scholarly journals Tribological Properties of Ti2AlNb Matrix Composites Containing Few-Layer Graphene Fabricated by Spark Plasma Sintering

Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 924
Author(s):  
Wei Wang ◽  
Ziru Han ◽  
Qingjuan Wang ◽  
Baojia Wei ◽  
Shewei Xin ◽  
...  
Keyword(s):  
Spark Plasma Sintering ◽  
Tribological Properties ◽  
Matrix Composites ◽  
X Ray Diffraction ◽  
Layer Graphene ◽  
Plasma Sintering ◽  
Ti2alnb Alloy ◽  
The Coefficient Of Friction ◽  
Spark Plasma ◽  
Few Layer Graphene

Ti2AlNb alloys with few-layer graphene were fabricated by spark plasma sintering (SPS) to enhance the tribological properties (TP) of the composite materials. Microstructure characteristics of the original few-layer graphene (FLG), Ti2AlNb powders, and the sintered composites were characterized by X-Ray Diffraction (XRD), scanning electron microscopy (SEM), and Raman spectroscopy. The experimental results indicated that FLGs were homogeneously distributed in the composites. Tribological results indicated that the coefficient of friction (COF) of the composites was reduced as the content of FLG increased. Compared with the pure Ti2AlNb alloy, the average COF of the composite with 1.0 wt.% FLG was decreased by 9.4% and the wear rate was decreased by 36%. Meanwhile, the microstructures of the worn surface showed that TiC particles and friction layers formed by residual FLGs were present on the surface of the composites after tribological test. It is proposed that Ti2AlNb alloys with FLGs presented the enhanced wear resistance.

Microstructure and Properties of TiB2/AlFeNiCoCr Composites by Spark Plasma Sintering

2020 ◽  
Vol 842 ◽  
pp. 83-89
Author(s):  
Dai Hong Xiao ◽  
Min Dong Wu
Keyword(s):  
Spark Plasma Sintering ◽  
Phase Evolution ◽  
High Entropy Alloy ◽  
Matrix Composites ◽  
X Ray Diffraction ◽  
Alloy Matrix ◽  
High Entropy ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Temperature And Pressure

TiB2/AlFeNiCoCr high-entropy-alloy-matrix composites were fabricated by spark plasma sintering. Effects of SPS process on microstructure and mechanical properties of 0.5 vol.% TiB2/AlFeNiCoCr composites were studied using X-ray diffraction, density testing, scanning electron microscopy, mechanical property testing. It is shown that increasing of sintering temperature and pressure can improve the relative density and compressive properties of 5 vol. %TiB2/AlCoCrFeNi composites. During the spark plasma sintering, there is phase evolution in the composites. The 5 vol. % TiB2/AlCoCrFeNi composite after sintering at 1200 °C and 30 ~ 45 MPa is composed of phases BCC, B2, FCC, σ and TiB2.

scholarly journals Microstructure and Properties of TiB2 Composites Produced by Spark Plasma Sintering with the Addition of Ti5Si3

Materials ◽  
2021 ◽  
Vol 14 (14) ◽  
pp. 3812
Author(s):  
Agnieszka Twardowska ◽  
Marcin Podsiadło ◽  
Iwona Sulima ◽  
Krzysztof Bryła ◽  
Paweł Hyjek
Keyword(s):  
Spark Plasma Sintering ◽  
Diffraction Method ◽  
X Ray Diffraction ◽  
Wear Properties ◽  
Plasma Sintering ◽  
Diamond Indenter ◽  
The Coefficient Of Friction ◽  
Spark Plasma ◽  
Sliding Test ◽  
Disc Configuration

