Microstructure Evolution and Mechanical Properties of Bimodal Grains Induced by Reverse Phase Transformation of 301 Stainless Steel Stripe

2021 ◽  
Author(s):  
Yu Wang ◽  
Yuxiong Hu ◽  
Feng Mao ◽  
Jun li ◽  
Jie zhou ◽  
...  
Materials ◽  
2018 ◽  
Vol 11 (9) ◽  
pp. 1633 ◽  
Author(s):  
Yan Zhao ◽  
Lifeng Fan ◽  
Bin Lu

In order to develop a third-generation automobile steel with powerful strength and elongation, we propose a method through high temperature quenching and two-phase region reverse-phase transformation annealing to develop such steel with 0.13% C and 5.4% Mn. To investigate the microstructure evolution and mechanical properties of manganese steel, SEM, XRD and TEM are employed in our experiments. Experimental results indicate that the microstructure after quenching is mainly lath martensite microstructure with average of lath width at 0.5 μm. The components of the steel after along with reverse-phase transformation annealing are ultra-fine grain ferrite, lath martensite and different forms of austenite microstructure. When the temperature at 625 °C, the components of the steel mainly includes lath martensite microstructure and ultra-fine grain ferrite and the fraction of austenite volume is only 5.09%. When the annealing temperature of reverse-phase transformation increase into 650 °C and 675 °C, the austenite appears in the boundary of the ferritic grain boundary and the boundary of lath martensite as the forms of bulk and lath. The phenomenon appears in the bulk of austenite, and the size of is 0.22 μm, 0.3 μm. The fraction of austenite volume is 22.34% at 675 °C and decreases into 9.32% at 700 °C. The components of austenite mainly includes ultra-fine grained ferrite and lath martensite. Furthermore, the density of decreases significantly, and the width of martensite increases into 0.32 μm. In such experimental settings, quenching at 930 °C with 20 min and at 675 °C with 30 min reverse-phase transformation annealing, the austenite volume fraction raises up to 22.34%.


Metals ◽  
2019 ◽  
Vol 9 (7) ◽  
pp. 790 ◽  
Author(s):  
Fuwen Chen ◽  
Guanglong Xu ◽  
Kechao Zhou ◽  
Hui Chang

Bimodal microstructures where globular α and acicular α phases are embedded in the β matrix are commonly used in industry-relevant Ti-55531. To optimize the performance of Ti-55531 through heat treatment, it is crucial to understand and control the phase transformation in the as-received bimodal Ti-55531 as well as its microstructure evolution. In this work, the isochronal phase transformations and microstructure evolution in the bimodal Ti-55531 during the continuous heating were systematically studied by combining dilatometry, XRD phase analyses, and SEM observation. The β → α transformation occurred at 678 K only with the acicular α. When the temperature was higher than 788 K, α → β transformation took place in two separate stages (i.e., αacicular → β and αglobular → β transformation). The dissolution of αglobular occurred after the dissolution of αacicular was completed. Due to the difference in the chemical composition and interface curvature between αacicular and αglobular, the average activation energy for αacicular → β transformation was lower than that for the αglobular → β transformation. The isochronal phase transformation and microstructure evolution during continuous heating in the present work could be used to optimize heat treatment procedures for desired mechanical properties.


Materials ◽  
2018 ◽  
Vol 11 (9) ◽  
pp. 1557 ◽  
Author(s):  
Yi Xiong ◽  
Yun Yue ◽  
Tiantian He ◽  
Yan Lu ◽  
Fengzhang Ren ◽  
...  

The impacts of rolling temperature on phase transformations and mechanical properties were investigated for AISI 316LN austenitic stainless steel subjected to rolling at cryogenic and room temperatures. The microstructure evolution and the mechanical properties were investigated by means of optical, scanning, and transmission electron microscopy, an X-ray diffractometer, microhardness tester, and tensile testing system. Results showed that strain-induced martensitic transformation occurred at both deformation temperatures, and the martensite volume fraction increased with the deformation. Compared with room temperature rolling, cryorolling substantially enhanced the martensite transformation rate. At 50% deformation, it yielded the same fraction as the room temperature counterpart at 90% strain, while at 70%, it totally transformed the austenite to martensite. The strength and hardness of the stainless steel increased remarkably with the deformation, but the corresponding elongation decreased dramatically. Meanwhile, the tensile fracture morphology changed from a typical ductile rupture to a mixture of ductile and quasi-cleavage fracture. The phase transformation and deformation mechanisms differed at two temperatures, with the martensite deformation contributing to the former, and austenite deformation to the latter. Orientations between the transformed martensite and its parent phase followed the K–S (Kurdjumov–Sachs) relationship.


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