scholarly journals Evaluation of the Flexural Strength, Water Sorption, and Solubility of a Glass Ionomer Dental Cement Modified Using Phytomedicine

Materials ◽  
2020 ◽  
Vol 13 (23) ◽  
pp. 5352
Author(s):  
Lamia Singer ◽  
Gabriele Bierbaum ◽  
Katja Kehl ◽  
Christoph Bourauel
Keyword(s):  
Flexural Strength ◽  
Plant Extract ◽  
Plant Extracts ◽  
Water Sorption ◽  
Testing Machine ◽  
Glass Ionomer Cement ◽  
Biologically Active ◽  
Bending Test ◽  
Glass Ionomer ◽  
Freeze Dried

Various medicinal plant parts and extracts have been proven to be sources of biologically active compounds, many of which have been incorporated in the production of new pharmaceutical compounds. Thus, the aim of this study was to increase the antimicrobial properties of a glass ionomer cement (GIC) through its modification with a mixture of plant extracts, which were evaluated along with a 0.5% chlorohexidine-modified GIC (CHX-GIC) with regard to the water sorption, solubility, and flexural strength. Methods: Salvadora persica, Olea europaea, and Ficus carcia leaves were prepared for extraction with ethyll alcohol using a Soxhlet extractor for 12 h. The plant extract mixture (PE) was added in three different concentrations to the water used for preparation of a conventional freeze-dried GIC (groups 1:1, 2:1, and 1:2). Specimens were then mixed according to the manufacturer’s instructions and tested against the unmodified GIC (control) and a GIC modified with 0.5% chlorhexidine. Water sorption and solubility were evaluated after 7 days of immersion in distilled water. Flexural strength was evaluated in a three-point bending test after 24 h using a universal material testing machine at a crosshead speed of 1 mm/min. One-way analysis of variance (ANOVA) was used for comparison between the groups. Tukey’s post hoc test was used for pairwise comparison when the ANOVA test was significant. Results: There were no statistically significant differences between the control (M = 20.5%), CHX-GIC (M = 19.6%), 1:1 (M = 20.0%), 1:2 (M = 19.5%), and 2:1 (19.7%) groups with regard to the percentage of water sorption, while for water solubility the 2:1 (M = −0.39%) plant-modified group was significantly different from all of the other groups. Flexural strength test results showed that the 2:1 group (M = 26.1 MPa) recorded significantly higher mean values compared to all other tested groups. Conclusion and clinical relevance: The plant extracts did not negatively affect the water sorption and solubility of the GIC, while the flexural strength was improved by the addition of the plant extract at higher concentrations.

scholarly journals Comparative Evaluation of Flexural Strength of Glass Ionomer Cement and Cention N in Artificial Medium Over Time Intervals - An In-Vitro Study

2021 ◽  
Vol 10 (32) ◽  
pp. 2609-2614
Author(s):  
Risana K. ◽  
Prathyusha P ◽  
Amith Adyanthaya ◽  
Aparna Sivaraman ◽  
Nazreen Ayub K ◽  
...  
Keyword(s):  
Flexural Strength ◽  
Artificial Saliva ◽  
Testing Machine ◽  
Glass Ionomer Cement ◽  
Bending Test ◽  
Glass Ionomer ◽  
Time Intervals ◽  
Significant Difference ◽  
Duration Of Storage ◽  
Ionomer Cement

