In situ synchrotron radiation grazing incidence X-ray diffraction—A powerful technique for the characterization of solid-state ion-selective electrode surfaces

2006 ◽  
Vol 51 (23) ◽  
pp. 4886-4891 ◽  
Author(s):  
Roland De Marco ◽  
Zhong-Tao Jiang ◽  
Bobby Pejcic ◽  
Arie van Riessen
Keyword(s):  
Solid State ◽  
Synchrotron Radiation ◽  
Grazing Incidence ◽  
X Ray Diffraction ◽  
Selective Electrode ◽  
X Ray ◽  
Powerful Technique ◽  
Electrode Surfaces

X-RAY DIFFRACTION FOR SURFACES AND BURIED INTERFACES

2000 ◽  
Vol 07 (04) ◽  
pp. 437-446 ◽  
Author(s):  
G. RENAUD
Keyword(s):  
Grazing Incidence ◽  
X Rays ◽  
X Ray Diffraction ◽  
X Ray ◽  
Grain Sizes ◽  
Buried Interfaces ◽  
Surfaces And Interfaces ◽  
Coherent Interfaces

The application of X-rays to the structural characterization of surfaces and interfaces, in situ and in UHV, is discussed on selected examples. Grazing incidence X-ray diffraction is not only a very powerful technique for quantitatively investigating the atomic structure of surfaces and interfaces, but is also very useful for providing information on the interfacial registry for coherent interfaces or on the strain deformation, island and grain sizes for incoherent epilayers.

A flow cell for transient voltammetry and in situ grazing incidence X-ray diffraction characterization of electrocrystallized cadmium(II) tetracyanoquinodimethane

2011 ◽  
Vol 56 (3) ◽  
pp. 1546-1553 ◽  
Author(s):  
Jean-Pierre Veder ◽  
Ayman Nafady ◽  
Graeme Clarke ◽  
Ross P. Williams ◽  
Roland De Marco ◽  
...  
Keyword(s):  
Grazing Incidence ◽  
Flow Cell ◽  
X Ray Diffraction ◽  
X Ray

Growth mechanisms of Pd nanofilms electrodeposited onto Au(111): an in situ grazing incidence X-ray diffraction study

2016 ◽  
Vol 18 (4) ◽  
pp. 2830-2839 ◽  
Author(s):  
Yvonne Soldo-Olivier ◽  
Maurizio De Santis ◽  
Wang Liang ◽  
Eric Sibert
Keyword(s):  
Diffraction Study ◽  
Grazing Incidence ◽  
Growth Mechanisms ◽  
X Ray Diffraction ◽  
X Ray

Surface X-ray diffraction characterization of a Pd10ML/Au(111) film. A characteristic Pd rod with sharp Bragg-like peaks is observed, signature of 3D islands growth.

A Combined Voltammetric and Synchrotron Radiation-Grazing Incidence X-ray Diffraction Study of the Electrocrystallization of Zinc Tetracyanoquinodimethane

2012 ◽  
Vol 65 (3) ◽  
pp. 236 ◽  
Author(s):  
Jean-Pierre Veder ◽  
Ayman Nafady ◽  
Graeme Clarke ◽  
Roland De Marco ◽  
Alan M. Bond
Keyword(s):  
Synchrotron Radiation ◽  
Grazing Incidence ◽  
Ex Situ ◽  
X Ray Diffraction ◽  
Pt Electrode ◽  
Cyclic Voltammetric ◽  
X Ray ◽  
Ir And Raman ◽  
Voltammetric Peak

The in situ electrocrystallization of zinc tetracyanoquinodimethane (TCNQ) has been explored using synchrotron radiation-grazing incidence X-ray diffraction (SR-GIXRD) at potentials in the region of the cyclic voltammetric peak where reduction of TCNQ to TCNQ– occurs at a Pt electrode in acetonitrile (0.1 M [NBu4][PF6]) solution containing Zn(NO3)2·6H2O. The in situ SR-GIXRD data along with ex situ IR and Raman spectroscopy results all confirmed the formation of the kinetically favoured phase of Zn[TCNQ]2(H2O)2 as the product.

In Situ Characterization of Waters of Hydration in a Variable-Hydrate Active Pharmaceutical Ingredient Using 35Cl Solid-State NMR and X-ray Diffraction

2019 ◽  
Vol 19 (12) ◽  
pp. 7349-7362 ◽  
Author(s):  
David A. Hirsh ◽  
Sean T. Holmes ◽  
Paroma Chakravarty ◽  
Austin A. Peach ◽  
Antonio G. DiPasquale ◽  
...  
Keyword(s):  
Solid State ◽  
Solid State Nmr ◽  
Active Pharmaceutical Ingredient ◽  
X Ray Diffraction ◽  
In Situ Characterization ◽  
X Ray

In situ Characterization Of MBE Grown Surfaces And Interfaces By Grazing Incidence X-Ray Diffraction

1990 ◽  
Author(s):  
R. Pinchaux ◽  
M. Sauvage-Simkin ◽  
J. Massies ◽  
N. Jedrecy ◽  
N. Greiser ◽  
...  
Keyword(s):  
Grazing Incidence ◽  
X Ray Diffraction ◽  
In Situ Characterization ◽  
X Ray ◽  
Surfaces And Interfaces
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