Titanium diboride (TiB2) is a hard, refractory material, attractive for a number of applications, including wear-resistant machine parts and tools, but it is difficult to densify. The spark plasma sintering (SPS) method allows producing TiB2-based composites of high density with different sintering aids, among them titanium silicides. In this paper, Ti5Si3 is used as a sintering aid for the sintering of TiB2/10 wt % Ti5Si3 and TiB2/20 wt % Ti5Si3 composites at 1600 °C and 1700 °C for 10 min. The phase composition of the initial powders and produced composites was analyzed by the X-ray diffraction method using CuKα radiation. The microstructure was examined using scanning electron microscopy, accompanied by energy-dispersive spectroscopy (EDS). The hardness was determined using a diamond indenter of Vickers geometry loaded at 9.81 N. Friction–wear properties were tested in the dry sliding test in a ball-on-disc configuration, using WC as a counterpart material. The major phases present in the TiB2/Ti5Si3 composites were TiB2 and Ti5Si3. Traces of TiC were also identified. The hardness of the TiB2/Ti5Si3 composites was in the range of 1860–2056 HV1 and decreased with Ti5Si3 content, as well as the specific wear rate Wv. The coefficient of friction for the composites was in the range of 0.5–0.54, almost the same as for TiB2 sinters. The main mechanism of wear was abrasive.

scholarly journals Microstructure and properties of nano-laminated Y3Si2C2 ceramics fabricated via in situ reaction by spark plasma sintering

2021 ◽  
Vol 10 (3) ◽  
pp. 578-586
Author(s):  
Lin-Kun Shi ◽  
Xiaobing Zhou ◽  
Jian-Qing Dai ◽  
Ke Chen ◽  
Zhengren Huang ◽  
...  
Keyword(s):  
Spark Plasma Sintering ◽  
Atomic Scale ◽  
Max Phase ◽  
X Ray Diffraction ◽  
Selected Area Electron Diffraction ◽  
Plasma Sintering ◽  
Transmission Electron ◽  
Spark Plasma ◽  
Diffraction Patterns

AbstractA nano-laminated Y3Si2C2 ceramic material was successfully synthesized via an in situ reaction between YH2 and SiC using spark plasma sintering technology. A MAX phase-like ternary layered structure of Y3Si2C2 was observed at the atomic-scale by high resolution transmission electron microscopy. The lattice parameters calculated from both X-ray diffraction and selected area electron diffraction patterns are in good agreement with the reported theoretical results. The nano-laminated fracture of kink boundaries, delamination, and slipping were observed at the tip of the Vickers indents. The elastic modulus and Vickers hardness of Y3Si2C2 ceramics (with 5.5 wt% Y2O3) sintered at 1500 °C were 156 and 6.4 GPa, respectively. The corresponding values of thermal and electrical conductivity were 13.7 W·m-1·K-1 and 6.3×105 S·m-1, respectively.

Spark plasma sintering of Ti6Al4V metal matrix composites: Microstructure, mechanical and corrosion properties

2021 ◽  
Vol 865 ◽  
pp. 158875
Author(s):  
Neera Singh ◽  
Raghunandan Ummethala ◽  
Phani Shashanka Karamched ◽  
Rathinavelu Sokkalingam ◽  
Vasanth Gopal ◽  
...  
Keyword(s):  
Metal Matrix Composites ◽  
Spark Plasma Sintering ◽  
Metal Matrix ◽  
Matrix Composites ◽  
Corrosion Properties ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Mechanical And Corrosion Properties

Development of WC-Fe3Al Composites by Spark Plasma Sintering Process

2016 ◽  
Vol 881 ◽  
pp. 307-312
Author(s):  
Luis Antonio C. Ybarra ◽  
Afonso Chimanski ◽  
Sergio Gama ◽  
Ricardo A.G. da Silva ◽  
Izabel Fernanda Machado ◽  
...  
Keyword(s):  
Spark Plasma Sintering ◽  
Zinc Stearate ◽  
Sintering Process ◽  
X Ray Diffraction ◽  
X Ray ◽  
Plasma Sintering ◽  
Al Composite ◽  
Spark Plasma ◽  
Short Time ◽  
Vibration Mill

