scholarly journals Identification of five newly described bioactive chemical compounds in methanolic extract of Mentha viridis by using gas chromatography - mass spectrometry (GC-MS)

2015 ◽  
Vol 7 (7) ◽  
pp. 107-125 ◽  
Author(s):  
Hadi Hameed Imad ◽  
J Hussein Hussein ◽  
Abdulhasan Kareem Muhanned ◽  
Shihab Hamad Nidaa
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Methanolic Extract ◽  
Chemical Compounds ◽  
Gas Chromatography Mass Spectrometry ◽  
Chromatography Mass Spectrometry

scholarly journals SEPARATION AND IDENTIFICATION OF NORMAL HYDROCARBON, NONADECANE IN THE CABBAGE VEGETABLES SAMPLES (Brassica oleracea VAR. CAPITATA F. ALBA) BY GAS CHROMATOGRAPHY–MASS SPECTROMETRY

2010 ◽  
Vol 8 (3) ◽  
pp. 380-384
Author(s):  
M. Amzad Hossain ◽  
S. M. Salehuddin ◽  
M. J. Kabir
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Brassica Oleracea ◽  
Methanolic Extract ◽  
Biological Materials ◽  
Gas Chromatography Mass Spectrometry ◽  
Chromatography Mass Spectrometry ◽  
Identification And Quantification

Toxic normal hydrocarbon (NH), nonadecane in the methanolic extract of the whole of cabbage samples collected from different districts of Bangladesh was analyzed by GC-MS. It was observed that NH deposition on the samples takes place in different morphological parts of the biological materials. The NH, nonadecane, was found in the cabbage samples collected from the highway road side by the extraction of methanol. The identification and quantification of the title compounds have not been reported previously in the cabbage sample.   Keywords: Cabbage; brassica oleracea var. capitata f. alba; quantification; normal hydrocarbon, nonadecane, GC-MS

scholarly journals DETECTION OF PHYTOCHEMICAL CONSTITUENT IN FLOWERS OF VIOLA ODORATA BY GAS CHROMATOGRAPHY-MASS SPECTROMETRY

2018 ◽  
Vol 11 (5) ◽  
pp. 262 ◽  
Author(s):  
Shaimaa Fakhri Jasim ◽  
Noor Nihad Baqer ◽  
Esam Abd Alraheem
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Methanolic Extract ◽  
Gas Chromatography Mass Spectrometry ◽  
Viola Odorata ◽  
Chromatography Mass Spectrometry ◽  
Benzenedicarboxylic Acid ◽  
Medical Importance ◽  
Anti Hiv ◽  
Phytochemical Constituent

Objective: Viola odorata has a characteristic as antifungal, antibacterial, anticancer, antioxidant, antiasthmatic, anti-inflammatory, anti-HIV, and antipyretic agents. The aim of this study was detected about bioactive compounds in the methanolic extract of V. odorata. Methods: The methanolic extract was analyzed through gas chromatography-mass spectrometry (GC-MS) for the identification of different compounds.Results: The current study investigated about phytochemicals in flowers of V. odorata. GC-MS analysis of the methanol extract of flowers showed 84 compounds. The highest concentration was for components which include ethanol, 2-(9,12-octadecadienyl oxy) -, (Z,Z)-; pentadecanoic acid; 1-pentacosanol; 1-pentacosanol; 2-furan carboxaldehyde, 5-(hydroxymethyl)-; 1,2 benzenedicarboxylic acid, diisooctyl ester; and docosane, 11-butyl- and gamma-sitosterol. The peak area and retention time for each components, respectively, were (15.709, 25.51%), (14.015, 19.51%), (29.914, 4.69%), (27.292, 3.95%), (5.707, 4.05%), (20.357, 3.91%), (18.289, 2.48%), and (30.431, 2.37%). While the others components ranged the peak area from 2.03% to 0.05%.Conclusions: These results indicate that the flowers of V. odorata contain the numerous components which have medical importance and this study was one of the first studies to detect phytochemicals in V. odorata.

scholarly journals ANALYSIS OF CHEMICAL COMPOUNDS OF AGARWOOD OIL FROM DIFFERENT SPECIES BY GAS CHROMATOGRAPHY MASS SPECTROMETRY (GCMS)

2014 ◽  
Vol 15 (1) ◽  
Author(s):  
Yumi Zuhanis Has-Yun Hashim ◽  
Nur Izzah Ismail ◽  
Phirdaous Abbas
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Chemical Compounds ◽  
Gas Chromatography Mass Spectrometry ◽  
Chemical Components ◽  
Chromatography Mass Spectrometry ◽  
Three Samples ◽  
Pleasant Odour ◽  
Agarwood Resin ◽  
Agarwood Oil

