scholarly journals Elastic Mechanical Properties of 45S5-Based Bioactive Glass–Ceramic Scaffolds

Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3244 ◽  
Author(s):  
Francesco Baino ◽  
Elisa Fiume

Porosity is recognized to play a key role in dictating the functional properties of bioactive scaffolds, especially the mechanical performance of the material. The mechanical suitability of brittle ceramic and glass scaffolds for bone tissue engineering applications is usually evaluated on the basis of the compressive strength alone, which is relatively easy to assess. This work aims to investigate the porosity dependence of the elastic properties of silicate scaffolds based on the 45S5 composition. Highly porous glass–ceramic foams were fabricated by the sponge replica method and their elastic modulus, shear modulus, and Poisson’s ratio were experimentally determined by the impulse excitation technique; furthermore, the failure strength was quantified by compressive tests. As the total fractional porosity increased from 0.52 to 0.86, the elastic and shear moduli decreased from 16.5 to 1.2 GPa and from 6.5 to 0.43 GPa, respectively; the compressive strength was also found to decrease from 3.4 to 0.58 MPa, whereas the Poisson’s ratio increased from 0.2692 to 0.3953. The porosity dependences of elastic modulus, shear modulus and compressive strength obeys power-law models, whereas the relationship between Poisson’s ratio and porosity can be described by a linear approximation. These relations can be useful to optimize the design and fabrication of porous biomaterials as well as to predict the mechanical properties of the scaffolds.

Geofluids ◽  
2021 ◽  
Vol 2021 ◽  
pp. 1-9
Author(s):  
Mingxing Gao ◽  
Yongli Liu

Water injection in coal seams will lead to the increase of moisture content in coal, which plays an essential role in the physical and mechanical properties of coal. In order to study the influence of moisture content on the mechanical properties of soft media, the forming pressure (20 MPa) and particle size ratio (0-1 mm (50%), 1-2 mm (25%), and 2-3 mm (25%)) during briquette preparation were firstly determined in this paper. Briquettes with different moisture contents (3%, 6%, 9%, 12%, and 15%) were prepared by using self-developed briquettes. Uniaxial and triaxial compression tests were carried out using the RMT-150C rock mechanics test system. The results show that the uniaxial compressive strength and elastic modulus of briquette samples increase first and then decrease with the increase of briquette water, while Poisson’s ratio decreases first and then increases with the increase of briquette water. When the moisture content is around 9%, the maximum uniaxial compressive strength is 0.866 MPa, the maximum elastic modulus is 1.385 GPa, and Poisson’s ratio is at the minimum of 0.259. The compressive strength of briquettes increases with the increase of confining pressure. With the increase of moisture content, the cohesion and internal friction angle of briquettes first increased and then decreased.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Tanmoy Chatterjee ◽  
Souvik Chakraborty ◽  
Somdatta Goswami ◽  
Sondipon Adhikari ◽  
Michael I. Friswell

AbstractWe demonstrate that the consideration of material uncertainty can dramatically impact the optimal topological micro-structural configuration of mechanical metamaterials. The robust optimization problem is formulated in such a way that it facilitates the emergence of extreme mechanical properties of metamaterials. The algorithm is based on the bi-directional evolutionary topology optimization and energy-based homogenization approach. To simulate additive manufacturing uncertainty, combinations of spatial variation of the elastic modulus and/or, parametric variation of the Poisson’s ratio at the unit cell level are considered. Computationally parallel Monte Carlo simulations are performed to quantify the effect of input material uncertainty to the mechanical properties of interest. Results are shown for four configurations of extreme mechanical properties: (1) maximum bulk modulus (2) maximum shear modulus (3) minimum negative Poisson’s ratio (auxetic metamaterial) and (4) maximum equivalent elastic modulus. The study illustrates the importance of considering uncertainty for topology optimization of metamaterials with extreme mechanical performance. The results reveal that robust design leads to improvement in terms of (1) optimal mean performance (2) least sensitive design, and (3) elastic properties of the metamaterials compared to the corresponding deterministic design. Many interesting topological patterns have been obtained for guiding the extreme material robust design.


2010 ◽  
Vol 25 (3) ◽  
pp. 545-555 ◽  
Author(s):  
Uday Chippada ◽  
Bernard Yurke ◽  
Noshir A. Langrana

Besides biological and chemical cues, cellular behavior has been found to be affected by mechanical cues such as traction forces, surface topology, and in particular the mechanical properties of the substrate. The present study focuses on completely characterizing the bulk linear mechanical properties of such soft substrates, a good example of which are hydrogels. The complete characterization involves the measurement of Young's modulus, shear modulus, and Poisson's ratio of these hydrogels, which is achieved by manipulating nonspherical magnetic microneedles embedded inside them. Translating and rotating these microneedles under the influence of a known force or torque, respectively, allows us to determine the local mechanical properties of the hydrogels. Two specific hydrogels, namely bis-cross-linked polyacrylamide gels and DNA cross-linked polyacrylamide gels were used, and their properties were measured as a function of gel concentration. The bis-cross-linked gels were found to have a Poisson's ratio that varied between 0.38 and 0.49, while for the DNA-cross-linked gels, Poisson's ratio varied between 0.36 and 0.49. The local shear moduli, measured on the 10 μm scale, of these gels were in good agreement with the global shear modulus obtained from a rheology study. Also the local Young's modulus of the hydrogels was compared with the global modulus obtained using bead experiments, and it was observed that the inhomogeneities in the hydrogel increases with increasing cross-linker concentration. This study helps us fully characterize the properties of the substrate, which helps us to better understand the behavior of cells on these substrates.


