Extensive Assessment of the Physical, Mechanical, and Adhesion Behavior of a Low-viscosity Bulk Fill Composite and a Traditional Resin Composite in Tooth Cavities

2017 ◽  
Vol 42 (5) ◽  
pp. E159-E166 ◽  
Author(s):  
RX Sousa-Lima ◽  
LJA Silva ◽  
LVF Chaves ◽  
S Geraldeli ◽  
RCB Alonso ◽  
...  
Keyword(s):  
Resin Composite ◽  
Testing Machine ◽  
Physical And Mechanical Properties ◽  
Bending Test ◽  
Shrinkage Stress ◽  
Three Point Bending ◽  
Low Viscosity ◽  
Adhesion Behavior ◽  
Bottom To Top ◽  
Push Out

SUMMARY Objectives: To compare the degree of conversion (DC), depth of polymerization (DP), shrinkage stress (SS), flexural strength (FS), elastic modulus (EM), and bond strength (BS) of a low-viscosity bulk fill resin composite and a paste-like traditional composite. Methods: Tetric Evo-Flow Bulk Fill (TBF) and Empress Direct (ED; Ivoclar Vivadent) composites were used. DC (%) and FS/EM (MPa/GPa) were evaluated in bar specimens (7×2×1 mm; n=10) using Fourier-transform infrared spectroscopy and a three-point bending test in a universal testing machine (UTM), respectively. For DP and BS tests, conical cavities (n=10) were prepared in bovine dentin and restored with the composites. DP was analyzed by calculating the bottom-to-top surface microhardness ratio (BTHR), and BS (MPa) was determined by push-out testing in the UTM. SS (MPa) was measured for one increment of TBF and two increments of ED in a UTM attached to an extensometer (n=5). Data were analyzed using Student t-test and analysis of variance (α=0.05). Results: TBF presented higher values than ED for DC (85.7±6.6% vs 54.2±4.9%) and BS (0.95±0.70 MPa vs 0.35±0.15 MPa). TBF values were lower than ED values for FS (76.6±16.8 MPa vs 144.9±24.1 MPa) and maximum SS (0.77±0.07 MPa vs 1.07±0.15 MPa). TBF and ED values were similar for BTHR (0.83±0.16 vs 0.84±0.08) and EM (11.5±2.8 GPa vs 12.5±2.6 GPa). Conclusions: The physical and mechanical properties of TBF, a bulk fill resin composite, were similar or superior to those of ED, a conventional composite, with the exception of FS measurements.

Investigation of Mechanical Properties of Nano Sized Clay/LDH Particle as Hybrid Nano Composite Material

2015 ◽  
Vol 766-767 ◽  
pp. 355-361
Author(s):  
S. Sivasaravanan ◽  
V.K. Bupesh Raja ◽  
S. Prabhu ◽  
S. Dineshkumar ◽  
Gokulaprasad
Keyword(s):  
Composite Material ◽  
Testing Machine ◽  
Weight Ratio ◽  
High Strength ◽  
Sem Analysis ◽  
Bending Test ◽  
Flexural Property ◽  
Weight Percentage ◽  
Three Point Bending ◽  
Sonication Technique

Usage of Hybrid nanocomposite materials provides a greater opportunity to replace the conventional materials due to their properties such as light weight and high strength to based on weight ratio. In this synergitic study, nanosized clay particle and layered double hydroxide particles are used. nanoclay and LDH particles were mixed on the bases of weight percentage (1wt% to 5wt%) by ultra sonication technique. The composite material was fabricated by one of the most common method known as hand lay-up technique. The composite materials was prepared in the form of plate with 4mm of thickness.The characterization of tensile and flexural property of the nanoclay, LDH and combination of both was analysis by tensile test using universal testing machine and three point bending test respectively. The tensile and three point bending test specimens were cut to size as per ASTM standard.The morphology of composite was studied using SEM analysis.

scholarly journals Push-Out Bond Strength of Restorations with Bulk-Fill, Flow, and Conventional Resin Composites