ABSTRACT: Agarwood oil is a highly prized type of oil due to its unique aroma. The oil is extracted from the fragrant resin found in the agarwood tree (trunk).  The unique aroma and quality of agarwood resin and oil are contributed by the presence of certain chemical compounds. In this work, analysis and comparison of the chemical compounds of agarwood oil from A. malaccensis, A. sub-integra and a mixture of both were conducted.  The essential oils were diluted in hexane (5%) prior to gas chromatography mass spectrometry (GCMS) analysis performed using Agilent GCMS 7890A coupled with MSD quadrupole detector 5975 C.  Separation of analytes by gas chromatography was carried out using a Hewlett Packard HP-5MS silica capillary column (30 m X 0.25 mm X 0.25 mm). A total of 107 compounds were identified from the three samples of agarwood oils. Fifty-five (55) components were identified in A. malaccensis sample which contributes to the largest portion of the total compounds. About 20% of the compounds identified were aromatic and sesquiterpenes which have been revealed to be the main active compounds of agarwood oils which also give the aroma and pleasant odour of agarwood. Different compositions or profile of chemical components were found in agarwood oils from the two different species. Two compounds were commonly identified in all three samples namely 3-phenyl-2-butanone and alpha-cubebene.  Further studies are needed to refine the results which later can be used to assist detection and authentication of agarwood as well as its scientific-based grading. ABSTRAK: Minyak gaharu merupakan sejenis minyak beraroma unik yang mendapat permintaan tinggi dan mahal. Minyak ini diekstrak daripada resin beraroma yang terbentuk di dalam batang pokok gaharu. Keunikan aroma dan kualiti resin dan minyak gaharu ini bergantung kepada kehadiran bahan kimia tertentu. Penyelidikan ini menjurus kepada analisis dan perbandingan bahan-bahan kimia yang terdapat dalam minyak gaharu daripada spesis A. malaccensis, A. sub-integra dan campuran kedua-duanya. Minyak gaharu dilarutkan di dalam 5% heksana sebelum dianalisis menggunakan kromatografi gas Agilent GCMS 7890A berserta spektormetri jisim (MSD quadrupole detector 5975 C). Kolum kapilari silika Hewlet Packard HP-5MS (30 m X 0.25 mm X 0.25 mm) digunakan untuk pemisahan bahan-bahan kimia tersebut. Sejumlah 107 kompaun dikenalpasti dalam ketiga-tiga sampel minyak gaharu tersebut dengan 55 kompaun didapati di dalam sample A. malaccensis. Ini merupakan bahagian terbesar daripada keseluruhan kompaun. Sebanyak 20 % daripada keseluruhan kompaun yang dikenalpasti adalah daripada kumpulan seskuiterpena dan bersifat aromatik, juga merupakan kumpulan yang bertanggungjawab memberi aroma yang unik kepada minyak gaharu. Setiap spesis didapati mempunyai komposisi atau profil bahan kimia yang tersendiri. Dua kompaun iaitu 3-phenyl-2-butanone dan alpha-cubebene ditemui dalam ketiga-tiga sample yang dianalisis. Kajian lanjut adalah perlu untuk memurnikan dapatan hasil penyelidikan yang berpotensi bagi membantu pengenalpastian gaharu berserta pembangunan penggredan gaharu yang lebih saintifik.

scholarly journals GAS CHROMATOGRAPHY-MASS SPECTROMETRY ANALYSIS OF METHANOLIC LEAF EXTRACT OF CASSIA ANGUSTIFOLIA VAHL.

2016 ◽  
Vol 9 (9) ◽  
pp. 111 ◽  
Author(s):  
Shahina Parveen ◽  
Anwar Shahzad ◽  
Anamica Upadhyay ◽  
Vikas Yadav
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Vitamin E ◽  
Leaf Extract ◽  
Methanolic Extract ◽  
Mass Spectrometry Analysis ◽  
Gas Chromatography Mass Spectrometry ◽  
Spectrometry Analysis ◽  
Cassia Angustifolia ◽  
Chromatography Mass Spectrometry

ABSTRACTObjective: The leaves of Cassia angustifolia Vahl. are employed for the treatment of several human diseases. Therefore, the present study wasundertaken to determine the phytocomponents present in the methanolic extract of the leaves by gas chromatography-mass spectrometry (GC-MS)Methods: The collected leaf samples were dried and extracted in methanol. Screening of the extract was done by GC-MS which is an importanttechnique for the separation and identification of different phytochemicals.Results: The methanolic extract of the leaves of C. angustifolia revealed the presence of 45 different phytochemicals. The prevailing compounds were1 butanol, 3 methyl acetate (area % 7.47), 6, 6-dideutero-nonen-1-Ol-3 (area % 10.45), pentadecanoic acid (area % 9.22), and squalene (area %12.30). Vitamin E (area % 3.85) has also been found in the leaf extract. Some of the compounds possess biological activities.Conclusions: It can be concluded from the present study that some of the identified phytochemicals could be responsible for the medicinal value orbiological activity of the plant leaves.Keywords: Senna, Leaf extract, Methanol, Gas chromatography-mass spectrometry, Phytochemicals, Vitamin E.

