Fdtd Simulations And Analysis Of Thin Sample Dielectric Properties Measurements Using Coaxial Probes

1996 ◽  
Vol 430 ◽  
Author(s):  
S. Bringhurst ◽  
M. F. Iskander ◽  
M. J White

AbstractA metallized ceramic probe has been designed for high temperature broadband dielectric properties measurements. The probe was fabricated out of an alumina tube and rod as the outer and inner conductors respectively. The alumina was metallized with a 3 mil layer of moly-manganese and then covered with a 0.5 mil protective layer of nickel plating. The probe has been used to make complex dielectric properties measurements over the complete frequency band from 500 MHz to 3 GHz, and for temperatures as high as 1000 °C.

1992 ◽  
Vol 269 ◽  
Author(s):  
Shane Bringhurst ◽  
Octavio M. Andrade ◽  
Magdy F. Iskander

ABSTRACTThis paper dicusses experimental arrangements, describes measurement techniques and presents experimental results for hightemperature broadband dielectric properties measurements of ceramics. The cavity perturbation technique and the open-ended coaxial line method are used in these experimental measurements. The design and construction details of cavities and probes are described and representative results of measurements on zirconia and alumina samples (green and sintered) are presented. Results of measurements made on insulating materials are shown. In general measurements are made in the frequency band 1 to 10 GHz and temperatures up to 1000°C.


1994 ◽  
Vol 347 ◽  
Author(s):  
Shane Bringhurst ◽  
Magdy F. Iskander ◽  
Paul Gartside

ABSTRACTOpen-ended coaxial probes have been used in broadband dielectric properties measurements for several years. To aid in the ongoing numerical simulation and microwave sintering research at the University of Utah, we have found it necessary to make dielectric properties measurements up to temperatures as high as 1400 °C. The available cavity perturbation techniques were unsuitable in this application due to their relatively narrow band, and the available metal probes are also unsuitable due to the differential thermal expansions of the inner and outer conductors, which makes it difficult to carry out accurate and on-line calibration procedures for these probes.To help us achieve both broadband and high-temperature dielectric properties measurements, we have developed a new metallized ceramic coaxial probe. The detailed design of this probe is described and the metallization procedure is discussed.Also to optimize the design of the probe and in particular to increase the penetration of fields in samples under test and hence improve the probe sensitivity to variation in properties of a larger class of materials, and to determine the required minimum thickness of various samples to obtain accurate results, we modeled and simulated the probe performance using the Finite-Difference Time-Domain (FDTD) method. Results from the FDTD simulation are presented and some guidelines that may be used to optimize the design of the probe are discussed.


2013 ◽  
Vol 114 (2) ◽  
pp. 027014 ◽  
Author(s):  
Tian-Long Zhao ◽  
Jianguo Chen ◽  
Chun-Ming Wang ◽  
Yang Yu ◽  
Shuxiang Dong

Author(s):  
Stephen R. Swartz

Since the inception of the cyclone style boiler, industry has become accustomed to performing routine maintenance during every scheduled shutdown occurring 12 months to 18 months between cycles. These maintenance cycles are influenced by service factor, loading and the type design. The same problems exist in both the standard and super critical cyclones; severe deterioration of refractory and the anchoring pin studs. This paper focuses on one type of refractory failure mechanism caused by the anchoring pin studs. Most operators have found that the most effective means of applying refractory in this type situation is to “ram” the refractory in and around the anchoring pin studs thus creating a dense lining with maximum integrity. Coupled with proper application of anchoring pin studs and a special designed coating, typical volumetric expansion of the pin studs from corrosion attack and oxidation is eliminated thus extending the life of the refractory. This mechanism is discussed along with the results of the coating performance as it relates to extreme heat oxidation and thermal cycling in laboratory tests. A protective coating was developed using a nano-cored thermal spray wire technology that produces a uniform, adherent protective layer against high temperature corrosion and oxidation. The coating yields similar thermal conductivity as a bare stud thus experiencing excellent thermal cycle performance. This specially designed thermal spray coating is applied to standard 430 stainless steel pin studs thus providing the necessary barrier against aggressive high temperature environments while maintaining excellent heat conductivity. The coating has a high amount of tungsten (40+%) in a nickel matrix with greatly reduced oxides at the substrate and throughout the coating. With these attributes for the anchoring pin studs in mind, a newly designed stud was evaluated in heat oxidation tests up to 2000°F and thermal cycling test and compared to 430 stainless steel, chromized and Alloy 625. The new stud out-performed all others even in the as-welded condition. Further corrosion testing in ferric chloride (ASTM G48) showed them to be superior to Alloy 72 and Alloy 625 in the thermal spray and welded condition. Proper welding equipment and welding techniques are also discussed since weld continuity impacts overall performance of anchoring pin studs with refractory linings. A major test site will be examined in the spring of 2004 for it’s full effectiveness in service and will be documented in order that all data retrieved would be available to the entire industry.


