Microwave-assisted synthesis of β-Co(OH)2 and Co3O4 nanosheets via a layered precursor conversion method

2006 ◽  
Vol 84 (8) ◽  
pp. 1050-1053 ◽  
Author(s):  
Zhen-Hua Liang ◽  
Ying-Jie Zhu ◽  
Guo-Feng Cheng ◽  
Yue-Hong Huang

Single crystalline β-Co(OH)2 nanosheets have been synthesized from a layered precursor cobalt(II) acetate hydroxide by microwave heating. The average thickness of β-Co(OH)2 nanosheets is ~10 nm, with particle sizes up to 360 nm. The layered precursor was prepared using Co(CH3COO)2·4H2O, ethylene glycol, and H2O in some cases by microwave heating. Co3O4 nanosheets have been synthesized by hydrothermal oxidation of the layered precursor cobalt(II) acetate hydroxide using H2O2.Key words: nanosheets, microwave, cobalt hydroxide, cobalt oxide.

2020 ◽  
Vol 44 (42) ◽  
pp. 18308-18318
Author(s):  
V. Kepenienė ◽  
R. Stagniūnaitė ◽  
A. Balčiūnaitė ◽  
L. Tamašauskaitė-Tamašiūnaitė ◽  
E. Norkus

Deposition of AuNPs onto a CeO2/C substrate results in the enhanced electrocatalytic activity of the formed AuCeO2/C catalyst for the oxidation reaction of methanol, ethanol, ethylene glycol, and glycerol compared with the prepared Au/C catalyst.


2011 ◽  
Vol 125 (3) ◽  
pp. 347-350 ◽  
Author(s):  
Aarti Sripathi Bhatt ◽  
Denthaje Krishna Bhat ◽  
Cheuk-wai Tai ◽  
Mysore Sridhar Santosh

2004 ◽  
Vol 116 (11) ◽  
pp. 1434-1438 ◽  
Author(s):  
Ying-Jie Zhu ◽  
Wei-Wei Wang ◽  
Rui-Juan Qi ◽  
Xian-Luo Hu

2014 ◽  
Vol 406 ◽  
pp. 104-110 ◽  
Author(s):  
Zhiliang Li ◽  
Renyuan Teng ◽  
Shuqi Zheng ◽  
Yuzhuo Zhang ◽  
Ting Huang ◽  
...  

2010 ◽  
Vol 122 (44) ◽  
pp. 8429-8432 ◽  
Author(s):  
Xiaohe Liu ◽  
Renzhi Ma ◽  
Yoshio Bando ◽  
Takayoshi Sasaki

2019 ◽  
Vol 30 ◽  
pp. 27-33 ◽  
Author(s):  
Wen Luo ◽  
Jean-Jacques Gaumet ◽  
Pierre Magri ◽  
Sébastien Diliberto ◽  
Feng Li ◽  
...  

2013 ◽  
Vol 2013 ◽  
pp. 1-5
Author(s):  
Sheauly Khatun ◽  
M. Z. H. Khan ◽  
Khodeza Khatun ◽  
M. A. Sattar

An efficient synthesis of arylidene acetophenones have been achieved by using the microwave heating in comparison to the conventional heating. In this work compound 1-phenyle-3-(4-droxyphenyle)-2-propen-1-one, 1-(4-chlorophenyle)-3-phenyle-2-propen-1-one, and 1-(4-chlorophenyle)-3-(4-hydroxyphenyle)-2-propen-1-one have been synthesized by the condensation reaction between aromatic aldehydes and substituted acetophenones under microwave irradiation. The compounds of aldehydes and acetophenones were used as benzaldehyde, parahydroxybenzaldehyde, acetophenone, and parachloroacetophenone. The result shows that the time taken for the reaction was reduced from the conventional 1-2 hours to 60–120 seconds. The yield of the compounds in the conventional heating was moderate while the highest yield of 90–98% was observed in MWI method. The structure of the compounds was characterized by their IR,1H-NMR spectral data.


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