scholarly journals Study of Microvoids in High-Rate a-Si:H Using Positron Annihilation

1997 ◽  
Vol 467 ◽  
Author(s):  
X. Zou ◽  
D. P. Webb ◽  
S. H. Lin ◽  
Y. W. Lam ◽  
Y. C. Chan ◽  
...  

ABSTRACTIn this paper, we have carried out the positron annihilation measurement on high-rate and low-rate a-Si:H thin films deposited by PECVD. By means of the slow positron beam Doppler-broadening technique, the depth profiles of microvoids in a-Si:H have been determined. We have also studied the vacancy-type defect in the surface region in high-rate grown a-Si:H, making comparison between high-rate and low-rate a-Si:H. By plotting S and W parameters in the (S, W) plane, we have shown that the vacancies in all of the high-rate and low-rate deposited intrinsic samples, and in differently doped low-rate samples are of the same nature.

1998 ◽  
Vol 13 (10) ◽  
pp. 2833-2840
Author(s):  
X. Zou ◽  
D. P. Webb ◽  
Y. C. Chan ◽  
Y. W. Lam ◽  
Y. F. Hu ◽  
...  

In this paper, positron annihilation measurements have been carried out on a-Si: H thin films deposited by plasma-enhanced chemical vapor deposition (PECVD) at high and low rates by means of the variable energy positron beam Doppler-broadening technique. The depth profiles of microvoids in the films grown under different conditions have been determined. We found a smaller void fraction in the surface region of all films compared to the bulk, and a smaller void fraction in low rate than in high growth rate films. By plotting S and W parameters in the (S, W) plane, we have shown that the vacancies in all of the high-rate and low-rate deposited intrinsic samples, and in differently doped low-rate samples are of the same nature, although there appears to be a higher density of defects in the boron than phosphorus doped films. The depth profiles of the microvoid-like defects in the a-Si: H films are extracted by use of the vepfit program.


Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1689
Author(s):  
Vladimir Slugen ◽  
Jarmila Degmova ◽  
Stanislav Sojak ◽  
Martin Petriska ◽  
Pavol Noga ◽  
...  

New materials for advanced fission/fusion nuclear facilities must inevitably demonstrate resistance to radiation embrittlement. Thermal and radiation ageing accompanied by stress corrosion cracking are dominant effects that limit the operational condition and safe lifetime of the newest nuclear facilities. To study these phenomena and improve the current understanding of various aspects of radiation embrittlement, ion bombardment experiments are widely used as a surrogate for neutron irradiation. While avoiding the induced activity, typical for neutron-irradiated samples, is a clear benefit of the ion implantation, the shallow near-surface region of the modified materials may be a complication to the post-irradiation examination (PIE). However, microstructural defects induced by ion implantation can be effectively investigated using various spectroscopic techniques, including slow-positron beam spectroscopy. This method, typically represented by techniques of positron annihilation lifetime spectroscopy and Doppler broadening spectroscopy, enables a unique depth-profile characterisation of the near-surface region affected by ion bombardment or corrosion degradation. One of the best slow-positron beam facilities is available at the pulsed low-energy positron system (PLEPS), operated at FRM-II reactor in Munich (Germany). Bulk studies (such as high energy ion implantation or neutron irradiation experiments) can be, on the other hand, effectively performed using radioisotope positron sources. In this paper, we outline some basics of the two approaches and provide some recommendations to improve the validity of the positron annihilation spectroscopy (PAS) data obtained on ion-irradiated samples using a conventional 22Na positron source.


2007 ◽  
Vol 4 (10) ◽  
pp. 3659-3663 ◽  
Author(s):  
S. Neretina ◽  
D. Grebennikov ◽  
R. A. Hughes ◽  
M. Weber ◽  
K. G. Lynn ◽  
...  

2004 ◽  
Vol 19 (23) ◽  
pp. 3951-3959 ◽  
Author(s):  
CORINE BAS ◽  
N. DOMINIQUE ALBÉROLA ◽  
MARIE-FRANCE BARTHE ◽  
JÉRÉMIE De BAERDEMAEKER ◽  
CHARLES DAUWE

A series of dense copolyimide membranes was characterized using positron annihilation spectroscopy. The positron annihilation lifetime spectroscopy performed on film with a classical positron source gives informations on the positronium fraction formed and also on the hole size within the film. The Doppler broadening spectra (DBS) of the gamma annihilation rays coupled with a variable energy positron beam allow the microstructural analyses as a function of the film depth. Experimental data were also linked to the chemical structure of the polyimides. It was found that the presence of the fluorine atoms strongly affects the positron annihilitation process and especially the DBS responses.


1989 ◽  
Vol 67 (8) ◽  
pp. 813-817
Author(s):  
P. Hautojārvi

The use of positron annihilation to study defects in semiconductors is discussed. Positron-lifetime spectroscopy reveals As vacancies in as-grown GaAs and gives information on ionization levels. The vacancy profiles in ion-implanted Si are investigated by slow positron beam.


2017 ◽  
Vol 373 ◽  
pp. 91-95 ◽  
Author(s):  
Da Qing Yuan ◽  
Qiao Li Zhang ◽  
Ping Fan ◽  
Xian Ping Wang ◽  
Bin Long ◽  
...  

The oxide dispersed strengthened (ODS) ferritic-martensitic steel was irradiated by 100MeV iron ion whose energy was degraded by using a Ta foil of 4 μm thick, 100 keV Hydrogen and 200 keV Helium at 480, 515, 550 and 580 °C. The irradiation fluences were 1×1016, 1.1×1015 and 6.8×1013/cm2, respectively for Fe, H and He. The techniques of positron annihilation lifetime and Doppler broadening of slow positron beam were utilized to examine the produced radiation damage. At 550 °C the maximal positron annihilation lifetime and S parameter of Doppler broadening were observed, implyin g tha t 550 °C is the pea k temperature of swelling. The S parameter and annihilation lifetime of the sample irradiated at 515 °C by the single Fe ion beam were smaller compared to the triple beam irradiation at the same temperature, implying that the triple beam irradiation caused more severe damage than the single beam irradiation.


2008 ◽  
Vol 607 ◽  
pp. 238-242 ◽  
Author(s):  
Nagayasu Oshima ◽  
Ryoichi Suzuki ◽  
Toshiyuki Ohdaira ◽  
Atsushi Kinomura ◽  
T. Narumi ◽  
...  

To improve the spatial resolution of positron annihilation spectroscopy (PAS), a system to produce an intense positron microbeam was developed in AIST. A slow positron beam, which was produced by an electron linear accelerator, was focused by a lens onto a remoderator to enhance its brightness. The brightness-enhanced beam with an intensity of ≈1 × 106 e+/s was extracted from the remoderator and focused onto the sample by a lens. The beam size at the sample was 25 μm, which is more than two and half orders of magnitude smaller than that in the magnetic transport system (≈10 mm). Hence, the spatial resolution of PAS with an AIST positron microbeam can be drastically improved relative to PAS using conventional methods.


2009 ◽  
Vol 6 (11) ◽  
pp. 2589-2591 ◽  
Author(s):  
P. Maheshwari ◽  
D. Dutta ◽  
S. Samanta ◽  
A. Singh ◽  
D. K. Aswal ◽  
...  

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