Single Crystalline Nanowires of Lead Can Be Synthesized through Thermal Decomposition of Lead Acetate in Ethylene Glycol

Nano Letters ◽  
2003 ◽  
Vol 3 (8) ◽  
pp. 1163-1166 ◽  
Author(s):  
Yuliang Wang ◽  
Thurston Herricks ◽  
Younan Xia
Keyword(s):  
Thermal Decomposition ◽  
Ethylene Glycol ◽  
Lead Acetate ◽  
Single Crystalline

Enhancement of magnetic heating efficiency in size controlled MFe2O4 (M = Mn, Fe, Co and Ni) nanoassemblies

RSC Advances ◽  
2015 ◽  
Vol 5 (19) ◽  
pp. 14311-14321 ◽  
Author(s):  
Jeotikanta Mohapatra ◽  
Saumya Nigam ◽  
J. Gupta ◽  
A. Mitra ◽  
M. Aslam ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Ethylene Glycol ◽  
Magnetic Nanoparticle ◽  
Metal Chloride ◽  
Heating Efficiency ◽  
Magnetic Heating ◽  
Size Controlled

The MFe2O4 magnetic nanoparticle nanoassemblies (MNNAs) have been synthesized via thermal decomposition of metal chloride in ethylene glycol (EG) in the presence of ethylenediamine (EDA).

Seedless Synthesis and Thermal Decomposition of Single Crystalline Zinc Hydroxystannate Cubes

2009 ◽  
Vol 9 (10) ◽  
pp. 4456-4460 ◽  
Author(s):  
Gregory Wrobel ◽  
Martin Piech ◽  
Sameh Dardona ◽  
Yong Ding ◽  
Pu-Xian Gao
Keyword(s):  
Thermal Decomposition ◽  
Single Crystalline ◽  
Zinc Hydroxystannate

Microwave-assisted synthesis of β-Co(OH)2 and Co3O4 nanosheets via a layered precursor conversion method

2006 ◽  
Vol 84 (8) ◽  
pp. 1050-1053 ◽  
Author(s):  
Zhen-Hua Liang ◽  
Ying-Jie Zhu ◽  
Guo-Feng Cheng ◽  
Yue-Hong Huang
Keyword(s):  
Ethylene Glycol ◽  
Key Words ◽  
Microwave Heating ◽  
Cobalt Oxide ◽  
Cobalt Hydroxide ◽  
Microwave Assisted Synthesis ◽  
Particle Sizes ◽  
Average Thickness ◽  
Single Crystalline ◽  
Microwave Assisted

Single crystalline β-Co(OH)2 nanosheets have been synthesized from a layered precursor cobalt(II) acetate hydroxide by microwave heating. The average thickness of β-Co(OH)2 nanosheets is ~10 nm, with particle sizes up to 360 nm. The layered precursor was prepared using Co(CH3COO)2·4H2O, ethylene glycol, and H2O in some cases by microwave heating. Co3O4 nanosheets have been synthesized by hydrothermal oxidation of the layered precursor cobalt(II) acetate hydroxide using H2O2.Key words: nanosheets, microwave, cobalt hydroxide, cobalt oxide.

Mesoporous nanocrystalline ZnO microspheres by ethylene glycol mediated thermal decomposition

2018 ◽  
Vol 29 (12) ◽  
pp. 3455-3461 ◽  
Author(s):  
Emre Alp ◽  
Emre Can Araz ◽  
Ahmet Furkan Buluç ◽  
Yağmur Güner ◽  
Yücel Değer ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Ethylene Glycol

Synthesis of Copper Sulfide Nanoparticles by Thermal Decomposition Approach and Morphology Dependent Peroxidase-Like Activity

2020 ◽  
Vol 20 (5) ◽  
pp. 2763-2780
Author(s):  
Vanita Sharma ◽  
P. Jeevanandam
Keyword(s):  
Thermal Decomposition ◽  
Ethylene Glycol ◽  
Copper Sulfide ◽  
Diphenyl Ether ◽  
Decomposition Approach ◽  
Precursor Complex ◽  
Exposed Facets

Copper sulfide nanoparticles have been employed as artificial mimics for peroxidase-like activity. In the present study, copper sulfide nanoparticles with four different morphologies have been synthesized by thermal decomposition of cyclo-tri-μ-thioacetamide-tris(chlorocopper(I)) complex ([Cu3TAA3Cl3]) at 200 °C in different solvents such as diphenyl ether, ethylene glycol, 1-octadecene and also without any solvent. Hierarchical copper sulfide nanostructures are formed when the complex is decomposed in the absence of solvent, in diphenyl ether, and 1-octadecene while in the case of ethylene glycol, randomly agglomerated nanoparticles are formed. The precursor complex ([Cu3TAA3Cl3]) as well as copper sulfide nanoparticles were characterized using an array of techniques and after characterization, the peroxidase-like activity of copper sulfide nanoparticles was investigated.Morphologically different copper sulfide nanoparticles possess different exposed facets and due to this, the peroxidase-like activity was different among different morphologies.

Facile Synthesis of Hierarchically Macro/Mesoporous Carbons by Polymerization-Induced Phase Separation Combined with Starch Template

2012 ◽  
Vol 512-515 ◽  
pp. 1641-1646
Author(s):  
Ze Wen Xiao ◽  
Gang Zhang ◽  
Guan Jun Qiao
Keyword(s):  
Thermal Decomposition ◽  
Phase Separation ◽  
Ethylene Glycol ◽  
Phenolic Resin ◽  
Mesoporous Carbons ◽  
Hierarchical Porous Structure ◽  
Facile Synthesis ◽  
Surface Areas ◽  
Hierarchical Porous ◽  
Polymerization Induced Phase Separation

In this work, a facile approach combining polymerization-induced phase separation and starch-templating is presented to synthesize hierarchically macro/mesoporous carbons. The obtained porous carbons have bimodal macropores with pore diameters of 10~60 μm and 3~5 μm and 3D interconnected mesopores with pore diameters of 5~40 nm. The large macropores and the small macropores are obtained by the thermal decomposition and the closely stacking of starch particles, respectively. The 3D interconnected mesopores are developed through polymerization-induced phase separation between ethylene glycol and phenolic resin via spinodal decomposition mechanism. These as-prepared hierarchically macro/mesoporous carbons may have great potential for applications as electrodes materials for batteries, fuel cells, and supercapacitors due to their facile synthesis, unique hierarchical porous structure, and large BET surface areas (~ 610 m2/g).

High yield preparation of single crystalline Cd metal nanotubes by non-catalytic thermal decomposition route

2012 ◽  
Vol 14 (6) ◽  
pp. 693-697 ◽  
Author(s):  
Waheed S. Khan ◽  
Chuanbao Cao ◽  
Faheem K. Butt ◽  
Zulfiqar Ali ◽  
Ghulam Nabi ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
High Yield ◽  
Single Crystalline ◽  
Catalytic Thermal Decomposition ◽  
Metal Nanotubes
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