Materials ◽  
2020 ◽  
Vol 13 (24) ◽  
pp. 5644
Author(s):  
Sun-Youn Ryou ◽  
Chang-Soon Lee ◽  
In-Sik Cho ◽  
Auezhan Amanov

Glass with strong durability and transparency has been in the spotlight in various fields, including displays. Elastic and shear moduli and Poisson’s ratio are important properties of glasses. The purpose of this study is to evaluate the change in mechanical properties, such as the dynamic elastic modulus and Poisson’s ratio, with respect to the chemical strengthening time of glass for display applications, as measured by static and dynamic methods. The basic measurement principle of the dynamic method is to measure acoustic speed or resonant frequency using an ultrasonic generator. The mechanical properties of both non-strengthened and chemically strengthened glasses were investigated. It was found that the strength of the chemically strengthened glass decreased when chemical strengthening time increased. Chemical strengthening increased the bending strength and decreased the elastic modulus due to the introduction of compressive residual stress at the surface.


2020 ◽  
Vol 6 (1) ◽  
pp. 50-56
Author(s):  
Francesco Baino ◽  
Elisa Fiume

AbstractPorosity is known to play a pivotal role in dictating the functional properties of biomedical scaffolds, with special reference to mechanical performance. While compressive strength is relatively easy to be experimentally assessed even for brittle ceramic and glass foams, elastic properties are much more difficult to be reliably estimated. Therefore, describing and, hence, predicting the relationship between porosity and elastic properties based only on the constitutive parameters of the solid material is still a challenge. In this work, we quantitatively compare the predictive capability of a set of different models in describing, over a wide range of porosity, the elastic modulus (7 models), shear modulus (3 models) and Poisson’s ratio (7 models) of bioactive silicate glass-derived scaffolds produced by foam replication. For these types of biomedical materials, the porosity dependence of elastic and shear moduli follows a second-order power-law approximation, whereas the relationship between porosity and Poisson’s ratio is well fitted by a linear equation.


2021 ◽  
Author(s):  
Meng Meng ◽  
Luke Frash ◽  
James Carey ◽  
Wenfeng Li ◽  
Nathan Welch ◽  
...  

Abstract Accurate characterization of oilwell cement mechanical properties is a prerequisite for maintaining long-term wellbore integrity. The drawback of the most widely used technique is unable to measure the mechanical property under in situ curing environment. We developed a high pressure and high temperature vessel that can hydrate cement under downhole conditions and directly measure its elastic modulus and Poisson's ratio at any interested time point without cooling or depressurization. The equipment has been validated by using water and a reasonable bulk modulus of 2.37 GPa was captured. Neat Class G cement was hydrated in this equipment for seven days under axial stress of 40 MPa, and an in situ measurement in the elastic range shows elastic modulus of 37.3 GPa and Poisson's ratio of 0.15. After that, the specimen was taken out from the vessel, and setted up in the triaxial compression platform. Under a similar confining pressure condition, elastic modulus was 23.6 GPa and Possion's ratio was 0.26. We also measured the properties of cement with the same batch of the slurry but cured under ambient conditions. The elastic modulus was 1.63 GPa, and Poisson's ratio was 0.085. Therefore, we found that the curing condition is significant to cement mechanical property, and the traditional cooling or depressurization method could provide mechanical properties that were quite different (50% difference) from the in situ measurement.


Author(s):  
John J. Quicksall ◽  
Robert L. Jackson ◽  
Itzhak Green

This work uses the finite element technique to model the elasto-plastic deformation of a hemisphere contacting a rigid flat for various material properties typical of aluminum, bronze, copper, titanium and malleable cast iron. Additionally, this work conducted parametric FEM tests on a generic material in which the elastic modulus and Poisson’s ratio are varied independently while the yield strength is held constant. A larger spectrum of material properties are covered in this work than in most previous works. The results are compared to two previously formulated elasto-plastic models simulating the deformation of a hemisphere in contact with a rigid flat. Both of the previously formulated models use carbon steel mechanical properties to arrive at empirical formulations implied to pertain to various materials. While both models considered several carbon steels with varying yield strengths, they did not test materials with varying Poisson’s ratio or elastic modulus. The previously generated elasto-plastic models give fairly good predictions when compared to the FEM results for various material properties from the current work, except that one model produces more accurate predictions overall, especially at large deformations where other models neglect important trends due to decreases in “hardness” with increasing deformation.