BACKGROUND Glass ionomer cement (GIC) is a versatile restorative cement in paediatric dentistry. Due to its less flexural strength, alternative materials have been developed. Cention N is one such material, but since it’s a new material evidence is lacking regarding its physical properties, especially flexural strength for evaluating its clinical outcome. We wanted to compare the flexural strength of glass ionomer cement and Cention N stored in artificial saliva and its variation over different time intervals, i.e., after 24 hours, 1 week and 4 weeks. METHODS A total of 30 specimens were prepared for GIC (Fuji IX) and Cention N and were further categorized according to the duration of storage time of 24 hours, 1 week and 4 weeks (N = 10). A 3 - point bending test using a universal testing machine was used to evaluate the flexural strength. RESULTS GIC Fuji IX showed a mean flexural strength of 35.296 ± 1.61 Mpa at the end of 24 hours, 47.234 ± 4.12 after 1 week and 66.039 ± 11.05 Mpa at the end of 4 weeks. GIC showed a statistically significant increase of flexural strength from 24 hours to one week and a further increase after 4 weeks of storage. The flexural strength of Cention N at 24 hours was 175.985 ± 22.11 Mpa, at the end of one week was 163.486 ± 17.55 MPa, and after 4 weeks was 175.437 ± 27.22 Mpa. Cention N did not show any statistically significant change in flexural strength value from 24 hours to 4 weeks. Cention N showed highly significant difference between flexural strength compared to GIC at all - time intervals. CONCLUSIONS Cention N has a superior flexural strength compared to GIC at all - time intervals. KEY WORDS Cention N, Flexural Strength, Glass Ionomer Cement

scholarly journals Flexural Strength of Glass Carbomer Cement and Conventional Glass Ionomer Cement Stored in Different Storage Media over Time

2018 ◽  
Vol 27 (4) ◽  
pp. 372-377 ◽  
Author(s):  
Muhammad Ali Faridi ◽  
Abdul Khabeer ◽  
Saad Haroon
Keyword(s):  
Flexural Strength ◽  
Artificial Saliva ◽  
Glass Ionomer Cement ◽  
Bending Test ◽  
Glass Ionomer ◽  
Time Intervals ◽  
Storage Media ◽  
Unique Factor ◽  
Post Hoc ◽  
Ionomer Cement

Objectives: Glass ionomer cement (GIC) is routinely placed as a restorative material in dentistry. However, due to its poor physical properties, its use is limited to cases where the level of stress on restoration is minimal. Improved formulations of GIC have been developed to overcome these drawbacks. The purpose of this study was to evaluate flexural strength of a conventional GIC (Fuji IX) against a newly developed glass carbomer cement (GCP). Materials and Methods: For Fuji IX and GCP, a total of 80 blocks were prepared and divided into 16 groups (n = 5). These groups were further categorized according to the storage medium (artificial saliva and Vaseline) and time intervals (24 h and 1, 2, and 4 weeks). A 3-point bending test was carried out, and statistical analysis was done using ANOVA and Tukey post hoc tests. Results: Fuji IX showed a mean flexural strength of 25.14 ± 13.02 versus 24.27 ± 12.57 MPa for GCP. There was no significant statistical difference between both materials when compared under storage media. Both materials showed the highest value for flexural strength at 2 weeks of storage and lowest at 4 weeks. Conclusion: The storage media do not affect the flexural strength of the specimens with reference to time. Time is the unique factor with relative influence on mean resistance to fracture. Further testing is required to evaluate the true potential of the newly developed GCP.

scholarly journals Evaluation of the antimicrobial activity and compressive strength of a dental cement modified using plant extract mixture

2020 ◽  
Vol 31 (12) ◽  
Author(s):  
Lamia Singer ◽  
Gabriele Bierbaum ◽  
Katja Kehl ◽  
Christoph Bourauel
Keyword(s):  
Antimicrobial Activity ◽  
Compressive Strength ◽  
Plant Extract ◽  
Plant Extracts ◽  
Micrococcus Luteus ◽  
Testing Machine ◽  
Alcoholic Extract ◽  
Dental Cement ◽  
Freeze Dried ◽  
Significant Difference