2015 ◽  
Vol 2015 ◽  
pp. 1-5 ◽  
Author(s):  
Rodrigo Vieira Caixeta ◽  
Ricardo Danil Guiraldo ◽  
Edmilson Nobumitu Kaneshima ◽  
Aline Silvestre Barbosa ◽  
Cassiana Pedrotti Picolotto ◽  
...  
Keyword(s):  
Bond Strength ◽  
Light Emitting Diode ◽  
Resin Composite ◽  
Testing Machine ◽  
Adhesive System ◽  
Optical Microscope ◽  
Resin Composites ◽  
Conical Cavity ◽  
Significance Level ◽  
Push Out

The aim of this study was to evaluate the bond strengths of composite restorations made with different filler amounts and resin composites that were photoactivated using a light-emitting diode (LED). Thirty bovine incisors were selected, and a conical cavity was prepared in the facial surface of each tooth. All preparations were etched with Scotchbond Etching Gel, the Adper Scotchbond Multipurpose Plus adhesive system was applied followed by photoactivation, and the cavities were filled with a single increment of Filtek Z350 XT, Filtek Z350 XT Flow, or bulk-fill X-tra fil resin composite (n= 10) followed by photoactivation. A push-out test to determine bond strength was conducted using a universal testing machine. Data (MPa) were submitted to Student’st-test at a 5% significance level. After the test, the fractured specimens were examined using an optical microscope under magnification (10x). Although all three composites demonstrated a high prevalence of adhesive failures, the bond strength values of the different resin composites photoactivated by LED showed that the X-tra fil resin composite had a lower bond strength than the Filtek Z350 XT and Filtek Z350 XT Flow resin composites.

scholarly journals Influence of Modulated Photo-Activation on Shrinkage Stress and Degree of Conversion of Bulk-Fill Composites

2019 ◽  
Vol 30 (6) ◽  
pp. 592-598 ◽  
Author(s):  
Marilia Mattar de Amoêdo Campos Velo ◽  
Linda Wang ◽  
Adilson Yoshio Furuse ◽  
Letícia Ferreira de Freitas Brianezzi ◽  
Cassiana Koch Scotti ◽  
...  
Keyword(s):  
Testing Machine ◽  
Continuous Light ◽  
High Viscosity ◽  
Degree Of Conversion ◽  
Steel Plates ◽  
Attenuated Total Reflectance ◽  
Shrinkage Stress ◽  
Polymerization Shrinkage ◽  
Low Viscosity ◽  
Universal Testing

Abstract This study aimed to evaluate the polymerization properties of bulk-fill materials (low and high-viscosity) by using high-intensity continuous light and intermittent photo-activation in terms of polymerization shrinkage stress and degree of conversion (DC). The following Bulk-fill and Conventional nanofilled resin composites were evaluated: Filtek Z350XT Flow (3M/ESPE), SureFil SDR Flow (Dentsply), Filtek Bulk Fill Flow (3M/ESPE), Filtek Z350XT (3M/ESPE) and Filtek Bulk Fill Posterior (3M/ESPE). A LED device (DB 685, Dabi Atlante) was used for both protocols: continuous uniform and intermittent photo-activation (light-on and light-off cycles) with identical radiant exposure (14 J/cm2). The polymerization shrinkage stress (n=6) was evaluated by inserting a single increment of 12 mm3 between two stainless steel plates (6×2 mm) adapted to a Universal Testing Machine (UTM), at different times. Measurements were recorded after photo-activation. The degree of conversion was evaluated by Fourier transformed infrared spectroscope (FTIR) with an attenuated total reflectance (ATR) accessory (n=5). Data were analyzed by three-way ANOVA and Tukey’s HSD (α=0.05) tests. Bulk Fill Posterior presented higher shrinkage stress values when photo-activated with the intermittent technique (p<0.05). The intermittent photo-activation increased the degree of conversion for the low-viscosity bulk-fills (p<0.05). Therefore, the use of modulated photo-activation (intermittent) must be indicated with caution since its use can influence the shrinkage stress and degree of conversion of composites, which varies according to the resin formulations.

