scholarly journals Influence of the Chemical Composition of the Used Powder on the Fatigue Behavior of Additively Manufactured Materials

Metals ◽  
2019 ◽  
Vol 9 (12) ◽  
pp. 1285
Author(s):  
Bastian Blinn ◽  
Florian Krebs ◽  
Maximilian Ley ◽  
Christopher Gläßner ◽  
Marek Smaga ◽  
...  

To exploit the whole potential of Additive Manufacturing (AM), a sound knowledge about the mechanical and especially cyclic properties of AM materials as well as their dependency on the process parameters is indispensable. In the presented work, the influence of chemical composition of the used powder on the fatigue behavior of Selectively Laser Melted (SLM) and Laser Deposition Welded (LDW) specimens made of austenitic stainless steel AISI 316L was investigated. Therefore, in each manufacturing process two variations of chemical composition of the used powder were utilized. For qualitative characterization of the materials cyclic deformation behavior, load increase tests (LITs) were performed and further used for the physically based lifetime calculation method (PhyBaLLIT), enabling an efficient determination of stress (S)–number of cycles to failure (Nf) curves (S–Nf), which show excellent correlation to additionally performed constant amplitude tests (CATs). Moreover, instrumented cyclic indentation tests (PhyBaLCHT) were utilized to characterize the materials’ defect tolerance in a comparably short time. All material variants exhibit a high influence of microstructural defects on the fatigue properties. Consequently, for the SLM process a higher fatigue lifetime at lower stress amplitudes could be observed for the batch with a higher defect tolerance, resulting from a more pronounced deformation induced austenite–α’-martensite transformation. In correspondence to that, the batch of LDW material with an increased defect tolerance exhibit a higher fatigue strength. However, the differences in defect tolerance between the LDW batches is only slightly influenced by phase transformation and seems to be mainly governed by differences in hardening potential of the austenitic microstructure. Furthermore, a significantly higher fatigue strength could be observed for SLM material in relation to LDW specimens, because of a refined microstructure and smaller microstructural defects of SLM specimens.

Metals ◽  
2019 ◽  
Vol 9 (8) ◽  
pp. 843 ◽  
Author(s):  
André Reck ◽  
André Till Zeuner ◽  
Martina Zimmermann

The study presented investigates the fatigue strength of the (α+β) Ti-6Al-4V-ELI titanium alloy processed by laser cutting with and without mechanical post-processing. The surface quality and possible notch effects as a consequence of non-optimized intermediate cutting parameters are characterized and evaluated. The microstructural changes in the heat-affected zone (HAZ) are documented in detail and compared to samples with a mechanically post-processed (barrel grinding, mechanical polishing) surface condition. The obtained results show a significant increase (≈50%) in fatigue strength due to mechanical post-processing correlating with decreased surface roughness and minimized notch effects when compared to the surface quality of the non-optimized laser cutting. The martensitic α’-phase is detected in the HAZ with the formation of distinctive zones compared to the initial equiaxial α+β microstructure. The HAZ could be removed up to 50% by means of barrel grinding and up to 100% through mechanical polishing. A fracture analysis revealed that the fatigue cracks always initiate on the laser-cut edges in the as-cut surface condition, which could be assigned to an irregular macro and micro-notch relief. However, the typical characteristics of the non-optimized laser cutting process (melting drops and significant higher surface roughness) lead to early fatigue failure. The fatigue cracks solely started from the micro-notches of the surface relief and not from the dross. As a consequence, the fatigue properties are dominated by these notches, which lead to significant scatter, as well as decreased fatigue strength compared to the surface conditions with mechanical finishing and better surface quality. With optimized laser-cutting conditions, HAZ will be minimized, and surface roughness strongly decreased, which will lead to significantly improved fatigue strength.


2018 ◽  
Vol 165 ◽  
pp. 06001 ◽  
Author(s):  
André Reck ◽  
Stefan Pilz ◽  
Ulrich Thormann ◽  
Volker Alt ◽  
Annett Gebert ◽  
...  