AbstractLiterature lacks sufficient data regarding addition of natural antibacterial agents to glass ionomer cement (GICs). Hence, the aim of the study was to increase the antimicrobial properties of GICs through its modification with mixture of plant extracts to be evaluated along with an 0.5% chlorohexidine-modified GIC (CHX-GIC) with regard to biological and compressive strength properties. Conventional GIC (freeze-dried version) and CHX were used. Alcoholic extract of Salvadora persica, Olea europaea, and Ficus carcia leaves were prepared using a Soxhlet extractor for 12 h. The plant extract mixture (PE) was added in three different proportions to the water used for preparation of the dental cement (Group 1:1 PE, 2:1 PE, and 1:2 PE). Specimens were then prepared and tested against the unmodified GIC (control) and the 0.5% CHX-GIC. Chemical analysis of the extract mixture was performed using Gas chromatography–mass spectrometry. Antimicrobial activity was evaluated using agar diffusion assay against Micrococcus luteus and Streptoccocus mutans. Compressive strength was evaluated according to ISO 9917-1:2007 using a Zwick testing machine at a crosshead speed of 0.5 mm/min. Antimicrobial activity against Streptoccocus mutans was significantly increased for all the extract-modified materials compared to the unmodified cement, and the highest concentration was comparable to the CHX-GIC mixture. The activity against Micrococcus luteus was also significantly increased, but only for the material with the highest extract concentration, and here the CHX-GIC group showed statistically the highest antimicrobial activity. Compressive strength results revealed that there was no statistically significant difference between the different mixtures and the control except for the highest tested concentration that showed the highest mean values. The plant extracts (PEs) enhanced the antimicrobial activity against S. mutans and also against M. luteus in the higher concentration while compressive strength was improved by addition of the PE at higher concentrations.

scholarly journals Compressive and diametral tensile strength of glass ionomer cements

2004 ◽  
Vol 12 (4) ◽  
pp. 344-348 ◽  
Author(s):  
Eduardo Bresciani ◽  
Terezinha de Jesus Esteves Barata ◽  
Ticiane Cestari Fagundes ◽  
Akimi Adachi ◽  
Marina Martins Terrin ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Testing Machine ◽  
Glass Ionomer Cement ◽  
Mean Value ◽  
Atraumatic Restorative Treatment ◽  
Glass Ionomer ◽  
Restorative Treatment ◽  
Significant Difference ◽  
The Mean ◽  
Diametral Tensile Strength

The aim of this study was to compare, in different periods of time, the compressive and diametral tensile strength of a traditional high viscous glass ionomer cement: Fuji IX (GC Corporation), with two new Brazilian GIC's: Vitro-Molar (DFL) and Bioglass R (Biodinamica), all indicated for the Atraumatic Restorative Treatment (ART) technique. Fifteen disk specimens (6.0mm diameter x 3.0mm height) for the diametral tensile strength (DTS) test and fifteen cylindrical specimens (6.0mm diameter x 12.0mm height) for the compressive strength (CS) test were made of each GIC. Specimens were stored in deionized water at 37º C and 100% of humidity in a stove until testing. Five specimens of each GIC were submitted to CS and DTS test in each period, namely 1 hour, 24 hours and 7 days. The specimens were tested in a testing machine (Emic) at a crosshead speed of 1.0mm/min for CS and 0.5mm/min for the DTS test until failure occurred. The data were submitted to two-way ANOVA and Tukey tests (alpha=0.05). The mean CS values ranged from 42.03 to 155.47MPa and means DTS from 5.54 to 13.72 MPa, with test periods from 1h to 7 days. The CS and DTS tests showed no statistically significant difference between Fuji IX and Vitro Molar, except for CS test at 1-hour period. Bioglass R had lowest mean value for CS of the cements tested. In DTS test Bioglass R presented no statistically significant differences when compared with all others tested GICs at 1-hour period and Bioglass R presented no difference at 24-hour and 7-day periods when compared to Vitro-Molar. Further studies to investigate other physical properties such as fracture toughness and wear resistance, as well as chemical composition and biocompatibility, are now needed to better understand the properties of these new Brazilian GIC's.

scholarly journals A COMPARATIVE EVALUATION OF MICROLEAKAGE, COMPRESSIVE STRENGTH, FLEXURAL STRENGTH AND FLUORIDE RELEASE OF ZIRCONOMER AND KETAC SILVER: AN IN VITRO STUDY.