Bonding Interaction and Shrinkage Stress of Low-viscosity Bulk Fill Resin Composites With High-viscosity Bulk Fill or Conventional Resin Composites

2019 ◽  
Vol 44 (6) ◽  
pp. 625-636 ◽  
Author(s):  
ER Cerda-Rizo ◽  
M de Paula Rodrigues ◽  
ABF Vilela ◽  
SSL Braga ◽  
LRS Oliveira ◽  
...  
Keyword(s):  
Failure Mode ◽  
Resin Composite ◽  
High Viscosity ◽  
Shrinkage Stress ◽  
Resin Composites ◽  
Posterior Teeth ◽  
Low Viscosity ◽  
Bonding Interaction ◽  
Significant Difference ◽  
Chi Square Analysis

SUMMARY Objective: To analyze the shrinkage stress, bonding interaction, and failure modes between different low-viscosity bulk fill resin composites and conventional resin composites produced by the same manufacturer or a high-viscosity bulk fill resin composite used to restore the occlusal layer in posterior teeth. Methods & Materials: Three low-viscosity bulk fill resin composites were associated with the conventional resin composites made by the same manufacturers or with a high-viscosity bulk fill resin composite, resulting in six groups (n=10). The bonding interaction between resin composites was tested by assessing the microshear bond strength (μSBS). The samples were thermocycled and were tested with 1-mm/min crosshead speed, and the failure mode was evaluated. The post-gel shrinkage (Shr) of all the resin composites was measured using a strain gauge (n=10). The modulus of elasticity (E) and the hardness (KHN) were measured using the Knoop hardness test. Two-dimensional finite element models were created for analyzing the stress caused by shrinkage and contact loading. The μSBS, Shr, E, and KHN data were analyzed using the Student t-test and one-way analysis of variance. The failure mode data were subjected to chi-square analysis (α=0.05). The stress distribution was analyzed qualitatively. Results: No significant difference was verified for μSBS between low-viscosity bulk fill resin composites and conventional or high-viscosity bulk fill composites in terms of restoring the occlusal layer (p=0.349). Cohesive failure of the low-viscosity bulk fill resin composites was the most frequent failure mode. The Shr, E, and KHN varied between low-viscosity and high-viscosity resin composites. The use of high-viscosity bulk fill resin composites on the occlusal layer reduced the stress at the enamel interface on the occlusal surface. Conclusions: The use of high-viscosity bulk fill resin composites as an occlusal layer for low-viscosity bulk fill resin composites to restore the posterior teeth can be a viable alternative, as it shows a similar bonding interaction to conventional resin composites as well as lower shrinkage stress at the enamel margin.

scholarly journals Effects of Veneering Ceramic and Methods on Failure Load of Veneered Zirconia

2021 ◽  
Vol 11 (5) ◽  
pp. 2129
Author(s):  
Hattanas Kumchai ◽  
Patrapan Juntavee ◽  
Arthur F. Sun ◽  
Dan Nathanson
Keyword(s):  
Glass Ceramic ◽  
Failure Load ◽  
Testing Machine ◽  
Bending Test ◽  
Three Point Bending ◽  
Significant Difference ◽  
Load To Failure ◽  
Cad Cam ◽  
Feldspathic Porcelain ◽  
Post Hoc

