scholarly journals An Efficient Thermal Cure Profile for Thick Parts Made by Reactive Processing of Acrylic Thermoplastic Composites

2021 ◽  
Vol 5 (9) ◽  
pp. 229
Author(s):  
Barbara Palmieri ◽  
Angelo Petriccione ◽  
Giuseppe De Tommaso ◽  
Michele Giordano ◽  
Alfonso Martone
Keyword(s):  
Residual Stresses ◽  
Thermal Gradient ◽  
Temperature Fields ◽  
Thermoplastic Composites ◽  
Reactive Processing ◽  
Thermal Cure ◽  
Scanning Calorimetry ◽  
Thermal Exchange ◽  
Set Up ◽  
Semi Empirical

The process of curing of large thick composite parts needs attention regarding the formation of residual stresses. Similarly, novel reactive thermoplastics need investigating to produce an efficient thermal cure profile that decreases the risk of warpage and residual stress. In this work, the polymerization kinetics of the Elium resin system is investigated by differential scanning calorimetry (DSC) tests, the analysis of thermo-grams, and the parameters of Kamal and Sourour’s semi-empirical model. A numerical model based on finite elements was set up to reproduce the temperature fields during part consolidation. Several processing conditions were investigated (dwell temperature, environment, heat exchange) in order to predict the thermal gradient within the part. The optimal cure profile was identified as a function of process parameters with the aim of minimizing the thermal gradient within the composite element. The analysis revealed that, for the reactive thermoplastic Elium, the consolidation in facilities with high thermal exchange may increase the risk of residual stresses within the parts, erasing the advantage of short cure cycles.

Finite Element Simulation of Laser Beam Welding Induced Residual Stresses and Distortions in a T-Joint Configuration for Aeronautic Structures

2009 ◽  
Author(s):  
Muhammad Zain-ul-abdein ◽  
Daniel Ne´lias ◽  
Jean-Franc¸ois Jullien ◽  
Dominique Deloison
Keyword(s):  
Finite Element ◽  
Residual Stresses ◽  
Laser Beam ◽  
Boundary Conditions ◽  
Laser Beam Welding ◽  
Temperature Fields ◽  
Heat Transfer Analysis ◽  
Small Scale ◽  
Joint Configuration ◽  
Simulation Results

Laser beam welding has found its application in the aircraft industry for the fabrication of fuselage panels in a T-joint configuration. However, the inconveniences like distortions and residual stresses are inevitable consequences of welding. The effort is made in this work to experimentally measure and numerically simulate the distortions induced by laser beam welding of a T-joint with industrially used thermal and mechanical boundary conditions on the thin sheets of aluminium 6056-T4. Several small scale experiments were carried out with various instrumentations to establish a database necessary to verify the simulation results. Finite element (FE) simulation is performed with Abaqus and the conical heat source is programmed in FORTRAN. Heat transfer analysis is performed to achieve the required weld pool geometry and temperature fields. Mechanical analysis is then performed with industrial loading and boundary conditions so as to predict the distortion and the residual stress pattern. A good agreement is found amongst the experimental and simulation results.

External work in level and grade walking on a motor-driven treadmill

1960 ◽  
Vol 15 (5) ◽  
pp. 759-763 ◽  
Author(s):  
J. W. Snellen
Keyword(s):  
Heat Loss ◽  
Heat Production ◽  
Total Energy Expenditure ◽  
The Body ◽  
External Work ◽  
Thermal Exchange ◽  
Level Walking ◽  
The Subject ◽  
Set Up ◽  
Physical Laws