2020 ◽  
Vol 9 (4) ◽  
Author(s):  
CHARANTEJA VEMAGIRI ◽  
Uloopi KS ◽  
Vinay Chandrappa ◽  
Anusha Ch
Keyword(s):  
Compressive Strength ◽  
Flexural Strength ◽  
Testing Machine ◽  
In Vitro Study ◽  
Biological Properties ◽  
T Test ◽  
Fluoride Release ◽  
Restorative Material ◽  
Glass Ionomer

Background: A successful restorative material forms a better adhesion, resist the microleakage and releases fluoride. However, existing glass ionomer cements cannot be used as a posterior restorative material in stress bearing areas. A new ionomer called Zirconomer, zirconia reinforced glass ionomer claims to exhibit high physical and biological properties. Aim: To assess and compare the microleakage, compressive strength, flexural strength and fluoride release from zirconomer with ketac silver. Materials & Methods: On twenty caries free premolar teeth (10 per each group), a class v cavity was restored with zirconomer and ketac silver. The microleakage was assessed using dye penetration test and stereomicroscope. The compressive and flexural strengths of these materials were measured using Instron Universal testing machine. The amount of fluoride released from the modified ionomers at pH 5 and pH 7 was estimated using Orion fluoride specific electrode. The obtained data was then subjected to statistical analysis. Results: Data was analysed using paired t-test for intergroup comparisons and unpaired t-test for intragroup comparisons. The overall microleakage (0.5±0.48) of zirconomer was significantly less (p=0.000) compared to ketac silver (1.9±0.83). Zirconomer demonstrated a significant higher compressive strength (330.25±60.14), flexural strength (33.058±2.36) than ketac silver (p= 0.000). Zirconomer demonstrated high fluoride release from day 1 to day 7 at both pH 5 and pH 7. Conclusion: Zirconomer demonstrated better physical and biological properties compared with ketac silver.

scholarly journals Effects of Powdery Cellulose Nanofiber Addition on the Properties of Glass Ionomer Cement

Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3077 ◽  
Author(s):  
Takako Nishimura ◽  
Yukari Shinonaga ◽  
Chikoto Nagaishi ◽  
Rie Imataki ◽  
Michiko Takemura ◽  
...  
Keyword(s):  
Flexural Strength ◽  
Cellulose Nanofibers ◽  
Glass Ionomer Cement ◽  
Chemical Properties ◽  
Fluoride Ion ◽  
Strength Testing ◽  
Glass Ionomer ◽  
Ion Release ◽  
Diametral Tensile Strength ◽  
Ionomer Cement

In this study, we aimed to evaluate the effect of the addition of powdery cellulose nanofibers (CNFs) on the mechanical properties of glass ionomer cement (GIC) without negatively affecting its chemical properties. Commercial GIC was reinforced with powdery CNFs (2–8 wt.%) and characterized in terms of flexural strength, compressive strength, diametral tensile strength, and fluoride-ion release properties. Powdery CNFs and samples subjected to flexural strength testing were observed via scanning electron microscopy. CNF incorporation was found to significantly improve the flexural, compressive, and diametral tensile strengths of GIC, and the corresponding composite was shown to contain fibrillar aggregates of nanofibers interspersed in the GIC matrix. No significant differences in fluoride-ion release properties were observed between the control GIC and the CNF-GIC composite. Thus, powdery CNFs were concluded to be a promising GIC reinforcement agent.

scholarly journals The Effect of Altered pH on Push-Out Bond Strength of Biodentin, Glass Ionomer Cement, Mineral Trioxide Aggregate and Theracal

2015 ◽  
Vol 62 (1) ◽  
pp. 7-13 ◽  
Author(s):  
Sameer Makkar ◽  
Ruchi Vashisht ◽  
Anita Kalsi ◽  
Pranav Gupta
Keyword(s):  
Bond Strength ◽  
Alkaline Medium ◽  
Gold Foil ◽  
Testing Machine ◽  
Glass Ionomer Cement ◽  
Mineral Trioxide Aggregate ◽  
Glass Ionomer ◽  
Human Teeth ◽  
Push Out ◽  
Ionomer Cement

