CF3, M = Fe, Co, Ni, Cu, Zn) clusters produce monodisperse, phase-pure MFe2O4 nanocrystals.

scholarly journals Synthesis of metal sulfide nanomaterials via thermal decomposition of single-source precursors

2010 ◽  
Vol 20 (32) ◽  
pp. 6612 ◽  
Author(s):  
Ilan Jen-La Plante ◽  
Tahani W. Zeid ◽  
Peidong Yang ◽  
Taleb Mokari
Keyword(s):  
Thermal Decomposition ◽  
Metal Sulfide ◽  
Single Source ◽  
Single Source Precursors

In Air Synthesis of Bi2S3 and PbS Microcrystals by Thermolysis of Single-Source Precursors

2009 ◽  
Vol 79-82 ◽  
pp. 1343-1346
Author(s):  
Zhen Ni Du ◽  
Yong Cai Zhang
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Inert Gases ◽  
Formation Mechanisms ◽  
Single Source ◽  
X Ray Diffraction ◽  
Single Source Precursors ◽  
X Ray ◽  
Phase Pure ◽  
Scanning Electron

Without the protection of inert gases or vacuum environment, rod-like Bi2S3 and cubic-shaped PbS microcrystals were synthesized directly via pyrolyzing corresponding metal diethyldithiocarbamates in air at 300 °C for 3 h. The products have been characterized by X-ray diffraction and scanning electron microscope, and their possible formation mechanisms were also tentatively proposed. Furthermore, control experiments with multiple-source precursors revealed that our single-source precursors played an important role in preparing phase-pure Bi2S3 and PbS.

scholarly journals Exothermal effects in the thermal decomposition of [IrCl6]2−-containing salts with [M(NH3)5Cl]2+ cations: [M(NH3)5Cl][IrCl6] (M = Co, Cr, Ru, Rh, Ir)

2018 ◽  
Vol 42 (3) ◽  
pp. 1762-1770 ◽  
Author(s):  
S. A. Martynova ◽  
P. E. Plyusnin ◽  
T. I. Asanova ◽  
I. P. Asanov ◽  
D. P. Pishchur ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Ligand Exchange ◽  
Endothermic Effect ◽  
Single Source ◽  
Single Source Precursors ◽  
Bimetallic Alloys

[M(NH3)5Cl][IrCl6], M = Co, Cr, Ru, Rh, and Ir, were proposed as single-source precursors for bimetallic alloys. Upon heating, compounds show endothermic effect which can be corresponded with Ir(iv) reduction and ligand exchange.

Synthesis, characterisation and thermal decomposition of tin(IV) dithiocarbamate derivatives – single source precursors for tin sulfide powders

Polyhedron ◽  
2004 ◽  
Vol 23 (12) ◽  
pp. 2103-2109 ◽  
Author(s):  
D.C. Menezes ◽  
G.M. de Lima ◽  
A.O. Porto ◽  
C.L. Donnici ◽  
J.D. Ardisson ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Tin Sulfide ◽  
Single Source ◽  
Single Source Precursors ◽  
Dithiocarbamate Derivatives

An efficient method for the synthesis of nickel phosphide nanocrystals via thermal decomposition of single-source precursors

RSC Advances ◽  
2015 ◽  
Vol 5 (16) ◽  
pp. 11952-11959 ◽  
Author(s):  
Yuan Pan ◽  
Yunqi Liu ◽  
Chenguang Liu
Keyword(s):  
Thermal Decomposition ◽  
Reaction Time ◽  
Reaction Temperature ◽  
Efficient Method ◽  
Nickel Phosphide ◽  
Single Source ◽  
Single Source Precursors ◽  
First Time

We report an efficient method for the synthesis of nickel phosphide NCs for the first time. The size of Ni2P NCs can be controlled by changing reaction temperature and OAm quantity. The phase of nickel phosphide NCs can be controlled by increasing reaction time.

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