Background: A variety of veneering options to zirconia frameworks are now available. The purpose of this study is to evaluate the effect of veneer materials, veneering methods, cement materials, and aging on the failure load of bilayered veneer zirconia. Material and methods: Zirconia bars (20 × 4 × 1 mm) were veneered to 2 mm total thickness (n = 10/group). Veneering method groups included: 1. Hand-layered feldsparthic porcelain (VM = Vita VM9, Vident) and fluorapatite glass–ceramic (CR = IPS e.max Ceram, IvoclarVivadent); 2. Pressed feldspathic porcelain (PM = Vita PM9, Vident) and fluorapatite glass–ceramic (ZP = IPS e.max ZirPress, IvoclarVivadent); 3. CAD-/CAM-milled feldspathic ceramic (TF = Vitablocs Triluxe Forte, Vident) and lithium-disilicate glass–ceramic (CAD = IPS e.max CAD, IvoclarVivadent). CAD/CAM veneers were either cemented with resin cements (P = Panavia21, KurarayDental), (R = RelyX Ultimate, 3M ESPE), (M = Multilink Automix, Ivoclar Vivadent) or fused with fusion glass–ceramic (C = CrystalConnect, IvoclarVivadent). A three-point bending test (15 mm span, zirconia on tension side) was performed on Instron universal testing machine (ISO 6872) recording load-to-failure (LTF) of first veneer cracks or catastrophic failure. For group VM, PM, TF-M, TF-C, CAD-M, CAD-C, ten more bars were prepared and aged with cyclic loading (100,000 cycles, 50% LTF) and thermocycling (2000 cycles) before testing. Data were analyzed by ANOVA, Tukey HSD post hoc tests, and t-test (α = 0.05). Zirconia veneered with IPS e.max CAD by fusing had significantly higher failure load compared with zirconia veneered with other veneering materials. (p ≤ 0.05). For cemented veneers, the cement type had a significant effect on the failure load of the veneer zirconia specimens. Specimens cemented with Panavia 21 had a lower resistance to loading than other cements. The aging experiment revealed a significant difference in failure load between non-aged and aged bars in groups VM and PM, but not in the groups with CAD-/CAM-milled veneers. In conclusion, veneer materials, veneering methods, and cement materials have a significant effect on the failure load of bilayered veneer zirconia. CAD-/CAM-milled veneer zirconia is not susceptible to aging performed in this study.

scholarly journals Effect of Glazing on Flexural Strength of Full-Contour Zirconia

2018 ◽  
Vol 2018 ◽  
pp. 1-5 ◽  
Author(s):  
Hattanas Kumchai ◽  
Patrapan Juntavee ◽  
Arthur F. Sun ◽  
Dan Nathanson
Keyword(s):  
Flexural Strength ◽  
Significant Influence ◽  
Testing Machine ◽  
Surface Treatments ◽  
Bending Test ◽  
Three Point Bending ◽  
Universal Testing ◽  
Heat Treated ◽  
Significant Difference ◽  
Post Hoc

Objective. The purpose of this study was to evaluate the effect of glazing on flexural strength of highly translucent zirconia materials. Materials and Methods. Specimens of three brands of zirconia bars (Prettau Zirconia, Zirkonzahn; inCoris TZI, Sirona; and Zirlux FC, Pentron Ceramics) were prepared and polished according to manufacturers’ instructions. Final specimen dimensions were 20 × 4 × 2 mm. The specimens from each brand were divided into 3 groups (N = 10): control, heat-treated, and glazed. Heat-treated specimens were fired without the application of the glaze material. The glaze material was applied to the glazed specimens before being fired. A three-point bending test (15 mm span) was performed in an Instron universal testing machine (ISO 6872). Data were analyzed by ANOVA and Tukey’s HSD post hoc test (α = 0.05). Results. Two-way ANOVA showed a significant influence of surface treatments on flexural strength of zirconia materials (P≤0.05). There was no significant difference in flexural strength among the different brands of highly translucent zirconia (P≥0.05). Tukey’s HSD post hoc test showed that specimens in the “glazed” group had significantly lower flexural strength than the control and heat-treated groups (P≤0.05). Conclusion. Within the limitations of the study, external glazing decreased the flexural strength of highly translucent zirconia.

scholarly journals Microtensile bond strength of adhesive systems to dentin with or without application of an intermediate flowable resin layer

2008 ◽  
Vol 19 (1) ◽  
pp. 51-56 ◽  
Author(s):  
Mario Fernando De Goes ◽  
Marcelo Giannini ◽  
Vinícius Di Hipólito ◽  
Marcela Rocha de Oliveira Carrilho ◽  
Márcia Daronch ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
Composite Layer ◽  
Adhesive Systems ◽  
Microtensile Bond Strength ◽  
Flowable Composite ◽  
Low Viscosity ◽  
Occlusal Surfaces ◽  
Diamond Saw