When studying a walking subject's thermal exchange with the environment, it is essential to know whether in level walking any part of the total energy expenditure is converted into external mechanical work and whether in grade walking the amount of the external work is predictable from physical laws. For this purpose an experiment was set up in which a subject walked on a motor-driven treadmill in a climatic room. In each series of measurements a subject walked uphill for 3 hours and on the level for another hour. Metabolism was kept equal in both situations. Air and wall temperatures were adjusted to the observed weighted skin temperature in order to avoid any heat exchange by radiation and convection. Heat loss by evaporation was derived from the weight loss of the subject. All measurements were carried out in a state of thermal equilibrium. In grade walking there was a difference between heat production and heat loss by evaporation. This difference equaled the caloric equivalent of the product of body weight and gained height. In level walking the heat production equaled heat loss. Hence it was concluded that in level walking all the energy is converted into heat inside the body. Submitted on April 26, 1960

Evaluation by FEM of the Influence of the Preheating and Post-Heating Treatments on Residual Stresses in Welding

2014 ◽  
Vol 627 ◽  
pp. 93-96 ◽  
Author(s):  
Raffaele Sepe ◽  
Enrico Armentani ◽  
Giuseppe Lamanna ◽  
Francesco Caputo
Keyword(s):  
Temperature Distribution ◽  
Residual Stresses ◽  
Gas Metal Arc Welding ◽  
Welding Process ◽  
Element Model ◽  
Butt Joint ◽  
Temperature Fields ◽  
Heating Process ◽  
Butt Weld ◽  
Metal Arc Welding

During the last few years various experimental destructive and non-destructive methods were developed to evaluate residual stresses. However it is impossible to obtain a full residual stress distribution in welded structures by means of experimental methods. This disadvantage can be solved by means of computational analysis which allows to determine the whole stress and strain fields in complex structures. In this paper the temperature distribution and residual stresses were determined in a single-pass butt joint welded by GMAW (Gas Metal Arc Welding) process by finite element model (FEM). A 3D finite parametric element model has been carried out to analyze temperature distribution in butt weld joints and thermo-mechanical analyses were performed to evaluate resulting residual stresses. Temperature fields have been investigated by varying an initial preheating treatment. Moreover the technique of “element birth and death” was adopted to simulate the process of filler metal addition The high stresses were evaluated, with particular regard to fusion zone and heat affected zone. The influence of preheating and post-heating treatment on residual stresses was investigated. The residual stresses decrease when preheating temperature increases. The maximum value of longitudinal residual stresses without pre-heating can be reduced about 12% and 38% by using the preheating and post-heating process respectively.

scholarly journals Preparation of Maleic Anhydride Grafted Poly(trimethylene terephthalate) (PTT-g-MA) by Reactive Extrusion Processing

2019 ◽  
Vol 3 (2) ◽  
pp. 37 ◽  
Author(s):  
Natália F. Braga ◽  
Henrique M. Zaggo ◽  
Thaís L. A. Montanheiro ◽  
Fabio R. Passador
Keyword(s):  
Thermal Properties ◽  
Maleic Anhydride ◽  
Acrylonitrile Butadiene Styrene ◽  
Reactive Extrusion ◽  
Processing Route ◽  
Parallel Plates ◽  
Reactive Processing ◽  
Scanning Calorimetry ◽  
Trimethylene Terephthalate ◽  
Compatibilizing Agent

Maleic anhydride (MA) grafted with poly(trimethylene terephthalate) (PTT)—abbreviated as PTT-g-MA—can be used as a compatibilizing agent to improve the compatibility and dispersion of nanofillers and a dispersed polymer phase into PTT matrix. This work suggests the preparation of PTT-g-MA using a mixture of PTT, MA, and benzoyl peroxide (BPO) by a reactive extrusion process. PTT-g-MA was characterized to confirm the grafting reaction of maleic anhydride on PTT chains by Fourier transform infrared (FTIR) spectroscopy. Thermal properties (differential scanning calorimetry (DSC) and thermogravimetric analysis (TGA)) and rheological analysis (parallel plates rheology) were used to prove the changes that occurred after the graphitization reaction. The reactive processing route allowed the production of the compatibilizing agent (PTT-g-MA) with good thermal properties and with lower viscosity compared to neat PTT, and this could be an alternative for the compatibilization of polymer blends, as example for PTT/ABS (acrylonitrile butadiene styrene) blends and nanocomposites based on PTT matrix.

