Mechanical Stability Test for Hevea Latex

1950 ◽  
Vol 23 (4) ◽  
pp. 981-994
Author(s):  
H. G. Dawson

Abstract The mechanical stability test is a rapid, simple method of estimating the colloidal stability or quality of Hevea latex by high-speed stirring. Latex particles start to agglomerate as soon as the peripheral speed of the agitator reaches a certain minimum value. Progressive flocculation continues until mechanical coagulation occurs. The end point is defined as the time in seconds required to coagulate 0.5 to 1.0 per cent of the total solids. If the shear is constant, the time is proportional to the colloidal stability, which depends upon the interfacial film between the latex particles and the serum. The mechanical stability time depends critically on the size, the total solids, and the temperature of sample.

Author(s):  
Porntip Rojruthai ◽  
Narueporn Payungwong ◽  
Jitladda T Sakdapipanich

A model study on the influence of some heavy metal ions on the stability and vulcanization efficiency of uncompounded and compounded high-ammonia natural rubber (HANR) latex was carried out by an exogenous addition and then determined by Brookfield viscometer, mechanical stability time (MST) tester, and tensile testing machine. The case of pre-vulcanized HANR latex with different aging times was determined by the change in the volatile fatty acid (VFA) number, MST, and viscosity. The compounded HANR latex was coagulated by adding Mn2+and Mg2+ while it was unaltered by adding Zn2+, Fe2+, and Cu2+ ions, leading to their colloidal stability. Therefore, these metal ions were chosen further to study the pre-vulcanization of compounded HANR latex. The presence of Zn2+, Fe2+, and Cu2+ in the latex is responsible for the delay in the vulcanization process and changes the appearance of compounded latex. Before compounding, the addition of such metal ions led to the reduction in tensile strength of the obtained gloves. At the same time, there was no effect on the tensile properties of the gloves made from the compounded HANR latex containing the metal ions.


Author(s):  
Tomáš Hrnčíř ◽  
Marek Šikula ◽  
Jozef Vincenc Oboňa ◽  
Pascal Gounet

Abstract High speed FIB cross-sectioning of polyimide material was traditionally very difficult because of artifacts created by FIB on the cross section plane. Therefore we propose a simple method, which retains the high speed of the FIB process, but significantly improves the quality of the cross section plane. The method involves a hard mask positioned close to the intended place of the cross section using a precise manipulator. This then enables highly accurate and site-specific FIB cross-sectioning. Cross sections can be made very quickly and with the excellent quality in comparison to standard procedures based on gas-assisted deposition of a protection layer.


2020 ◽  
Vol 16 (4) ◽  
pp. 617-624 ◽  
Author(s):  
Yao Feng ◽  
Ran Wang ◽  
Juanjuan Yin ◽  
Fangke Zhan ◽  
Kaiyue Chen ◽  
...  

Background: 4-nitrophenol (4-NP) is one of the pollutants in sewage and harmful to human health and the environment. Cu is a non-noble metal with catalytic reduction effect on nitro compounds, and.has the advantages of simple preparation, abundant reserves, and low price. Carbon nanotubes (CNT) are widely used for substrate due to their excellent mechanical stability and high surface area. In this study, a simple method to prepare CNT-Cu2O by controlling different reaction time was reported. The prepared nanocomposites were used to catalyze 4-NP. Methods: CNTs and CuCl2 solution were put into a beaker, and then ascorbic acid and NaOH were added while continuously stirring. The reaction was carried out for a sufficiently long period of time at 60°C. The prepared samples were dried in a vacuum at 50°C for 48 h after washing with ethyl alcohol and deionized water. Results: Nanostructures of these composites were characterized by scanning electron microscope and transmission electron microscopy techniques, and the results at a magnification of 200 nanometers showed that Cu2O was distributed on the surface of the CNTs. In addition, X-ray diffraction was performed to further confirm the formation of Cu2O nanoparticles. The results of ultraviolet spectrophotometry showed that the catalytic effect of the compound on 4-NP was obvious. Conclusions: CNTs acted as a huge template for loading Cu2O nanoparticles, which could improve the stability and cycle performance of Cu2O. The formation of nanoparticles was greatly affected by temperature and the appropriate concentration, showing great reducibility for the 4-NP reduction reaction.