2017 ◽  
Vol 52 (3) ◽  
pp. 361-372 ◽  
Author(s):  
Gongdai Liu ◽  
R Ghosh ◽  
A Vaziri ◽  
A Hossieni ◽  
D Mousanezhad ◽  
...  

A typical plant leaf can be idealized as a composite having three principal fibers: the central mid-fiber corresponding to the mid-rib, straight parallel secondary fibers attached to the mid-fiber representing the secondary veins, and then another set of parallel fibers emanating from the secondary fibers mimicking the tertiary fibers embedded in a matrix material. This paper introduces a biomimetic composite design inspired by the morphology of venous leafs and investigates the effects of venation morphologies on the in-plane mechanical properties of the biomimetic composites using finite element method. The mechanical properties such as Young’s moduli, Poisson’s ratio, and yield stress under uniaxial loading of the resultant composite structures was studied and the effect of different fiber architectures on these properties was investigated. To this end, two broad types of architectures were used both having similar central main fiber but differing in either having only secondary fibers or additional tertiary fibers. The fiber and matrix volume fractions were kept constant and a comparative parametric study was carried out by varying the inclination of the secondary fibers. The results show that the elastic modulus of composite in the direction of main fiber increases linearly with increasing the angle of the secondary fibers. Furthermore, the elastic modulus is enhanced if the secondary fibers are closed, which mimics composites with closed cellular fibers. In contrast, the elastic modulus of composites normal to the main fiber ( x direction) exponentially decreases with the increase of the angle of the secondary fibers and it is little affected by having secondary fibers closed. Similar results were obtained for the yield stress of the composites. The results also indicate that Poisson’s ratio linearly increases with the secondary fiber angle. The results also show that for a constant fiber volume fraction, addition of various tertiary fibers may not significantly enhance the mechanical properties of the composites. The mechanical properties of the composites are mainly dominated by the secondary fibers. Finally, a simple model was proposed to predict these behaviors.


2020 ◽  
Vol 2020 ◽  
pp. 1-11
Author(s):  
Ke Yang ◽  
Zhen Wei ◽  
Xiaolou Chi ◽  
Yonggang Zhang ◽  
Litong Dou ◽  
...  

Due to the influence of the component structure and combination modes, the mechanical characteristics and failure modes of the coal-rock composite show different characteristics from the monomer. In order to explore the effect of different coal-rock ratios on the deformation and the failure law of the combined sample, the RMT rock mechanics test system and acoustic emission real-time monitoring system are adopted to carry out uniaxial compression tests on coal, sandstone, and three kinds of combined samples. The evolution rules of the mechanical parameters of the combined samples, such as the uniaxial compressive strength, elastic modulus, and Poisson’s ratio, are obtained. The expansion and failure deformation characteristics of the combined sample are analyzed. Furthermore, the evolution laws of the fractal and acoustic emission signals are combined to reveal the crack propagation and failure mechanism of the combined samples. The results show that the compressive strength and elastic modulus of the combined sample increase with the decrease of the coal-rock ratios, and Poisson’s ratio decreases with the decrease of the coal-rock ratios. The strain softening weakens at the postpeak stage, which shows an apparent brittle failure. The combined sample of coal and sandstone has different degrees of damages under load. The coal is first damaged with a high degree of breakage, with obvious tensile failure. The acoustic emission energy value presents different stage characteristics with increasing load. Crackling sound occurs in the destroy section before the sample reaches the peak, along with small coal block ejection and the partial destruction. The energy value fluctuates violently, with the appearance of several peaks. At the postpeak stage, the coal samples expand rapidly with a loud crackling sound in the destroy section, and the energy value increases dramatically. The crack propagation induces the damage in the sandstone; when the energy reaches the limit value, the instantaneous release of elastic energy leads to the overall structural instability.


2011 ◽  
Vol 250-253 ◽  
pp. 1452-1455 ◽  
Author(s):  
Lu Bo Meng ◽  
Tian Bin Li ◽  
Liang Wen Jiang ◽  
Hong Min Ma

High temperature conventional triaxial compression test of shale are carried out by the MTS815 servo-controlled testing machine, based on the experimental results, the relationships between temperature and shale peak strength, elastic modulus, Poisson's ratio, cohesion, internal friction angle are investigated. Although the experimental results are discrete comparatively, the general law is obvious. When the confining pressure imposed on shale is constant and the temperature changes form 25°C to 120°C, with the increasing of the temperature, the triaxial compression strength, shear strength gradually increase, while average elastic modulus, Poisson's ratio has a slightly decrease. The thermal stress generated by the high temperature plays a role to accommodate the deformation and the function of preventing crack propagation, thus the bearing capacity of shale samples are strengthened. But the influence of temperature on shale mechanical properties mutates when the temperature is at 80°C. Shale peak strength dramatically decreased, average elastic modulus decreased slightly, and Poisson's ratio also increased slightly, which indicated that at 80°C, different thermal expansivity of mineral particles of shale may cause cross-grain boundary thermal expansion incongruous, creating additional thermal stress, thus the sample’s bearing capacity decreased.


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