The Small-Drillhole Minipermeameter Probe for In-Situ Permeability Measurement

2005 ◽  
Vol 8 (06) ◽  
pp. 491-501 ◽  
Author(s):  
Cynthia L. Dinwiddie

Summary Laboratory measurement of permeability using a Hassler cell is the industry standard; however, consistently removing undisturbed rock samples from friableout crops is difficult. Although various conventional surface-sealing mini-permeameters are developed as an alternative for permeability measurement, these devices generally suffer from difficulties in maintaining optimal forces on the tip seal when dealing with outcrop irregularities in the field; outcrop weathering is also problematic. Because a reliable field method is needed for studies of friable geological units, this paper presents an innovative technique for measuring permeability in situ. The design of the small-drill hole minipermeameter probe is discussed, as well as the accompanying analytical technique and the size and shape of the instrument's averaging volume. Small-diameter holes [i.e., 1.8 cm (0.7 in.)] are drilled into an outcrop with a masonry drill, followed by drillhole vacuuming, probe insertion, sealexpansion, gas injection, and calculation of the intrinsic permeability through measurement of the injection pressure, gas-flow rate, and knowledge of the system geometry. Advantages of this approach include access to a nonweathered surface, an operator-independent sealing mechanism around the air-injection zone, and the potential for permeability measurement at multiple depths below an outcrop surface. To date, data have been collected from four diverse porousmedia: upper and lower shoreface sandstone (Escalante, Utah), saprolitic soils(Clemson, South Carolina), nonwelded and sintered ignimbrite (Bishop, California), and fluvially reworked tuffaceous sedimentary rock (Bishop, California). The probe has proved durable and robust, with a single probe sufficient for making thousands of measurements in a variety of environments. Data quality supports the conclusion that the drillhole probe is a practical field instrument. Introduction Small-scale permeability heterogeneity plays a substantial role in petroleum migration and reservoir performance; this parameter commonly ranges over many orders of magnitude (e.g., 0.01 to more than 10,000 md). Permeability heterogeneities on the meter-to-micrometer scale associated with beds, laminae, internal sedimentary structures, and variations in pore morphology are the source of most retrieval difficulties during enhanced-oil-recovery operations, thus negatively affecting reservoir recovery efficiency. Considerable heterogeneity is evident when permeability measurements are made on small scales, either in the field or on field samples in a laboratory setting. Traditionally, small-scale permeability measurements are made by inducing 1D gas flow through a cylindrical core plug in a Hassler sleeve or cell. Recently, such measurements also are made by inducing multidimensional gas flow through a sample with various configurations of the conventional surface-sealing gas minipermeameter. Cylindrical plugs generally are extracted from continuous core at 30-cmintervals for Hassler-cell permeability measurement, preserving a majority of the core while minimizing associated costs. Except for relatively homogeneous formations, this scale of permeability measurement is in an ill-defined geologic region, falling within the range of laminae and lamina sets. Furthermore, core-plug samples tend to be biased toward the more consolidated, less permeable, and less friable core sections. As an example, the effect of this arbitrary sampling density on Hassler-sleeve measurements for the case of tight gas sands is that magnitudes of permeability less than 100 md frequently result, even when coarser-grained beds that would operate as preferential flow channels or "thief zones" are clearly present. Currently, the scale of sedimentary heterogeneity is best resolved by use of the minipermeameter, which allows investigation of permeability heterogeneity at much greater (and statistically significant) sampling densities and on much smaller scales than is possible with the traditional technique. The literature documents use of the conventional surface-sealing minipermeameter probe for measurements made on outcrop surfaces, core plugs, slabbed cores, or large-cut blocks. One motivation for using cores, plugs, or blocks of rock is that natural weathering processes may greatly affect permeability values obtained from exposed outcrop surfaces. The weathering effect has been shown to extend up to several inches below the rock surface. Beyond the issue of weathering, there are other rationales for discouraging use of the conventional surface-sealing minipermeameter probe in a field setting. When applying this probe geometry to natural rock outcroppings in the field, as opposed to cut specimens in an automated laboratory setting, seal-quality problems are often encountered because of irregular, rough surfaces and difficulties associated with manually holding the probe stationary while applying a uniform normal force of the optimal magnitude on the tip seal. To enable in-situ measurements of friable geologic units and to overcome weathering and seal-quality problems, a new minipermeameter probe has been developed that is specifically intended for application inside a small drilled hole. The design of the small-drillhole minipermeameter probe is discussed in what follows, as well as the accompanying analytical technique and the size and shape of the instrument's averaging volume. This article concludes with brief reviews of data collected using the technique.