Author(s):  
Dongjun Yang ◽  
Wongyu Lee ◽  
Jehyeok Oh

Although the use of audio feedback with devices such as metronomes during cardiopulmonary resuscitation (CPR) is a simple method for improving CPR quality, its effect on the quality of pediatric CPR has not been adequately evaluated. In this study, 64 healthcare providers performed CPR (with one- and two-handed chest compression (OHCC and THCC, respectively)) on a pediatric resuscitation manikin (Resusci Junior QCPR), with and without audio feedback using a metronome (110 beats/min). CPR was performed on the floor, with a compression-to-ventilation ratio of 30:2. For both OHCC and THCC, the rate of achievement of an adequate compression rate during CPR was significantly higher when performed with metronome feedback than that without metronome feedback (CPR with vs. without feedback: 100.0% (99.0, 100.0) vs. 94.0% (69.0, 99.0), p < 0.001, for OHCC, and 100.0% (98.5, 100.0) vs. 91.0% (34.5, 98.5), p < 0.001, for THCC). However, the rate of achievement of adequate compression depth during the CPR performed was significantly higher without metronome feedback than that with metronome feedback (CPR with vs. without feedback: 95.0% (23.5, 99.5) vs. 98.5% (77.5, 100.0), p = 0.004, for OHCC, and 99.0% (95.5, 100.0) vs. 100.0% (99.0, 100.0), p = 0.003, for THCC). Although metronome feedback during pediatric CPR could increase the rate of achievement of adequate compression rates, it could cause decreased compression depth.


2017 ◽  
Vol 09 (05) ◽  
pp. 1750064 ◽  
Author(s):  
A. Van Hirtum ◽  
X. Pelorson

Experiments on mechanical deformable vocal folds replicas are important in physical studies of human voice production to understand the underlying fluid–structure interaction. At current date, most experiments are performed for constant initial conditions with respect to structural as well as geometrical features. Varying those conditions requires manual intervention, which might affect reproducibility and hence the quality of experimental results. In this work, a setup is described which allows setting elastic and geometrical initial conditions in an automated way for a deformable vocal fold replica. High-speed imaging is integrated in the setup in order to decorrelate elastic and geometrical features. This way, reproducible, accurate and systematic measurements can be performed for prescribed initial conditions of glottal area, mean upstream pressure and vocal fold elasticity. Moreover, quantification of geometrical features during auto-oscillation is shown to contribute to the experimental characterization and understanding.


Author(s):  
Adel Abidi ◽  
Sahbi Ben Salem ◽  
Mohamed Athmane Yallese

Among advanced cutting methods, High Speed Milling (HSM) is often recommended to improve the productivity and to reduce the costs of machining parts. As every cutting process, HSM is characterized by some defects like surface roughness and delamination are the main defects generated in composite materials. The aim of this experimental work is the studying of the machining quality of woven Carbon fiber reinforced plastics (CFRP) using the HSM technology. Experiments were done using different machining parameters combinations to make opened holes in CFRP laminates. This study investigated the effect of cutting speed, orbital feed speed, hole diameter on the delamination defect and surface roughness responses generated in the drilled holes. The design of experimental tests was generated using the approach of Central Composite Design (CCD). The characterization of these responses was treated with the Analysis of variance (ANOVA) and Response surface methodology (RSM). Results showed that the surface roughness is highly affected by the orbital feed speed (F) with contribution of 22.45%. The delamination factor at entry and exit of holes is strongly influenced by the hole diameter D (25.97% and 57.43%) respectively. The developed model equations gave a good correlation between the empirical and predicted results. The optimization of the milling parameters was treated using desirability function to minimize the surface roughness (Ra) and the delamination factor simultaneously.


Author(s):  
Nguyen Duy Canh ◽  
Nguyen Van Canh ◽  
Pham Xuan Hong ◽  
Nguyen Ngoc Hue ◽  
Tran Dinh Duy

2009 ◽  
Author(s):  
Naotoshi Fujita ◽  
Asumi Yamazaki ◽  
Katsuhiro Ichikawa ◽  
Yoshie Kodera

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