scholarly journals Effect of Reverse-phase Transformation Annealing Process on Microstructure and Mechanical Properties of Medium Manganese Steel

Materials ◽  
2018 ◽  
Vol 11 (9) ◽  
pp. 1633 ◽  
Author(s):  
Yan Zhao ◽  
Lifeng Fan ◽  
Bin Lu

In order to develop a third-generation automobile steel with powerful strength and elongation, we propose a method through high temperature quenching and two-phase region reverse-phase transformation annealing to develop such steel with 0.13% C and 5.4% Mn. To investigate the microstructure evolution and mechanical properties of manganese steel, SEM, XRD and TEM are employed in our experiments. Experimental results indicate that the microstructure after quenching is mainly lath martensite microstructure with average of lath width at 0.5 μm. The components of the steel after along with reverse-phase transformation annealing are ultra-fine grain ferrite, lath martensite and different forms of austenite microstructure. When the temperature at 625 °C, the components of the steel mainly includes lath martensite microstructure and ultra-fine grain ferrite and the fraction of austenite volume is only 5.09%. When the annealing temperature of reverse-phase transformation increase into 650 °C and 675 °C, the austenite appears in the boundary of the ferritic grain boundary and the boundary of lath martensite as the forms of bulk and lath. The phenomenon appears in the bulk of austenite, and the size of is 0.22 μm, 0.3 μm. The fraction of austenite volume is 22.34% at 675 °C and decreases into 9.32% at 700 °C. The components of austenite mainly includes ultra-fine grained ferrite and lath martensite. Furthermore, the density of decreases significantly, and the width of martensite increases into 0.32 μm. In such experimental settings, quenching at 930 °C with 20 min and at 675 °C with 30 min reverse-phase transformation annealing, the austenite volume fraction raises up to 22.34%.

1996 ◽  
Vol 118 (4) ◽  
pp. 463-470 ◽  
Author(s):  
Yhu-Jen Hwu ◽  
J. G. Lenard ◽  
J. J. M. Too

Continuous cooling curves of an extra-low carbon steel under three cooling rates are measured. The flow stress of the steel is established in compression tests during which the temperature is continuously decreasing. The phase transformation temperatures are determined from the cooling rate curve. The latent heat during phase transformation is calculated. A new variable, related to the volume fraction of transformation, is defined. Experimental results show that the relationship between the softening ratio of the flow stress due to phase transformation and this new variable may be described by a quadratic relationship. Based on this relationship and the continuous cooling curves, the flow stresses in the two-phase region are successfully predicted.


2012 ◽  
Vol 510-511 ◽  
pp. 420-428
Author(s):  
A. Ahmad ◽  
A. Ali ◽  
G.H. Awan ◽  
K.M. Ghauri ◽  
R. Aslam

The paper presents the role of equiaxed α׳ in the bimodal microstructure to attain an optimal combination of ductility and strength. The study revealed that the production of bimodal microstructure and volume fraction of equiaxed α׳ were reliant on the forging temperature and subsequent heat treatment. The Ti-6Al-4V alloy was forged in the two phase region and different heat treatment cycles were employed to get the desired bimodal microstructure and thus the combination of strength and ductility. The mechanical properties of fully lamellar microstructure were compared with bimodal microstructure containing equiaxed α׳. The experimental results showed that the amount of equiaxed α׳ in the bimodal microstructure was critical for achieving a well-balanced profile of mechanical properties.


2018 ◽  
Vol 941 ◽  
pp. 346-351
Author(s):  
Fei Fei Hou ◽  
Atsushi Ito ◽  
Yu Bai ◽  
Akinobu Shibata ◽  
Nobuhiro Tsuji

Medium manganese steels are nowadays energetically investigated as the third generation advanced high strength steels (AHSS) because of their excellent balance between material cost and mechanical properties. However, the phase transformation and microstructure evolution in medium manganese steels during various heat treatments and thermomechanical processing are still unclear. The present study firstly examined kinetics of static phase transformation behavior and microstructural change in a 3Mn-0.1C medium manganese steel. Hot compression tests were also carried out to investigate the influences of high-temperature thermomechanical processing on the microstructure evolution. It was found that ferrite transformation was quite slow in static conditions but greatly accelerated by hot compression in (austenite and ferrite) two phase region. Dual phase microstructures composed of martensite and ferrite with ferrite grain sizes of 1~2 μm were obtained, which exhibited superior mechanical properties.


2020 ◽  
Vol 34 (25) ◽  
pp. 2050269
Author(s):  
Yuqi Mao ◽  
Yuehong Zheng ◽  
Yu Shi ◽  
Min Zhu ◽  
Saitejin ◽  
...  

In order to further expand the application scope of 2205 duplex stainless steel (DSS), its microstructure and mechanical properties require as much attention as its corrosion properties. In this study, 2205DSSs were prepared by aluminothermic reaction and the microstructures and mechanical behavior of the rolled alloys were analyzed. The micro-nanocrystals composite structure appears in the alloys after rough rolling with deformation of 40% at [Formula: see text]C followed by finishing rolling with deformation of 30%, 50% and 70% at [Formula: see text]C. With the increase of rolling deformation, the two-phase structure is gradually elongated, the average size of the two-phase grains is gradually increased, and some [Formula: see text] phase will change to [Formula: see text] phase, the volume fraction of [Formula: see text] phase is gradually increased, and the distribution of nanocrystals is gradually uniform. Meanwhile, the fracture mode of alloy is gradually changed from ductile fracture to brittle fracture. The strength and hardness of the alloy increase gradually.


Crystals ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 435
Author(s):  
Xiangpeng Xiao ◽  
Jian Huang ◽  
Jinshui Chen ◽  
Hai Xu ◽  
Zhao Li ◽  
...  

Cu-Ni-Si alloy with a different Co content was prepared by inductive melting and hot rolling. The alloy was solution treated at 950 °C for 1.5 h and aged at 450 °C, 500 °C, and 550 °C for different times. The phase diagram calculation and transmission electron microscopy was used to investigate the effect of Co addition on the aging precipitation behavior of the Cu-Ni-Si alloy. The phase transformation kinetics equation was calculated as well. The results show that, with the increase of aging temperature, the two-phase region of Fcc + Ni2Si in the Cu-Ni-Si ternary diagram would get wider. Some NixSiy phases would also form in the Cu-rich isothermal section. The addition of Co would replace part of Ni to form the (Ni, Co)2Si phase, which inhibits the spinodal decomposition process of the Cu-Ni-Si alloy during the aging process. The precipitated phase of the Cu-Ni-Si alloy with a high content of the Co element is more likely to grow with the extension of aging time. The phase transformation kinetic equations of the Cu-Ni-Si alloy at 450 °C and 500 °C showed good agreement with the experimental results. Furthermore, it can be seen from the precipitation kinetic curve the addition of the Co element accelerates precipitation in the aging process.


2000 ◽  
Vol 2000.3 (0) ◽  
pp. 473-474 ◽  
Author(s):  
Norikazu MATSUKURA ◽  
Masahiro NOMURA ◽  
Kouichi MAKII ◽  
Shigenobu NANBA

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