scholarly journals Chemical Compound Of Liquid Smoke Derived From Leaf Of Piper betle L And Piper crocatum Ruiz & Pav

2018 ◽  
Vol 9 (1) ◽  
pp. 35-43
Author(s):  
Dodi Irwandi ◽  
Ai Emalia Sukmawati ◽  
Dian Maria Ulfah
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Chemical Compound ◽  
Chemical Compounds ◽  
Gas Chromatography Mass Spectrometry ◽  
Piper Betle ◽  
Test Results ◽  
Betel Leaf ◽  
Liquid Smoke ◽  
Chromatography Mass Spectrometry

Liquid smoke made from green betel leaf (Piper betle L) and red betel leaf (Piper crocatum Ruiz & Pav) has been made by pyrolysis. To determine the allegations of the chemical compounds contained in these two liquid smoke, they were tested by Gas Chromatography–Mass Spectrometry (GC-MS) method. Based on the test results it was found that there were 7 suspected compounds in the liquid smoke of green betel leaf and 30 compounds in red betel liquid smoke. The main compounds contained in the liquid smoke of green betel leaf are Isamoxole as the anti-allergic, 5,10-Diethoxy-2,3,7,8-tetrahydro-1H, 6H-dipyrrolo [1,2-a; 1', 2'-d ] Pyrazine as an antifungal and 3,5-Dimethoxyphenol has the potential to be antibacterial while in red betel leaves are 4- (1H-1,3-Benzodiazol-2-yl) phenol and Benzene, 1,2,3-trimethoxy-5- (2 -propenyl) - Bioactivity potential of the two compounds has not been found.

scholarly journals SCREENING OF BIOACTIVE COMPOUNDS FROM UNKNOWN MARINE SPONGES COLLECTED FROM KOVALAM, CHENNAI

2017 ◽  
Vol 10 (5) ◽  
pp. 231 ◽  
Author(s):  
Yuvarani Thambidurai ◽  
Skm Habeeb ◽  
Joe Kizhakudan ◽  
Sudarsanam D
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Secondary Metabolites ◽  
Bioactive Compounds ◽  
Chemical Compounds ◽  
Marine Sponges ◽  
Gas Chromatography Mass Spectrometry ◽  
Chromatography Mass Spectrometry ◽  
Ms Analysis ◽  
Dysidea Herbacea

Objective: This study is designed to hunt for the presence of bioactive compounds from three marine sponges collected from Kovalam.Methods: Zoochemical analysis is performed to screen for the presence of secondary metabolites. Based on those results, only two sponges which showed a significant presence of secondary metabolites has been subjected to gas chromatography-mass spectrometry (GC-MS) analysis to identify the unknown chemical compounds present in those sponges.Results: On analyzing the results, two sponges, namely, Dysidea herbacea and Sigmadocia pumila, has shown a significant presence of secondary metabolites while the third sponge Acanthella elongata have shown moderate presence of secondary metabolites. Since the first two sponges results are remarkable, these two samples have been subjected to GC-MS analysis to separate and identify the unknown chemical compounds present in the sample.Conclusion: Samples, namely, D. herbacea and S. pumila, indicated the presence of several components. From both the sponges, eleven different secondary metabolites were identified by GC-MS. Most of these compounds are widely used in cosmetic, pharmaceutical, and other industries and therefore a vital source for industrial biotechnology and related products in healthcare and skincare.Keywords: Dysidea herbacea, Sigmadocia pumila, Acanthella elongata, Secondary metabolites, Gas chromatography-mass spectrometry analysis, Bioactive compounds.

scholarly journals Phytochemical Constituents of Leaves Essential oils of Achillea fragrantissima (Asteraceae) from Iraq

2018 ◽  
Vol 6 (2) ◽  
pp. 56
Author(s):  
Karzan O. Qader ◽  
Sahar A.A. Malik Al-Saadi ◽  
Ibrahim M. Faraj
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Essential Oil ◽  
Essential Oils ◽  
Chemical Compounds ◽  
Gas Chromatography Mass Spectrometry ◽  
Chromatography Mass Spectrometry ◽  
Achillea Fragrantissima ◽  
Phytochemical Constituents

Essential oils of Achillea fragrantissima extract were prepared and analyzed by gas chromatography–mass spectrometry (GC-MS). A total of 57 phytochemical constituents of chemical compounds were identified in leaves of A. fragrantissima. The major constituents of the essential oil were camphor (34.50%), 1, 8-cineole (14.60%), artemisia ketone (10.25%), and 3-thujanone (7.82%). In addition, 43 components were present at <1%. From the 57 identified compounds, four of them was sesquiterpenes (7.01%), whereas 35 compounds were monoterpenes (61.40%).

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