scholarly journals Optimization of Electroless Ni-P-W Coatings for Minimum Friction and Wear Using Grey-Taguchi Method

2013 ◽  
Vol 2013 ◽  
pp. 1-13 ◽  
Author(s):  
Supriyo Roy ◽  
Prasanta Sahoo

The present experimental investigation deals with the deposition of electroless Ni-P-W coating on mild steel substrate and optimization of tribological parameters for better tribological behaviour like minimization of wear depth and coefficient of friction. Three tribological test parameters, namely, load, speed, and time, are optimized for minimum friction and wear of the coating. Friction and wear tests are carried out in a multitribotester using block on roller configuration under dry conditions. Taguchi based grey relational analysis is employed for optimization of this multiple response problem using L27 orthogonal array. Analysis of variance shows that load, speed, time, and interaction between load and speed have significant influence on controlling the friction and wear behavior of Ni-P-W coating. It is observed that wear mechanism is mild adhesive in nature. The structural morphology, composition, and phase structure of the coating are studied with the help of scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDX), and X-ray diffraction analysis (XRD), respectively.

Author(s):  
Arkadeb Mukhopadhyay ◽  
Santanu Duari ◽  
Tapan Kr. Barman ◽  
Prasanta Sahoo

Friction and wear behavior of electroless Ni-P coating under lubricated condition is studied on a block – on – roller type tribo – tester by varying applied normal load, sliding speed of the roller and sliding time. Electroless Ni-P coating is deposited on AISI 1040 steel substrates. Surface morphology, phase transformation, composition and analysis of wear mechanism are done using scanning electron microscope, X-ray diffraction techniques and energy dispersive X-ray analysis respectively. Based on Taguchi experimental data, a multiple regression model is fitted to relate the coefficient of friction and wear depth with the tribo – testing parameters. Three dimensional surface and contour plots are generated to analyze the trends in variation of the response variables with the interaction of the process parameters (load, speed and time). Significant improvement in wear depth and COF of electroless Ni-P coating is observed under lubrication. Optimization of wear depth and coefficient of friction is conducted using genetic algorithm.


Author(s):  
Santanu Duari ◽  
Arkadeb Mukhopadhyay ◽  
Tapan Kumar Barman ◽  
Prasanta Sahoo

The present chapter aims to determine optimal tribo-testing condition for minimum coefficient of friction and wear depth of electroless Ni-P, Ni-P-W and Ni-P-Cu coatings under lubrication using grey relational analysis. Electroless Ni-P, Ni-P-W and Ni-P-Cu coatings are deposited on AISI 1040 steel substrates. They are heat treated at suitable temperatures to improve their hardness. Coating characterization is done using scanning electron microscope, energy dispersive X-Ray analysis and X-Ray diffraction techniques. Typical nodulated surface morphology is observed in the scanning electron micrographs of all the three coatings. Phase transformation on heat treating the deposits is captured through the use of X-Ray diffraction technique. Vicker's microhardness of the coatings in their as-deposited and heat treated condition is determined. Ni-P-W coatings are seen to exhibit the highest microhardness. Friction and wear tests under lubricated condition are carried out following Taguchi's experimental design principle. Finally, the predominating wear mechanism of the coatings is discussed.


Author(s):  
Prasanta Sahoo ◽  
Supriyo Roy ◽  
J. Paulo Davim

Chemically deposited nickel coatings possess superior tribological properties such as high hardness, good wear, and corrosion resistance. The quest for improved tribological performance has led to the design and selection of newer variants of these coatings. The present chapter deals with the development of Ni-P-W coating on mild steel substrate and the improvement of tribological characteristics through modification of the coating process parameters. Three coating process parameters, concentration of nickel source, concentration of reducing agent, and concentration of tungsten source along with the annealing temperature, are optimized for minimum friction and wear of the coating. Friction and wear tests are carried out in a multi-tribotester using block on roller configuration under dry conditions. Taguchi-based grey relational analysis is employed for the optimization of this multiple response problem using L27 orthogonal array. Analysis of variance shows that the concentration of nickel source, the interaction between nickel source concentration, and reducing agent concentration, and also the interaction between nickel source concentration and tungsten source concentration have significant influence in controlling the friction and wear behavior of chemically deposited Ni-P-W coating. It is observed that wear mechanism is a mild adhesive in nature. The structural morphology, composition, and phase structure of the coating are studied with the help of Scanning Electron Microscopy (SEM), Energy Dispersive X-Ray analysis (EDX), and X-Ray Diffraction analysis (XRD), respectively.