2000 ◽  
Author(s):  
Zhiyong Liang ◽  
Chuck Zhang ◽  
Ben Wang ◽  
Chiang Shih

Abstract In a liquid composite molding (LCM) process such as resin transfer molding (RTM), quality control depends on an in-situ permeability profile of the fibrous preform taken just before resin injection. However, the conventional permeability measurement method, which uses liquid (oil or resin) as its working fluid, only measures the average preform permeability in an off-line mode. It cannot be used to create an in-situ permeability profile because of fiber pollution, and cannot be used to reveal local permeability variations of preform. This study develops a new permeability characterization method that uses gas flow and pressure profiles to measure preform permeability variation in a closed mold assembly. This method is based upon two research findings: (1) that the air permeability of a preform can be obtained through measuring the pressure profile of gas flow, and (2) that resin permeability is highly correlated with air permeability for the same fiber preform. In this paper, the validity of this method is discussed. Experimental results of gas permeability measurement with defective and defect-free preforms are presented, and quantitative models for correlation of gas permeability versus pressure profile and of gas permeability versus resin permeability are also provided. Finally, the efficacy of the proposed method is illustrated through experimental results.


2010 ◽  
Vol 10 ◽  
pp. 546-562 ◽  
Author(s):  
Tye Langston

A portable, rapid, and economical method forin situtrace explosive detection in aqueous solutions was demonstrated using photoluminescence. Using europium/thenoyltrifluoroacetone as the reagent, dissolved nitroglycerin was fluorescently tagged and detected in seawater solutions without sample preparation, drying, or preconcentration. The chemical method was developed in a laboratory setting and demonstrated in a flow-through configuration using lightweight, inexpensive, commercial components by directly injecting the reagents into a continually flowing seawater stream using a small amount of organic solvent (approximately 8% of the total solution). Europium's vulnerability to vibrational fluorescence quenching by water provided the mode of detection. Without nitroglycerin in the seawater solution, the reagent's fluorescence was quenched, but when dissolved nitroglycerin was present, it displaced the water molecules from the europium/thenoyltrifluoroacetone compound and restored fluorescence. This effort focused on developing a seawater sensor, but performance comparisons were made to freshwater. The method was found to perform better in freshwater and it was shown that certain seawater constituents (such as calcium) have an adverse impact. However, the concentrations of these constituents are not expected to vary significantly from the natural seawater used herein.


2020 ◽  
Vol 58 (1) ◽  
pp. 30-43
Author(s):  
N.D. Yakimov ◽  
◽  
A.I. Khafizova ◽  
N.D. Chichirova ◽  
O.S. Dmitrieva ◽  
...  
Keyword(s):  
Gas Flow ◽  

1975 ◽  
Vol 40 (11) ◽  
pp. 3315-3318 ◽  
Author(s):  
M. Rylek ◽  
F. Kaštánek ◽  
L. Nývlt ◽  
J. Kratochvíl
Keyword(s):  
Gas Flow ◽  

Hydrobiologia ◽  
1989 ◽  
Vol 188-189 (1) ◽  
pp. 277-283 ◽  
Author(s):  
C. Lindblad ◽  
U. Kautsky ◽  
C. André ◽  
N. Kautsky ◽  
M. Tedengren

Author(s):  
D.M. Seyedi ◽  
C. Plúa ◽  
M. Vitel ◽  
G. Armand ◽  
J. Rutqvist ◽  
...  

2021 ◽  
Vol 11 (4) ◽  
pp. 1936
Author(s):  
Abdel-Hakim Bouzid

The accurate prediction of liquid leak rates in packing seals is an important step in the design of stuffing boxes, in order to comply with environmental protection laws and health and safety regulations regarding the release of toxic substances or fugitive emissions, such as those implemented by the Environmental Protection Agency (EPA) and the Technische Anleitung zur Reinhaltung der Luft (TA Luft). Most recent studies conducted on seals have concentrated on the prediction of gas flow, with little to no effort put toward predicting liquid flow. As a result, there is a need to simulate liquid flow through sealing materials in order to predict leakage into the outer boundary. Modelling of liquid flow through porous packing materials was addressed in this work. Characterization of their porous structure was determined to be a key parameter in the prediction of liquid flow through packing materials; the relationship between gland stress and leak rate was also acknowledged. The proposed methodology started by conducting experimental leak measurements with helium gas to characterize the number and size of capillaries. Liquid leak tests with water and kerosene were then conducted in order to validate the predictions. This study showed that liquid leak rates in packed stuffing boxes could be predicted with reasonable accuracy for low gland stresses. It was found that internal pressure and compression stress had an effect on leakage, as did the thickness change and the type of fluid. The measured leak rates were in the range of 0.062 to 5.7 mg/s for gases and 0.0013 and 5.5 mg/s for liquids.


Author(s):  
Lei Xu ◽  
Wen Zhang ◽  
Tao Luo ◽  
Jin-Hui Yang ◽  
Zhaochu Hu

High precise and accurate measurements of Fe isotope ratios for fourteen reference materials from the USGS, MPI-DING and CGSG were successfully carried out using a developed analytical technique by fs...


1990 ◽  
Vol 140 ◽  
pp. 133-134
Author(s):  
J. Panesar ◽  
A.H. Nelson

We report here some preliminary results of 3–D numerical simulations of an α–ω dynamo in galaxies with differential rotation, small–scale turbulence, and a shock wave induced by a stellar density wave. We obtain the magnetic field from the standard dynamo equation, but include the spiral shock velocity field from a hydrodynamic simulation of the gas flow in a gravitational field with a spiral perturbation (Johns and Nelson, 1986).


Sign in / Sign up

Export Citation Format

Share Document