scholarly journals Optimizing air velocity for the underfloor forced ventilation to protect a refrigerated warehouse from frost heaving

2018 ◽  
Vol 38 (3) ◽  
pp. 321-327
Author(s):  
Jingfu Jia ◽  
Manjin Hao ◽  
Jianhua Zhao
Keyword(s):  
Heat Transfer ◽  
Mathematical Model ◽  
Natural Ventilation ◽  
Ventilation System ◽  
Three Dimensional ◽  
Temperature Fields ◽  
Frost Heave ◽  
Forced Ventilation ◽  
Air Velocity ◽  
Set Up

Forced or natural ventilation is the most common measure of frost heave protection for refrigerated warehouse floor. To optimize air velocity for the underfloor forced ventilation system of refrigerated warehouse, a steady state three-dimensional mathematical model of heat transfer is set up in this paper. The temperature fields of this system are simulated and calculated by CFD software PHOENICS under different air velocity, 1.5m/s, 2.5m/s or 3.5m/s. The results show that the optimized air velocity is 1.5m/s when the tube spacing is 1.5m.

Processing and Characterization of Thermoplastic Polyurethane Nanocomposite Thin Films

2010 ◽  
Vol 133 (1) ◽  
Author(s):  
Anandh Balakrishnan ◽  
Mrinal C. Saha
Keyword(s):  
Thin Film ◽  
Thin Films ◽  
Molecular Weight ◽  
Optical Microscopy ◽  
Carbon Nanofiber ◽  
Droplet Diameter ◽  
Thermoplastic Polyurethane ◽  
Scanning Calorimetry ◽  
Ultrasound Assisted ◽  
Set Up

In this article, we have set up protocols for fabricating thermoplastic polyurethane thin films of about 30 μm (neat polyurethane and carbon nanofiber (CNF) containing polyurethane) via ultrasound assisted atomization at 20 kHz. From processing to thin film peel off, we have set up procedures for fabricating our samples. Using optical microscopy, we have examined the manufacturing of these films from a droplet diameter perspective. Our optical microscopy results indicate that the final film microstructure was directly dependent on the physical properties of the neat/CNF reinforced solution. Mechanical testing of these films was then carefully carried out using a dynamic mechanical analyzer (DMA) unit utilizing a specialized thin film test clamp fixture. These test results were compared with control cast films fabricated from the same solutions. For the similar extensions, we observed a drastic increase in the softness of the atomized film. We surmise that the ultrasound assisted droplet generation concurrent with secondary atomization and evaporation could have resulted in reduction of the molecular weight of the polyurethane in our atomized samples relative to the neat ones. Differential scanning calorimetry (DSC) scans have been conducted to confirm the changes in molecular weight. Although results were inconclusive there is evidence of exotherms at 49C in our atomized samples suggested of changes to molecular weight distribution.

scholarly journals Structural and Thermo-Mechanical Properties of Poly(ε-caprolactone) Modified by Various Peroxide Initiators

Polymers ◽  
2019 ◽  
Vol 11 (7) ◽  
pp. 1101 ◽  
Author(s):  
Przybysz ◽  
Hejna ◽  
Haponiuk ◽  
Formela
Keyword(s):  
Mechanical Properties ◽  
Differential Scanning Calorimetry ◽  
Cross Linking ◽  
Mechanical And Thermal Properties ◽  
Dicumyl Peroxide ◽  
Organic Peroxides ◽  
Reactive Processing ◽  
Scanning Calorimetry ◽  
Melting Temperatures ◽  
Gel Fraction