Summary Introduction Throughout the history of dentistry, a wide variety of materials such as gold-foil, silver posts, amalgam, zinc oxide eugenol, glass ionomer cements, mineral trioxide aggregate have been used as retrograde fillings. Altered pH in periapical lesions can affect push-out bond strength of these materials. The aim of this study was to evaluate the effect of altered pH on push-out bond strength of Biodentin, Glass ionomer cement (GIC), Mineral trioxide aggregate (MTA) and Theracal. Material and Methods Forty-eight dentin slices of extracted single-rooted human teeth were sectioned and their canal portion instrumented to achieve a diameter of 1.4 mm. The specimens were then assigned into the four groups (one group for each material) with 12 samples in each group. All groups were further divided into 3 subgroups (with 4 specimens in each subgroup): acidic (butyric acid buffered at pH 6.4), neutral (phosphate buffer saline solution at pH 7.4) and alkaline (buffered potassium hydroxide at pH 8.4). Samples were incubated for 4 days at 37°C in acidic, neutral or alkaline medium. Push-out bond strength was measured using a Universal Testing Machine. The slices were examined under a stereomicroscope to determine the nature of bond failure. Results GIC showed the highest bond strength (33.33MPa) in neutral and acidic medium (26.75MPa) compared to other materials. Biodentin showed the best result in alkaline medium. Conclusion Altered pH level affected push-out bond strength of root end materials. GIC demonstrated good push-out bond strength that increased with decrease of pH whereas newer materials Biodentin and Theracal showed satisfying results in altered pH.

scholarly journals A Comparative Evaluation of Flexural Strength of Commercially Available Acrylic and Modified Polymethylmethacrylate: An in vitro Study

2013 ◽  
Vol 14 (1) ◽  
pp. 80-83 ◽  
Author(s):  
Naveen S Yadav ◽  
Teerthesh Jain ◽  
Amrita Pandita ◽  
SMA Feroz ◽  
UK Kartika ◽  
...  
Keyword(s):  
Flexural Strength ◽  
Methacrylic Acid ◽  
Comparative Evaluation ◽  
Testing Machine ◽  
Acrylic Resin ◽  
Bending Test ◽  
Control Group ◽  
Diabetic Patients ◽  
Denture Stomatitis

ABSTRACT Aim The purpose of this study was to evaluate and compare the flexural strength of commercially available acrylic (trevalone) and modified polymethylmethacrylate (PMMA). Materials and methods Four groups were tested; Group 1— control group regular MMA, group 2—2% methacrylic acid, 88% MMA, group 3—16% methacrylic acid, 84% MMA group 4— 20% methacrylic acid, 80% MMA 15 resin specimens of each group were polymerized. After processing, the specimens were subjected for flexural strength testing using three point bending test in a Universal Testing Machine. All data was statistically analyzed with one-way ANOVA, differences within the groups were analyzed by Scheffe's analysis. Results As the ratio of incorporated methacrylic acid to PMMA increased, the flexural strength decreased. Analysis of data revealed a significant decrease in flexural strength of specimens (p < 0.000) after incorporation of 12%, 16%, 20% methacrylic acid to heat polymerized acrylic resin, when compared with the control group. Lowest flexural strength was observed with specimens containing 20% methacrylic acid and highest flexural strength was observed with specimens containing conventional monomer without methacrylic acid. Conclusion It was observed that as the concentration of methacrylic acid in heat polymerized acrylic resin increases, the flexural strength decreases. Lowest flexural strength was observed with specimens containing 20% methacrylic acid and highest flexural strength was observed with specimens containing conventional monomer without methacrylic acid. Clinical significance The major advantages of addition of methacrylic acid to polymethylmethacrylate could be for the elderly people with restricted manual dexterity or cognitive disturbances, especially for patients who do not follow an adequate denture cleansing protocol and diabetic patients who are more susceptible for denture stomatitis. How to cite this article Jain T, Yadav NS, Pandita A, Feroz SMA, Kartika UK, Singh PP. A Comparative Evaluation of Flexural Strength of Commercially Available Acrylic and Modified Polymethylmethacrylate: An in vitro Study. J Contemp Dent Pract 2013;14(1):80-83.

scholarly journals Compressive strength of glass ionomer cements using different specimen dimensions