This study examined the fatigue properties of a newly developed cast and thermomechanical processed (β)-Ti-40Nb alloy for a possible application as biomedical alloy due to exceptional low Young’s modulus (64-73 GPa), high corrosion resistance and ductility (20-26%). Focusing on the influence of two microstructural states with fully recrystallized β-grain structure as well as an aged condition with nanometer-sized ω-precipitates, tension-compression fatigue tests (R=-1) were carried out under lab-air and showed significant differences depending on the β-phase stability under cyclic loading. Present ω- precipitates stabilized the β-phase against martensitic α’’ phase transformations leading to an increased fatigue limit of 288 MPa compared to the recrystallized state (225 MPa), where mechanical polishing and subsequent cyclic loading led to formation of α’’-phase due to the metastability of the β-phase. Additional studied commercially available (β)-Ti-45Nb alloy revealed slightly higher fatigue strength (300 MPa) and suggest a change in the dominating cyclic deformation mechanisms according to the sensitive dependence on the Nb-content. Further tests in simulated body fluid (SBF) at 37°C showed no decrease in fatigue strength due to the effect of corrosion and prove the excellent corrosion fatigue resistance of this alloy type under given test conditions.


2016 ◽  
Vol 2016 ◽  
pp. 1-9 ◽  
Author(s):  
Y. Fan ◽  
W. Tian ◽  
Y. Guo ◽  
Z. Sun ◽  
J. Xu

The microstructures of Ti6Al4V are complex and strongly affect its mechanical properties and fatigue behavior. This paper investigates the role of microstructure on mechanical and fatigue properties of thin-section Ti6Al4V sheets, with the aim of reviewing the effects of microstructure on fatigue properties where suboptimal microstructures might result following heat treatment of assemblies that may not be suited to further annealing, for example, following laser welding. Samples of Ti6Al4V sheet were subjected to a range of heat treatments, including annealing and water quenching from temperatures ranging from 650°C to 1050°C. Micrographs of these samples were inspected for microstructure, and hardness, 0.2% proof stress, elongation, and fracture strength were measured and attributed back to microstructure. Fractography was used to support the findings from microstructure and mechanical analyses. The strength ranking from high to low for the microstructures of thin Ti6Al4V sheets observed in this study is as follows: acicularα′martensite, Widmanstätten, bimodal, and equiaxed microstructure. The fatigue strength ranking from high to low is as follows: equiaxed, bimodal, Widmanstätten, and acicularα′martensite microstructure.


Metals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1510
Author(s):  
Abootorab Baqerzadeh Chehreh ◽  
Michael Grätzel ◽  
Jean Pierre Bergmann ◽  
Frank Walther

The load increase method, which is highly efficient in rapidly identifying the fatigue performance and strength of materials, is used in this study to investigate friction stir welded (FSW) EN AW-5754 aluminum alloys. Previous investigations have demonstrated the accuracy and efficiency of this method compared to Woehler tests. In this study, it is shown that the load increase method is a valid, accurate and efficient method for describing the fatigue behavior of FSW weld seams. The specimen tests were performed on 2 mm thick aluminum sheets using conventional and stationary tool configurations. It is shown that an increase in fatigue strength of the FSW EN AW-5754 aluminum alloys can be achieved by using the stationary shoulder tool configuration rather than the conventional one.


2014 ◽  
Vol 598 ◽  
pp. 13-19
Author(s):  
Ewelina Böhm ◽  
Tadeusz Łagoda

The paper presents an analysis of aluminium and its alloys in terms of fatigue strength. The paper contains information in terms of cyclic fatigue tests of aluminium alloys. On the basis of available literature data, Basquin fatigue characteristics have been designated. On their basis a comparison between chosen fatigue characteristics of aluminium alloys with different chemical composition and element percentage in the substance have been done.


Materials ◽  
2020 ◽  
Vol 13 (11) ◽  
pp. 2486
Author(s):  
Mirko Teschke ◽  
Julian Rozo Vasquez ◽  
Lukas Lücker ◽  
Frank Walther

In continuous casting processes, inevitable voids (damage) are generated inside the material. The subsequent forming process of hot flat rolling offers the potential of healing these defects by closing the voids and bonding the internal surfaces. In this paper, different forming conditions from hot flat rolling process were characterized with micromagnetic measurement techniques and the influence of the damage evolution on the fatigue behavior was investigated. To characterize the reduction of voids through hot flat rolling processes, nondestructive testing techniques are required. Therefore, micromagnetic measurements such as Barkhausen noise, incremental permeability, and harmonic analysis were carried out, correlated with the number of voids, and compared with each other. The influence of damage evolution of different forming conditions on the fatigue behavior was characterized based on instrumented constant amplitude and multiple amplitude (load increase) tests. A significant increase in fatigue strength due to the hot flat rolling process, which leads to a reduction in the number of voids, was observed. In addition, the fracture surfaces of the specimens were analyzed in the scanning electron microscope.