The modification of poly(ε-caprolactone) (PCL) was successfully conducted during reactive processing in the presence of dicumyl peroxide (DCP) or di-(2-tert-butyl-peroxyisopropyl)-benzene (BIB). The peroxide initiators were applied in the various amounts of 0.5 or 1.0 pbw (part by weight) into the PCL matrix. The effects of the initiator type and its concentration on the structure and mechanical and thermal properties of PCL were investigated. To achieve a detailed and proper explication of this phenomenon, the decomposition and melting temperatures of DCP and BIB initiators were measured by differential scanning calorimetry. The conjecture of the branching or cross-linking of PCL structure via used peroxides was studied by gel fraction content measurement. Modification in the presence of BIB in PCL was found to effectively increase gel fraction. The result showed that the cross-linking of PCL started at a low content of BIB, while PCL modified by high DCP content was only partially cross-linked or branched. PCL branching and cross-linking were found to have a significant impact on the mechanical properties of PCL. However, the effect of used initiators on poly(ε-caprolactone) properties strongly depended on their structure and content. The obtained results indicated that, for the modification towards cross-linking/branching of PCL structure by using organic peroxides, the best mechanical properties were achieved for PCL modified by 0.5 pbw BIB or 1.0 pbw DCP, while the PCL modified by 1.0 pbw BIB possessed poor mechanical properties, as it was related to over cross-linking.

scholarly journals A comparison of mechanical properties and X-ray tomography analysis of different out-of-autoclave manufactured thermoplastic composites

2020 ◽  
Vol 39 (19-20) ◽  
pp. 703-720
Author(s):  
Diego Saenz-Castillo ◽  
María I Martín ◽  
Vanessa García-Martínez ◽  
Abhiram Ramesh ◽  
Mark Battley ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Raw Material ◽  
Thermoplastic Composites ◽  
Scanning Calorimetry ◽  
Consolidation Process ◽  
Plane Shear ◽  
X Ray ◽  
Void Distribution ◽  
Out Of Autoclave

Three different out-of-autoclave manufacturing processes of CF/poly-ether-ether-ketone thermoplastic composites were characterized, including innovative laser-assisted automated fibre placement with in situ consolidation. Characterization techniques included differential scanning calorimetry, ultrasonic non-destructive testing and matrix digestion, in addition to 3D X-ray microcomputed tomography to investigate the void distribution, size and shape. The results revealed that in situ consolidation process can lead to the accumulation of large voids between the upper layers. Interlaminar shear, in-plane shear, tensile and flexure testing were used for mechanical evaluation. A reduction in the mechanical properties was observed for in situ consolidation laminates when compared to the other out-of-autoclave methods. The drop in mechanical properties of in situ consolidation laminates was mainly attributed to the differences found in void distribution and size. Optimization of processing parameters along with higher quality prepreg raw material could be of assistance for the improvement of mechanical properties of in situ consolidation structures.

Thermal Aspects in Resistance Welding of Thermoplastic Composites

2003 ◽  
Author(s):  
Darko Stavrov ◽  
Harald E. N. Bersee
Keyword(s):  
Temperature Distribution ◽  
Power Level ◽  
Resistance Welding ◽  
Thermoplastic Composites ◽  
Transient Temperature ◽  
Temperature Profiles ◽  
Stainless Steel Mesh ◽  
Type K ◽  
Glass Fiber Reinforced ◽  
Set Up

This paper presents a comprehensive experimental study on the thermal aspects in resistance welding of thermoplastic composites. A special test set-up was developed to perform the experiments. Glass fiber reinforced polyetherimide was the material used for manufacturing the welding specimens. Stainless steel mesh was used for production of heating elements. The temperature distribution was monitored using type-K thermocouples connected to a data acquisition system. The main objective of the study was investigating a possible solution for the edge effect. Temperature profiles over the weld length and over the weld width were monitored. The focus was on the transient temperature profiles at the edges of the weld. The temperature distribution through the weld thickness was also monitored. The influence of factors like insulation and power level was investigated. Finally, conclusions are drawn and options for improving the temperature distribution and modification of the models are being discussed.

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