1968 ◽  
Vol 39 (1) ◽  
pp. 70-74 ◽  
Author(s):  
Robert T. Smith ◽  
Gary D. Achenbach ◽  
Robert Gerson ◽  
W. J. James

Author(s):  
Yu. Tsapko ◽  
◽  
А. Tsapko ◽  
O. Bondarenko ◽  
V. Lomaha ◽  
...  

Abstract. The processes of creation of fire-retardant varnish for wood consisting of a mixture of inorganic and polymeric substances are investigated in the work. It is established that the optimization of the inorganic component leads to a directional ratio of mineral acids and urea capable of effective fire protection of the material. Studies have shown that at the initial temperature of gaseous combustion products T = 68 °C, when exposed to the radiation panel, the untreated sample ignited after 146 s, the flame spread over the entire surface, instead, the sample fire-protected varnish did not ignite, the maximum temperature was 105 °C. In this case, as evidenced by the results of heat resistance, there is a change in the structure of the protective film of the coating. The thickness of the protective layer increases due to the decomposition of the composition, which leads to inhibition of oxidation in the gas and condensed phase, change the direction of decomposition towards the formation of non-combustible gases and combustible coke residue, reduce material combustion and increase flammability index. The coating under the influence of high temperature promotes the formation of a heat-insulating layer of coke, which prevents burning and the passage of high temperature to the material, which is confirmed by the absence of the process of ignition of fire-retardant wood. Features of braking of process of ignition and distribution of a flame of the wood processed by a varnish which consist in several aspects are established. This is the formation of a heat-insulating layer of coke, which prevents burning and the passage of high temperatures to the material, which is confirmed by the absence of the process of ignition of fire-retardant reeds. This indicates the possibility of targeted control of high temperature transfer processes to organic material through the use of special coatings for wood products.


2020 ◽  
Vol 11 (3) ◽  
Author(s):  
V. V. Lomaha ◽  
O. Yu. Tsapko ◽  
Yu. V. Tsapko ◽  
O. P. Bondarenko

Reducing the fire prevention of timber is not only an economic task, but also has a social and environmental focus. From economic, technological and environmental perspective, an important problem in ensuring the viability and safe operation of construction sites is the development of fire-retardant coatings for wooden structures. The construction is increasingly looking for new highly effective means of fire protection of wood and wood products which should not only ensure the standardized fire resistance of wood, but also to maintain its operational parameters to solve environmental safety and durability. Studies of the effect of the radiation panel on the ignition of the wood sample have set the parameters of the flame ignition, which makes it possible to influence this process. It is proved that they consist in the formation of a layer of organic material on the surface, which provides heating to a critical temperature, when the intensive decomposition of the material begins with the release of the required amount of combustible gases and their ignition. This makes it possible to determine the effect of fire protection and the properties of protective compositions on the process of slowing down the rate of burning of wood. Experimental studies have confirmed that the untreated sample of wood, under the thermal action of the radiation panel has taken up, the flames spread over the entire surface, which led to its combustion. The application of a fire retardant varnish under the influence of temperature leads to a layer of foam coke and inhibition of heat transfer of high-temperature flame to the material and its ignition. Thanks to this, it became possible to determine the conditions for changing the parameters of combustion and braking during fire protection of wood, by forming a barrier for thermal conductivity. Thus, there is reason to argue for the possibility of directional control of the processes of fire protection of wood by the use of fireproof coatings that can form a protective layer on the surface of the material, which slows down the rate of burning of wood.


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