scholarly journals Fabrication, Morphology Analysis, and Mechanical Properties of Ti Foams Manufactured Using the Space Holder Method for Bone Substitute Materials

Metals ◽  
2019 ◽  
Vol 9 (3) ◽  
pp. 340 ◽  
Author(s):  
Oktay Cetinel ◽  
Ziya Esen ◽  
Bora Yildirim

Porous titanium (Ti) offers several key attributes as a biomedical material. Among the known characteristics of Ti relevant to biomedical applications, the mechanical performance and effects of a pore structure on the deformation characteristics under compressive loading were examined. The space holder method was employed to generate Ti foams with target porosities of 60%, 70%, and 80%. A micro-computed to mography analysis and light and scanning electron microscopy were performed to examine the pore morphology and microstructure. The mechanical properties along with the elastic modulus and compressive strength were evaluated via uniaxial compression testing. Ti foam samples with three porosity levels displayed average elastic moduli and compressive strengths comparable with those of human cancellous and cortical bone. All the Ti foam samples had elastic moduli similar to those of cancellous bone with their open porous structures. Although the foam samples with ~60% porosity had compressive strength comparable to that of cortical bone, the samples with ~80% porosity displayed compressive strength similar to that of cancellous bone. The results indicate that Ti foam scaffolds produced using the space holder method have great potential for applications in hard tissue engineering, as their mechanical properties and pore structures are similar to those of bone.

2019 ◽  
Vol 5 (5) ◽  
pp. 1007-1019 ◽  
Author(s):  
Babar Ali ◽  
Liaqat Ali Qureshi ◽  
Ali Raza ◽  
Muhammad Asad Nawaz ◽  
Safi Ur Rehman ◽  
...  

Despite plain cement concrete presenting inferior performance in tension and adverse environmental impacts, it is the most widely used construction material in the world. Consumption of fibers and recycled coarse aggregates (RCA) can add ductility and sustainability to concrete. In this research, two mix series (100%NCA, and 100%RCA) were prepared using four different dosages of GF (0%GF, 0.25%GF, 0.5%GF, and 0.75%GF by volume fraction).  Mechanical properties namely compressive strength, splitting tensile strength, and flexural strength of each concrete mixture was evaluated at the age of 28 days. The results of testing indicated that the addition of GF was very useful in enhancing the split tensile and flexural strength of both RCA and NCA concrete. Compressive strength was not highly sensitive to the addition of GF. The loss in strength that occurred due to the incorporation of RCA was reduced to a large extent upon the inclusion of GF. GF caused significant improvements in the split tensile and flexural strength of RCA concrete. Optimum dosage of GF was determined to be 0.25% for NCA, and 0.5% for RCA concrete respectively, based on the results of combined mechanical performance (MP).


2014 ◽  
Vol 57 ◽  
pp. 712-718 ◽  
Author(s):  
Byounggab Lee ◽  
Taekyung Lee ◽  
Yongmoon Lee ◽  
Dong Jun Lee ◽  
Jiwon Jeong ◽  
...  

Crystals ◽  
2020 ◽  
Vol 10 (10) ◽  
pp. 917
Author(s):  
Penchal Reddy Matli ◽  
Joshua Goh Yong Sheng ◽  
Gururaj Parande ◽  
Vyasaraj Manakari ◽  
Beng Wah Chua ◽  
...  

In this study, hybrid composite consisting of aluminium (Al) shell and magnesium/glass microballoon (Mg-20 wt.% GMB) syntactic composite core was fabricated in a shell-core pattern by combining powder metallurgy and disintegrated melt deposition (DMD) techniques. Physical, microstructural and mechanical properties of as-cast Al and Al/Mg-20GMB hybrid composite were examined. Approximately 13% reduction in density (with respect to aluminium) was realized through the use of a syntactic composite core. Microstructural investigations revealed reasonable interfacial integrity between aluminium shell and Mg-GMB core material and the presence of Al, Mg and GMB phases. The interface region showed a hardness of 109 ± 2 Hv in comparison to the hardness of Al shell region (68 ± 4 Hv) and Mg-20GMB core region (174 ± 5 Hv). In comparison to as-cast Al, the yield strength and ultimate compressive strength of the as-cast Al/Mg-20GMB hybrid composite increased by ~65.4% and ~60%, respectively. Further, the energy absorption under compressive loading for the Al/Mg-20GMB hybrid composite was ~26% higher compared to pure Al. This study validated that Al/Mg-20GMB hybrid composite with superior absolute and specific mechanical properties can be fabricated and used for weight critical applications.