This study evaluated the effect of flowable composite resin application on the microtensile bond strength (muTBS) of adhesive systems to dentin. Occlusal surfaces of human third molars were ground to obtain flat dentin surfaces. The crown of each tooth was sectioned occluso-gingivally into four quarters with a water-cooled diamond saw. One of the following adhesive systems was applied to dentin surface in each quarter of the same tooth, following manufacturers' instructions: Scotchbond Multipurpose, Single Bond Adper Prompt and Clearfil SE Bond. Experimental and control groups received the same treatment, except for the fact that a layer of flowable composite (Filtek Flow) was placed and light-cured on top of the adhesive layer in the specimens of the experimental groups. Resin composite (Filtek Z250) crown buildups were then made on the bonded surfaces and incrementally light-cured for 20 s. The restored teeth were stored in water at 37ºC for 24 h. Each tooth quarter was serially cut in a longitudinal direction in order to obtain several bonded sticks (0.9-mm² in cross-section). Maximal microtensile stress (in MPa) at failure was recorded using a universal testing machine. Data were analyzed by two-way ANOVA and Tukey's test at 5% significance level. Placement of a low-viscosity resin to the hybridized dentin increased the muTBS for all tested adhesive systems. However, such increase was significant only for Clearfil SE Bond (p<0.05). When the restorations were placed without low-viscosity resin, Clearfil SE Bond presented higher muTBS than Adper Prompt (p<0.05). For the groups treated with flowable composite, Clearfil SE Bond produced the highest muTBS means to dentin. In conclusion, the effect of the addition of an intermediate flowable composite layer on muTBS to dentin was material-dependent and resulted in an increased adhesion for all tested materials, though with significance only for Clearfil SE Bond.

scholarly journals Comparison of physical and mechanical properties of microwave-polymerized acrylic resin after disinfection in sodium hypochlorite solutions

2009 ◽  
Vol 20 (4) ◽  
pp. 331-335 ◽  
Author(s):  
Helena de Freitas Oliveira Paranhos ◽  
Letícia Resende Davi ◽  
Amanda Peracini ◽  
Rafael Bellini Soares ◽  
Cláudia Helena da Silva Lovato ◽  
...  
Keyword(s):  
Surface Roughness ◽  
Flexural Strength ◽  
Sodium Hypochlorite ◽  
Testing Machine ◽  
Physical And Mechanical Properties ◽  
Color Stability ◽  
Acrylic Resin ◽  
Bending Test ◽  
Water Control ◽  
Before And After

This study evaluated the color stability, surface roughness and flexural strength of a microwave-polymerized acrylic resin after immersion in sodium hypochlorite (NaOCl), simulating 20 min of disinfection daily during 180 days. Forty disk-shaped (15 x 4 mm) and 40 rectangular (65 x 10 x 3 mm) specimens were prepared with a microwave-polymerized acrylic resin (Onda-Cryl). Specimens were immersed in either 0.5% NaOCl, 1% NaOCl, Clorox/Calgon and distilled water (control). Color measurements were determined by a portable colorimeter. Three parallel lines, separated by 1.0 mm, were registered on each specimen before and after immersion procedures to analyze the surface roughness. The flexural strength was measured using a 3-point bending test in a universal testing machine with a 50 kgf load cell and a crosshead speed of 1 mm/min. Data were analyzed statistically by ANOVA and Tukey's test (?=0.05). There was no statistically significant differences (p>0.05) among the solutions for color, surface roughness and flexural strength. It may be concluded that immersion in NaOCl solutions simulating short-term daily use during 180 days did not influence the color stability, surface roughness and flexural strength of a microwave-polymerized acrylic resin.

scholarly journals Evaluation of New Hollow Sleeve Composites for Direct Post-Core Construction