2007 ◽  
Vol 21 (3) ◽  
pp. 204-208 ◽  
Author(s):  
André Mallmann ◽  
Jane Clei Oliveira Ataíde ◽  
Rosa Amoedo ◽  
Paulo Vicente Rocha ◽  
Letícia Borges Jacques
Keyword(s):  
Compressive Strength ◽  
Testing Machine ◽  
Glass Ionomer Cement ◽  
Strength Test ◽  
Glass Ionomer Cements ◽  
Glass Ionomer ◽  
Universal Testing ◽  
Resin Modified Glass Ionomer ◽  
Compressive Strength Test ◽  
Ionomer Cement

The purpose of this study was to evaluate the compressive strength of two glass ionomer cements, a conventional one (Vitro Fil® - DFL) and a resin-modified material (Vitro Fil LC® - DFL), using two test specimen dimensions: One with 6 mm in height and 4 mm in diameter and the other with 12 mm in height and 6 mm in diameter, according to the ISO 7489:1986 specification and the ANSI/ADA Specification No. 66 for Dental Glass Ionomer Cement, respectively. Ten specimens were fabricated with each material and for each size, in a total of 40 specimens. They were stored in distilled water for 24 hours and then subjected to a compressive strength test in a universal testing machine (EMIC), at a crosshead speed of 0.5 mm/min. The data were statistically analyzed using the Kruskal-Wallis test (5%). Mean compressive strength values (MPa) were: 54.00 ± 6.6 and 105.10 ± 17.3 for the 12 mm x 6 mm sample using Vitro Fil and Vitro Fil LC, respectively, and 46.00 ± 3.8 and 91.10 ± 8.2 for the 6 mm x 4 mm sample using Vitro Fil and Vitro Fil LC, respectively. The resin-modified glass ionomer cement obtained the best results, irrespective of specimen dimensions. For both glass ionomer materials, the 12 mm x 6 mm matrix led to higher compressive strength results than the 6 mm x 4 mm matrix. A higher variability in results was observed when the glass ionomer cements were used in the larger matrices.

scholarly journals Effect of Luting Cements On the Bond Strength to Turkom-Cera All-Ceramic Material

2018 ◽  
Vol 6 (3) ◽  
pp. 548-553 ◽  
Author(s):  
Bandar M. A. Al–Makramani ◽  
Abdul A. A. Razak ◽  
Mohamed I. Abu–Hassan ◽  
Fuad A. Al–Sanabani ◽  
Fahad M. Albakri
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Glass Ionomer Cement ◽  
Resin Cement ◽  
Glass Ionomer ◽  
Luting Cement ◽  
Significant Difference ◽  
All Ceramic ◽  
Ionomer Cement

BACKGROUND: The selection of the appropriate luting cement is a key factor for achieving a strong bond between prepared teeth and dental restorations.AIM: To evaluate the shear bond strength of Zinc phosphate cement Elite, glass ionomer cement Fuji I, resin-modified glass ionomer cement Fuji Plus and resin luting cement Panavia-F to Turkom-Cera all-ceramic material.MATERIALS AND METHODS: Turkom-Cera was used to form discs 10mm in diameter and 3 mm in thickness (n = 40). The ceramic discs were wet ground, air - particle abraded with 50 - μm aluminium oxide particles and randomly divided into four groups (n = 10). The luting cement was bonded to Turkom-Cera discs as per manufacturer instructions. The shear bond strengths were determined using the universal testing machine at a crosshead speed of 0.5 mm/min. The data were analysed using the tests One Way ANOVA, the nonparametric Kruskal - Wallis test and Mann - Whitney Post hoc test.RESULTS: The shear bond strength of the Elite, Fuji I, Fuji Plus and Panavia F groups were: 0.92 ± 0.42, 2.04 ± 0.78, 4.37 ± 1.18, and 16.42 ± 3.38 MPa, respectively. There was the statistically significant difference between the four luting cement tested (p < 0.05).CONCLUSION: the phosphate-containing resin cement Panavia-F exhibited shear bond strength value significantly higher than all materials tested.

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