Author(s):  
K. S. Kanaga Karuppiah ◽  
Angela L. Bruck ◽  
Sriram Sundararajan

In this study the friction and wear behavior of medical grade ultra-high molecular weight polyethylene (UHMWPE) (GUR 1050 resin) were evaluated as a function of polymer crystallinity. Crystallinity was controlled by heating UHMWPE samples to a temperature above its melting point and varying the hold time and cooling rates. Degree of crystallinity of the samples was evaluated using differential scanning calorimetry (DSC). Quantitative friction experiments were conducted at two different scales. A custom-made microtribometer with commercially available spherical Si3N4 probes in dry conditions was used to test friction at the microscale. An atomic force microscope with commercially available Si3N4 probes under dry conditions was used for nanoscale experiments. A higher degree of crystallinity in the UHMWPE resulted in lower friction force and an increase in scratch resistance at both scales. Reciprocating wear tests preformed using the tribometer show that higher crystallinity also results in lower friction, as well as lower wear depth and width.


2016 ◽  
Vol 879 ◽  
pp. 164-168
Author(s):  
Auezhan Amanov ◽  
Jun Hyong Kim ◽  
Young Sik Pyun

In this study, two different AISI 52100 bearing and D2 tool steels were subjected to ultrasonic nanocrystalline surface modification (UNSM) technique at ambient and high temperature of 500 °C. The objective of this study is to characterize the microstructure and to investigate the effectiveness of UNSM technique on the friction and wear behavior of those steels. The friction and wear behavior of the specimens against AISI52100 bearing steel ball with a diameter of 10 mm was carried out using a micro-tribo tester under dry conditions. The hardness with respect to depth from the top surface was measured using a microhardness. The change in the microstructure of the specimens before and after UNSM treatment was characterized by scanning electron microscopy (SEM). The findings from this preliminary study are expected to be implemented to the bearings and tools to increase the efficiency and performance of the components.


2018 ◽  
Vol 913 ◽  
pp. 168-175
Author(s):  
Xian Ye Liang ◽  
Guang Bao Mi ◽  
Liang Ju He ◽  
Pei Jie Li

The abnormal local friction and wear phenomena usually generate during the service of the titanium alloy rotor /stator parts of the aero engine compressor under high temperature conditions. This phenomenon is the main cause of the occurrence of titanium fire failure and has great harm. In the present investigation the friction and wear behavior of the combustion resistant titanium alloy at high temperature was studied by finite element numerical simulation and experimental verification of the pin-on-disk model. Firstly, the geometrical model of the round bottom pin-on-disk contact was established. Then, the friction process was simulated by the Coulomb friction model. The ALE technique of ABAQUS was applied to move the contact nodes and update the grid. The finite element simulation of the ARCHARD wear model was realized. In order to deal with the increasing contact area, a simplify wear direction was proposed. Finally, the wear depth and volume was calculated and the wear law at 500 °C -900 °C was revealed. The results show that the wear process is gentle at the temperature of 500-700 °C, and the wear depth is within 0.08mm when the sliding distance reaches 1800m. When the temperature exceeds 800 °C, the wear rate increased sharply and the wear depth beyond 0.1mm, the FE result is consistent with the test results.


Author(s):  
R. Ribeiro ◽  
S. Ingole ◽  
O. Juan ◽  
H. Liang ◽  
M. Usta ◽  
...  

Enhanced corrosion and wear resistance are crucially important to prolong the service life of biomaterials. Boronizing has been reported to enhance the wear resistance of pure chromium. In this research, we investigate friction and wear behavior of boronized chromium. Pin-on-disc tribometer was used to conduct the wear and friction tests. Experiments were conducted in dry conditions as well as in simulated body fluid (SBF). Fundamental aspects of wear mode and lubrication behavior were studied using surface characterization techniques such as TEM, and X-ray diffraction. Results showed evidence of tribo-chemical interactions between SBF and work piece materials.


2017 ◽  
Vol 140 (1) ◽  
Author(s):  
F. Zouch ◽  
Z. Antar ◽  
A. Bahri ◽  
K. Elleuch ◽  
M. Ürgen

Ternary iron–tungsten–phosphorus (Fe–W–P) coatings were electrodeposited with different sodium tungstate (NaWO4·2H2O) concentration on stainless steel 316 L substrate. These coatings were characterized by energy dispersive X-ray spectrometer (EDX), scanning electron microscope (SEM), and X-ray diffraction (XRD). The friction and wear behavior of these coatings were investigated using ball-on-disk tribometer under dry conditions. This study reveals a nanocrystalline and nodular structure with nanometric grain size of the deposited alloy. The maximum level of incorporation of tungsten (W) is about 29.54 at %. It was obtained with 0.5 M of sodium tungstate concentration, and it increases the microhardness of the coatings. Moreover, it was found that Fe–W–P coatings had significantly improved the tribological properties of the substrate due to their higher wear resistance and lower friction coefficient.


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