Growth of 130 μm Thick Epitaxial KNbO3 Film by Hydrothermal Method

2013 ◽  
Vol 1494 ◽  
pp. 291-296 ◽  
Author(s):  
T. Shiraishi ◽  
H. Einishi ◽  
M. Ishikawa ◽  
T. Hasegawa ◽  
M. Kurosawa ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Film Thickness ◽  
Hydrothermal Method ◽  
Thick Film ◽  
Xrd Analysis ◽  
Structure Change ◽  
Thickness Direction ◽  
Cross Sectional ◽  
Sem Observation ◽  
Raman Spectral

ABSTRACTKNbO3 thick films were deposited on (100)c SrRuO3//(100)SrTiO3 substrates at 240 °C for 3 h by hydrothermal method. Film thickness increased linearly with increasing the deposition number of times and 130 μm thickness was achieved by the 6 time deposition. XRD analysis showed the growth of epitaxial orthorhombic films with the mixture orientation of (100), (010) and (001). Cross-sectional SEM observation showed that the 130 μm-thick film was dense and no obvious voids inside the film. In addition, the crystal structure change along film thickness direction was not detected from the cross-sectional Raman spectral observation.

Examination of Rubber Adhesion Property of Brass Film on Steel Formed by Magnetron Sputtering

2005 ◽  
Vol 78 (1) ◽  
pp. 105-113 ◽  
Author(s):  
Michael T. Yamauchi ◽  
Toshi Shimizu ◽  
Mitch Doi ◽  
David T. Yasunaga ◽  
Takenori Nakayama ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Magnetron Sputtering ◽  
Film Thickness ◽  
Adhesion Force ◽  
Adhesion Property ◽  
Cross Sectional ◽  
Steel Cord ◽  
Ar Plasma ◽  
Excellent Adhesion

Abstract Brass films were formed on steel rods by magnetron sputtering by using 63 wt% Cu - 37 wt% Zn target in Ar plasma. The brass plated steel rods were inserted in crude rubber and then cured to form various samples. Rubber-brass inter-reacted layers were investigated by cross sectional TEM observation. Evaluation of adhesion force was also conducted in order to compare with the TEM investigation. The magnetron sputtering brass film has strongly oriented columner crystal structure and thickness of the film is uniform in whole area. The magnetron sputtering film has excellent adhesion regardless of the film thickness that cannot be attained by that of commercially manufactured steel cord.

Structural, Thermal and Electrical Properties of Doped Poly(3,4 ethylenedioxythiophene)

2016 ◽  
Vol 10 (4) ◽  
pp. 395-400 ◽  
Author(s):  
Deepali Kelkar ◽  
◽  
Ashish Chourasia ◽  
◽  
Keyword(s):  
Crystal Structure ◽  
Electrical Properties ◽  
Xrd Analysis ◽  
Structure Modification ◽  
Camphorsulfonic Acid ◽  
Thermal And Electrical Properties ◽  
Ft Ir

Poly(3,4-ethylenedioxythiophene) (PEDOT) was chemically synthesized, undoped and then re-doped using FeCl3 as well as camphorsulfonic acid (CSA). FT-IR results confirm the nature of the synthesized and doped samples. XRD analysis indicates crystal structure modification after doping and was also used to calculate crystallinity of samples. Crystallinity increases after FeCl3 doping, whereas it reduces due to CSA doping. TGA-DTA results show reduction in Tg value for FeCl3 doped sample while it increases for CSA doped samples compared to that of undoped PEDOT. Reduction in Tg indicates plasticizing effect of FeCl3 whereas increase in Tg show anti-plasticizing effect of CSA in PEDOT. Conductivity value () increases by two orders of magnitude after doping. Log vs. 1/T graph show metallic nature of undoped PEDOT above 308 K, however both doped samples show semiconducting nature from 301 to 383 K.