2007 ◽  
Vol 330-332 ◽  
pp. 999-1002 ◽  
Author(s):  
J.P. Li ◽  
J.R. Wijn ◽  
Clemens A. van Blitterswijk ◽  
K. de Groot

The present investigation gives a comparison of the structure and properties of porous Ti6Al4V made by sponge replication (Sponge Ti) and directly 3D fiber deposition (D3DF Ti) and cancellous bone. Although the macrostructure of these two materials differs, their microstructure seems to be similar. Both scaffolds reveal an open pore structure, while D3DF Ti shows a fairly regular open pore structure, sponge Ti6Al4V exhibit an irregular open pore structure similar to that of cancellous bone. The mechanisms resulting in mechanical properties like stiffness or strength are, accordingly, different. The compressive strength and E’ modulus of Ti6Al4V scaffold are higher than that of cancellous bone,. The permeability results show both Ti6Al4V scaffolds are quite comparable with cancellous bone.


2004 ◽  
Vol 844 ◽  
Author(s):  
Amanpreet K. Bembey ◽  
Vanessa Koonjul ◽  
Andrew J. Bushby ◽  
Virginia L. Ferguson ◽  
Alan Boyde

ABSTRACTCortical bone is an anisotropic material, and its mechanical properties are determined by its composition as well as its microstructure. Mechanical properties of bone are a consequence of the proportions of, and the interactions between, mineral, collagen and water. Mid-shaft palmar cortical tissue from the equine third metacarpal bone is relatively dense and uniform with low porosity. The mainly primary osteons are aligned to within a few degrees of the long axis of the bone. Beams of compact cortical bone were prepared to examine effects of dehydration and embedding and to study contribution of collagen and mineral to nano-scale material properties. Five beams were tested: untreated (hydrated); 100% ethanol (dehydrated); or embedded in poly-methylmethacrylate (PMMA) for one normal, one decalcified, and one deproteinated bone sample. Elastic modulus was obtained by nanoindentation using spherical indenters, with the loading direction transverse [1] and longitudinal to the bone axis. By selectively removing water, mineral and organic components from the composite, insights into the ultrastructure of the tissue can be gained from the corresponding changes in the experimentally determined elastic moduli.


Crystals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1331
Author(s):  
Xinjiang Song ◽  
Haibo Xu ◽  
Deqin Zhou ◽  
Kai Yao ◽  
Feifei Tao ◽  
...  

In order to explore the effect of composite materials on the mechanical properties of coastal cement soil, cement soil samples with different iron tailings and nano silica contents were prepared, and unconfined compression and scanning electron microscope tests were carried out. The results show that: (1) The compressive strength of cement soil containing a small amount of iron tailings is improved, and the optimum content of iron tailings is 20%. (2) Nano silica can significantly improve the mechanical properties of iron tailings and cement soil (TCS). When the content of nano silica is 0.5%, 1.5%, and 2.5%, the unconfined compressive strength of nano silica- and iron tailings-modified cement soil (STCS) is 24%, 137%, and 323% higher than TCS, respectively. (3) Nano silica can promote the hydration reaction of cement and promote the cement hydration products to adhere to clay particles to form a relatively stable structure. At the same time, nano silica can fill the pores in TCS and improve the compactness of STCS.


2019 ◽  
Vol 116 (49) ◽  
pp. 24457-24462 ◽  
Author(s):  
Ashley M. Torres ◽  
Adwait A. Trikanad ◽  
Cameron A. Aubin ◽  
Floor M. Lambers ◽  
Marysol Luna ◽  
...  