Tungsten carbide (WC) based composites are usually produced with cobalt, but this binder has the inconvenience of shortage, unstable price and potential carcinogenicity. The objective of this study was to develop WC composite with intermetallic Fe3Al matrix. Powders of WC, iron and aluminum, with composition WC-10 wt% Fe3Al, and 0.5 wt% zinc stearate were milled in a vibration mill for 6 h and sintered in a SPS (spark plasma sintering) furnace at 1150 °C for 8 min under pressure of 30 MPa. Measured density and microstructure analysis showed that the composite had significant densification during the (low-temperature, short time) sintering, and X-ray diffraction analysis showed the formation of intermetallic Fe3Al. Analysis by Vickers indentation resulted in hardness of 11.2 GPa and fracture toughness of 24.6 MPa.m1/2, showing the feasibility of producing dense WC-Fe3Al composite with high mechanical properties using the SPS technique.

Spark Plasma Sintering of Ti-4.5Al-3V-2Fe-2Mo (SP-700)

2010 ◽  
Vol 654-656 ◽  
pp. 819-822
Author(s):  
Genki Kikuchi ◽  
Hiroshi Izui ◽  
Yuya Takahashi ◽  
Shota Fujino
Keyword(s):  
Spark Plasma Sintering ◽  
Room Temperature ◽  
Volume Fraction ◽  
Titanium Boride ◽  
Tensile Tests ◽  
X Ray Diffraction ◽  
X Ray ◽  
Plasma Sintering ◽  
Spark Plasma ◽  
Tib2 Particles

In this study, we focused on the sintering performance of Ti-4.5Al-3V-2Mo-2Fe (SP-700) and mechanical properties of SP-700 reinforced with titanium boride (TiB/SP-700) fabricated by spark plasma sintering (SPS). TiB whiskers formed in titanium by a solid-state reaction of titanium and TiB2 particles were analyzed with scanning electron microscopy and X-ray diffraction. The TiB/SP-700 was sintered at temperatures of 1073, 1173, and 1273 K and a pressure of 70 MPa for 10, 30, and 50 min. The volume fraction of TiB ranged from 1.7 vol.% to 19.9 vol.%. Tensile tests of TiB/SP-700 were conducted at room temperature, and the effect of TiB volume fraction on the tensile properties was investigated.

Formation of Metal-Intermetallic Laminate Composites by Spark Plasma Sintering of Metal Plates and Powder Work Pieces

2014 ◽  
Vol 698 ◽  
pp. 277-282 ◽  
Author(s):  
Daria V. Lazurenko ◽  
Vyacheslav I. Mali ◽  
Alexander Thoemmes
Keyword(s):  
Spark Plasma Sintering ◽  
Titanium Aluminide ◽  
Elevated Temperatures ◽  
Intermetallic Layer ◽  
Functional Materials ◽  
X Ray Diffraction ◽  
Laminate Composites ◽  
Plasma Sintering ◽  
Metal Plates ◽  
Spark Plasma

Laminate composites with an intermetallic component are some of the most prospective constructional and functional materials. The basic formation method of such materials consists in heating a stack composed of metallic plates reacting at elevated temperatures to form intermetallic phases. The temperature of the process is usually approximately equal to a melting point of a more easily fusible component. In this study, an alternative technology of producing a titanium – titanium aluminide composite with a laminate structure is suggested. It consists in combining metallic (titanium and aluminum) powder mixtures pre-sintered at 400 оС with titanium plates, alternate stacking of these components and subsequent spark plasma sintering (SPS) of the fabricated workpieces. Applying this technology allowed for the fabrication of metal-intermetallic laminate (MIL) materials with an inhomogeneous structure of intermetallic interlayers. The phases revealed in the composite by X-Ray diffraction (XRD) were α-Ti, Al, Al3Ti and Al2Ti. Moreover, the results of the energy-dispersive analysis gave the evidence of the formation of Ti-enriched phases in powder layers after SPS. A small number of voids were observed between the structural components of the intermetallic layers. Voids were also detected at “metal-intermetallic” interfaces; however, the quality of connection between different layers in the composite was very high. The microhardness of an intermetallic layer formed in the composite was comparable to the microhardness of the Al3Ti compound. The microhardness of titanium was equal to 1600 MPa.

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