Microstructure Characterization of Ag Nanoparticles Prepared by Hydrothermal Method

2012 ◽  
Vol 476-478 ◽  
pp. 1138-1141
Author(s):  
Zhi Qiang Wei ◽  
Qiang Wei ◽  
Li Gang Liu ◽  
Hua Yang ◽  
Xiao Juan Wu
Keyword(s):  
Crystal Structure ◽  
Particle Size ◽  
Hydrothermal Method ◽  
Ag Nanoparticles ◽  
Average Particle Size ◽  
Average Particle ◽  
Face Centered Cubic ◽  
Selected Area Electron Diffraction ◽  
Transmission Electron ◽  
Face Centered

Ag nanoparticles were successfully synthesized by hydrothermal method under the polyol system combined with traces of sodium chloride, Silver nitrate(AgNO3) and polyvinylpyrrolidone (PVP) acted as the silver source and dispersant respectively. The samples by this process were characterized via X-ray powder diffraction (XRD), Brunauer–Emmett–Teller (BET) adsorption equation, transmission electron microscopy (TEM) and the corresponding selected area electron diffraction (SAED) to determine the chemical composition, particle size, crystal structure and morphology. The experiment results indicate that the crystal structure of the samples is face centered cubic (FCC) structure as same as the bulk materials, The specific surface area is 24 m2/g, the particle size distribution ranging from10 to 50 nm, with an average particle size about 26 nm obtained by TEM and confirmed by XRD and BET results.

Effect of Film Thickness on Fatigue Strength of TiAl Alloy Coated with TiAlN Film at Elevated Temperature

2005 ◽  
Vol 297-300 ◽  
pp. 1446-1451 ◽  
Author(s):  
Takeshi Kasuya ◽  
Hideto Suzuki
Keyword(s):  
Thin Film ◽  
Fatigue Strength ◽  
Film Thickness ◽  
Thick Film ◽  
Physical Vapor Deposition ◽  
Tial Alloy ◽  
Testing Machine ◽  
Intermetallic Alloy ◽  
Fracture Control ◽  
The Difference

The fatigue strength of TiAl intermetallic alloy coated with TiAlN film was studied in vacuum at 1073K using a SEM-servo testing machine. In addition, three kinds of TiAlN films were given by physical vapor deposition (1, 3, and 10μ m). The fatigue strength of 3μ m was highest. Also, the fatigue strength of 1μ m was lowest. From this result, existence of optimum film thickness was suggested because the difference of fatigue strength arose in each film thickness. The justification for existence of optimum film thickness is competition of 45-degree crack and 90-degree crack. The 45-degree crack is phenomenon seen in the thin film (1μ m), and is caused by plastic deformation of TiAl substrate. The 45-degree crack is the factor of the fatigue strength fall by the side of thin film. In contrast, the 90-degree crack is phenomenon in the thick film (10μ m), and is caused as result of reaction against load to film. The 90-degree crack is the factor of the fatigue strength fall by the side of thick film. In conclusion, the optimum film thickness can perform meso fracture control, and improves fatigue strength.

Synthesis, Characterization, and Gas Sensing performance of Nanometer TiO2 thick film by Hydrothermal method

2020 ◽  
Vol 13 (5) ◽  
pp. 360-364
Author(s):  
J. R. Pitrubhakta ◽  
Tushar A. Kere ◽  
Shilpa S. Shinde ◽  
Suyog A. Soni ◽  
V. R. Jadhav
Keyword(s):  
Hydrothermal Method ◽  
Thick Film ◽  
Gas Sensing ◽  
Sensing Performance

Microstructure of LaB6-base thick film resistors

1992 ◽  
Vol 7 (8) ◽  
pp. 2225-2229 ◽  
Author(s):  
Z.G. Li ◽  
P.F. Carcia ◽  
P.C. Donohue
Keyword(s):  
Electron Microscopy ◽  
Transmission Electron Microscopy ◽  
Thick Film ◽  
Surface Area ◽  
Ion Milling ◽  
Cross Sectional ◽  
Electrically Conductive ◽  
Transmission Electron ◽  
High Temperature Processing ◽  
Thin Wedge

The microstructure of LaB6-base thick film resistors was investigated by cross-sectional transmission electron microscopy. The specimens were prepared by a technique that polished them to a thin wedge, thus avoiding ion-milling and permitting imaging over a distance of tens of microns. The resistor microstructure contained a finely divided electrically conductive phase of TaB2 and nonconducting crystals of CaTa4O11, formed during high temperature processing of glass and LaB6 ingredients of the thick film ink. Using higher surface area ingredients virtually suppressed the formation of CaTa4O11 crystals, and the microstructure became more uniform. Resistors made with higher surface area intermediates also had better voltage withstanding properties.

scholarly journals Magnetic Properties and SAR for Gadolinium-Doped Iron Oxide Nanoparticles Prepared by Hydrothermal Method