2019 ◽  
Vol 9 (9) ◽  
pp. 1001-1008 ◽  
Author(s):  
Li-Hui Zhao ◽  
Hong-Chang Cai ◽  
Shuo Weng ◽  
Song-Lin Zheng

The present research envisages the effects of different uniaxial tensile pre-strain levels on the fatigue properties of the SAPH440 steel. The S-N curves of different pre-strain levels (0%, 6%, 12%, 18%) were drawn using different load levels, with a stress ratio R = –1. The test results show that the fatigue strength of the SAPH440 steel increased with an increasement in the uniaxial tensile pre-strain levels. The static tensile test was carried out on different uniaxial tensile and different pre-strain levels specimens. The results show that with an increase in the uniaxial tensile pre-strain levels, the degree of work hardening of the SAPH440 steel and the static strength increased. Additionally, the hardening index and the elongation at break reduced, while the tensile strength and yield strength increased. TEM (Transmission Electron Microscopy) observation of the test samples with different pre-strain levels showed that the dislocation density of different pre-strain levels specimens increased with an increasement in the pre-strain levels. This resulted in an increasement in the fatigue strength of the SAPH440 steel, the degree of work hardening, and the static strength. However, compared with fatigue strength, the increase of dislocation density has a more significant effect on static strength.


2010 ◽  
Vol 24 (15n16) ◽  
pp. 2502-2505 ◽  
Author(s):  
MD. SHAMIMUR RAHMAN ◽  
TAKESHI KATSUMA ◽  
DAISUKE YONEKURA ◽  
RI-ICHI MURAKAMI

Titanium alloy has an attractive strength-to-weight ratio and good fatigue properties. However, the titanium alloy has very poor wear resistance, therefore, surface treatments must be considered in order to make the contact parts. Hard thin film deposited by PVD technique is well-known to improve the wear resistance. In this study, chromium nitride ( CrN ) film was applied to titanium alloy and its effect on the fatigue behavior was investigated. Ti -6 Al -4 V alloy was used as a substrate material. The CrN film was deposited by arc ion plating (AIP) method at two different negative bias voltages because the film hardness, crystal orientation and surface morphology were strongly depended on the bias voltage during the deposition. Tension-tension fatigue test and tensile test were carried out to investigate the fatigue properties. As the result, the fatigue strength was influenced by the deposition of the CrN film, especially, the fatigue strength was remarkable decreased by the deposition of the CrN film at high negative bias voltage compared to the uncoated specimen and the deposition of the CrN at low negative bias voltage. The difference of the fatigue strength was also investigated on the basis of crack initiating behavior during fatigue test and tensile test.


Author(s):  
H. Kisuki ◽  
M. Sugano ◽  
T. Oshima ◽  
Y. Nasu ◽  
K. Okazaki ◽  
...  

Abstract Fatigue properties of the Al2O3 plasma-sprayed SUS316L stainless steel rod specimens coated on different spraying conditions have been studied in a physiological saline solution (0.9 % NaCl solution) to evaluate the potential of surgical implant application. Fatigue tests were conducted in push-pull loading at the stress ratio of R = -1, and frequency of 2 Hz. Microstructure related with fatigue damage was examined by SEM and TEM. The fatigue strength of Al2O3 plasma-sprayed metals significantly depended on spraying conditions: the effects of spraying on fatigue strength decreased with increasing the applied stress amplitude. As-blasted specimens were higher in fatigue strength than Al2O3 plasma-sprayed specimens. It was found that the plasma spraying had significant effects on fatigue crack growth behavior in the early stage of crack propagation. Fatigue cracks preferentially originated from dents that had been caused on the substrata metal surface subjected to grit-blasting. These results are discussed with both the compressive residual stresses due to the grit blasting which was carried out prior to plasma spraying and the corrosion-resistance of the alumina deposit.


2010 ◽  
Vol 638-642 ◽  
pp. 618-623
Author(s):  
Norio Maruyama

A fretting fatigue test method in a simulated body fluid is shown to evaluate fatigue properties of metallic materials which are used in the orthopaedics field. Next, fatigue/fretting fatigue behavior in a simulated body fluid is given for 316L stainless steel, Ti-6% Al-4% V alloy, pure Ti for industrial use and Co-Cr-Mo alloy. Finally, we discuss the relationship between the tensile strength and the fatigue strength/fretting fatigue strength of metallic biomaterials at 107 cycles in air and in a simulated body fluid. For all of the biomaterials tested, the fatigue strength at 107 cycles is similar in air and in a simulated body fluid. The fatigue strength is closely correlated to the tensile strength: The fatigue strength increases with increasing tensile strength. However, a correlation is not observed between the fretting fatigue strength at 107 cycles and the fatigue strength or the tensile strength.


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