Microarchitectured materials achieve superior mechanical properties through geometry rather than composition. Although ultralightweight microarchitectured materials can have high stiffness and strength, application to durable devices will require sufficient service life under cyclic loading. Naturally occurring materials provide useful models for high-performance materials. Here, we show that in cancellous bone, a naturally occurring lightweight microarchitectured material, resistance to fatigue failure is sensitive to a microarchitectural trait that has negligible effects on stiffness and strength—the proportion of material oriented transverse to applied loads. Using models generated with additive manufacturing, we show that small increases in the thickness of elements oriented transverse to loading can increase fatigue life by 10 to 100 times, far exceeding what is expected from the associated change in density. Transversely oriented struts enhance resistance to fatigue by acting as sacrificial elements. We show that this mechanism is also present in synthetic microlattice structures, where fatigue life can be altered by 5 to 9 times with only negligible changes in density and stiffness. The effects of microstructure on fatigue life in cancellous bone and lattice structures are described empirically by normalizing stress in traditional stress vs. life (S-N) curves by √ψ, where ψ is the proportion of material oriented transverse to load. The mechanical performance of cancellous bone and microarchitectured materials is enhanced by aligning structural elements with expected loading; our findings demonstrate that this strategy comes at the cost of reduced fatigue life, with consequences to the use of microarchitectured materials in durable devices and to human health in the context of osteoporosis.


Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3244 ◽  
Author(s):  
Francesco Baino ◽  
Elisa Fiume

Porosity is recognized to play a key role in dictating the functional properties of bioactive scaffolds, especially the mechanical performance of the material. The mechanical suitability of brittle ceramic and glass scaffolds for bone tissue engineering applications is usually evaluated on the basis of the compressive strength alone, which is relatively easy to assess. This work aims to investigate the porosity dependence of the elastic properties of silicate scaffolds based on the 45S5 composition. Highly porous glass–ceramic foams were fabricated by the sponge replica method and their elastic modulus, shear modulus, and Poisson’s ratio were experimentally determined by the impulse excitation technique; furthermore, the failure strength was quantified by compressive tests. As the total fractional porosity increased from 0.52 to 0.86, the elastic and shear moduli decreased from 16.5 to 1.2 GPa and from 6.5 to 0.43 GPa, respectively; the compressive strength was also found to decrease from 3.4 to 0.58 MPa, whereas the Poisson’s ratio increased from 0.2692 to 0.3953. The porosity dependences of elastic modulus, shear modulus and compressive strength obeys power-law models, whereas the relationship between Poisson’s ratio and porosity can be described by a linear approximation. These relations can be useful to optimize the design and fabrication of porous biomaterials as well as to predict the mechanical properties of the scaffolds.


2019 ◽  
Vol 2019 ◽  
pp. 1-10
Author(s):  
Shuai Zhang ◽  
Weiguo Qiao ◽  
Yanzhi Li ◽  
Kai Xi ◽  
Pengcheng Chen

Enhancement of the fluidity and mechanical performance of grouting materials has proven to be an effective method of seepage prevention in geotechnical engineering. In this research, a microfine-cement-based grout mixed with microfine fly ash (MFA), nano-CaCO3 (NC), and superplasticizer (SP) was designed to improve the rheological and mechanical properties of grouting materials, and the particle size distribution, fluidity, spreading ability, bleed capacity, setting time, and mechanical properties were studied. A water/solid (W/S) ratio of 1.2 was selected, and the contents of MFA, NC, and SP by mass of microfine cement (MC) were 0–40%, 0–2.0%, and 1.5%, respectively. The results showed that MFA and 1.5% SP improved the fluidity and spreading ability of fresh grouts, while prolonging the setting time. The addition of NC can increase the yield stress and plastic viscosity and decrease the fluidity and spreading ability; nevertheless, it obviously enhances the stability and shortens the setting time of grouts. The addition of MFA and 1.5% SP reduced the compressive strength of hardened grouts; however, the addition of NC improved the mechanical properties.


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