Materials ◽  
2021 ◽  
Vol 14 (23) ◽  
pp. 7397
Author(s):  
Shinji Yoshii ◽  
Sufyan Garoushi ◽  
Chiaki Kitamura ◽  
Pekka K. Vallittu ◽  
Lippo V. Lassila
Keyword(s):  
Mechanical Properties ◽  
Flexural Strength ◽  
Resin Composite ◽  
Flexural Modulus ◽  
Accelerated Aging ◽  
Fracture Analysis ◽  
Bending Test ◽  
Outer Diameter ◽  
Fiber Post ◽  
Three Point Bending

The preset shape and diameter of a prefabricated FRC post rarely follows the anatomy of the root canal. To solve this problem, a new hollow sleeve composite (HSC) system for post-core construction was developed and characterized. A woven fiber was impregnated with two types of resins: Bis-GMA or PMMA, and rolled into cylinders with outer diameter of 2 mm and two different inner diameters, namely 1.2 or 1.5 mm. The commercial i-TFC system was used as a control. Dual-cure resin composite was injected into these sleeves. Additionally, conventional solid fiber post was used as the inner part of the sleeve. The three-point bending test was used to measure the mechanical properties of the specimens and the fracture surface was examined using an electron microscope (SEM). The HSC (1.5 mm, Bis-GMA) revealed a statistically similar flexural modulus but higher flexural strength (437 MPa) compared to i-TFC (239 MPa; ANOVA, p < 0.05). When a fiber post was added inside, all values had a tendency to increase. After hydrothermal accelerated aging, the majority of specimens showed a significant (p < 0.05) decrease in flexural strength and modulus. SEM fracture analysis confirmed that the delamination occurred at the interface between the outer and inner materials. The HSC system provided flexibility but still high mechanical values compared to the commercial system. Thus, this system might offer an alternative practical option for direct post-core construction.

scholarly journals Microhardness Assessment of Two Nanohybrid Composite Resins with Two Curing Technologies

2021 ◽  
Vol 9 (D) ◽  
pp. 81-86
Author(s):  
Ebaa Ibrahim Alagha ◽  
Mustafa Ibrahim Alagha
Keyword(s):  
Composite Resin ◽  
Resin Composite ◽  
Testing Machine ◽  
Degree Of Polymerization ◽  
Composite Resins ◽  
Blue Laser ◽  
Light Sources ◽  
Energy Effect ◽  
The Difference ◽  
Bottom To Top

AIM:This study evaluated the influence of two light sources on the microhardness of two recent composite resins. MATERIALS AND METHODS: A total of 120 specimens were prepared and divided into two groups according to the composite resin restoration used (Tetric EvoCeram Bulk fill) and (Universal Nanohybrid Mosaic). Each group was subdivided into four subgroups according to the curing sources used with different curing duration’s laser curing system (SIROLaser) for 10, 15, and 20 s and conventional blue light system (LED) for 20 s. A microhardness testing machine was used to assess the microhardness of Tetric EvoCeram Bulk fill and Universal Nanohybrid Mosaic. Two-way ANOVA statistical test was used for comparing resin composite and curing energy effect on different variable studied. One-way ANOVA followed by pair-wise Tukey’s post hoc tests was performed to detect significance between each composite subgroups and t-test for subgroups. P ≤ 0.05 is considered statistically significant in all tests. RESULTS: LED cured Tetric EvoCeram Bulk fill composite resin recorded higher bottom to top ratio (B/T ratio) than laser cured one and the difference in B/T ratio between both energies was statistically non-significant. LED cured Mosaic composite resin recorded higher B/T ratio than laser cured one . The difference in bottom to top ratio between both curing devices was statistically significant. CONCLUSION: SIROLaser Blue laser device increases the degree of polymerization and achieves better curing of composite resins than LED. RECOMMENDATION: Different types of curing systems are present in the dental practice. The use of SIROLaser Blue laser to photopolymerize composite resin will offers proper polymerization properties.

Sign in / Sign up

Export Citation Format

Share Document