Crystals ◽  
2021 ◽  
Vol 11 (10) ◽  
pp. 1153
Author(s):  
Heba Kahil ◽  
Ahmed Faramawy ◽  
Hesham El-Sayed ◽  
Adel Abdel-Sattar
Keyword(s):  
Iron Oxide ◽  
Hydrothermal Method ◽  
Iron Oxide Nanoparticles ◽  
Photoelectron Spectroscopy ◽  
Pure Iron ◽  
Xrd Analysis ◽  
Solubility Limit ◽  
Great Promise ◽  
Oxide Nanoparticles ◽  
Pure Iron Oxide

This study is an attempt to produce gadolinium-doped iron oxide nanoparticles for the purpose of utilization in magnetic fluid hyperthermia (MFH). Six gadolinium-doped iron oxide samples with varying gadolinium contents ( were prepared using the hydrothermal method and high vapor pressure to incorporate gadolinium ions in the iron oxide structure. The samples were indexed as , with varying from 0.0 to 0.1. The results reveal that gadolinium ions have a low solubility limit in the iron oxide lattice (x = 0.04). The addition of gadolinium caused distortion in the produced maghemite phase and formation of other phases. Based on X-ray diffraction (XRD) analysis and photoelectron spectroscopy (XPS), it was observed that gadolinium mostly crystalized as gadolinium hydroxide, for gadolinium concentrations above the solubility limit. The measured magnetization values are consistent with the formed phases. The saturation magnetization values for all gadolinium-doped samples are lower than the undoped sample. The specific absorption rate (SAR) for the pure iron oxide samples was measured. Sample GdIO/0.04, pure iron oxide doped with gadolinium, showed the highest potential to produce heat at a frequency of 198 kHz. Therefore, the sample is considered to hold great promise as an MFH agent.

Photocatalytic Oxidation of Arsenic(III) by Hydrothermal Synthesized TiO2 Loaded on Activated Carbon Fiber

2013 ◽  
Vol 631-632 ◽  
pp. 176-180 ◽  
Author(s):  
Ying Hao Xie ◽  
Zhan Chang Pan ◽  
Zhi Gang Wei ◽  
Wei Lin Feng ◽  
Jun Hui Zuo ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Activated Carbon ◽  
Carbon Fiber ◽  
Hydrothermal Method ◽  
Photocatalytic Oxidation ◽  
Catalytic Efficiency ◽  
Activated Carbon Fiber ◽  
Acidic Environment ◽  
Effect Of Ph ◽  
Alkaline Environment

In this paper, nano TiO2 loaded on activated carbon fiber(ACF) was prepared by hydrothermal method as TiO2/ACF photocatalytic.The material crystal structure, the superficial appearance of catalyst, were analyzed and measured by XRD and SEM images.Moreover, it used for photocatalytic oxidation As(Ⅲ).The effect of pH on the oxidation of As(Ⅲ) was studied. The oxidation of As(Ⅲ) efficiency increasing markedly with pH, and the catalytic efficiency is much higher in the alkaline environment than in the acidic environment.

scholarly journals X-ray diffraction analysis of MTA-Plus, MTA-Angelus and DiaRoot BioAggregate

2014 ◽  
Vol 08 (02) ◽  
pp. 211-215 ◽  
Author(s):  
Yeliz Guven ◽  
Elif Bahar Tuna ◽  
Muzaffer Emin Dincol ◽  
Oya Aktoren
Keyword(s):  
Crystal Structure ◽  
Tantalum Oxide ◽  
Xrd Analysis ◽  
Tricalcium Silicate ◽  
Dicalcium Silicate ◽  
Glass Slide ◽  
Phase Identification ◽  
X Ray Diffraction ◽  
X Ray ◽  
Tricalcium Aluminate

ABSTRACT Objective: The purpose of this study was to investigate and compare the crystalline structures of recently released MTA Plus (MTA-P), MTA Angelus (MTA-A), DiaRoot BioAggregate (BA) by X-ray diffraction (XRD) analysis. Materials and Methods: Phase analysis was carried out on powder and set forms of tested materials. The powder specimens placed into sample holders that were packed with a glass slide and the set samples prepared according to the manufacturer's instructions were placed into molds. The samples after being set for three days at 37°C and 100% humidity in an incubator were mounted onto the XRD machine and phase identification was accomplished using a search-match software program. Results: XRD findings indicated that major constituents of MTA-P were bismuth oxide, portlandite, dicalcium silicate and tricalcium silicate. The crystal structure of MTA-A were similar to those of MTA-P except for the absence of portlandite. Additionally, MTA-A had tricalcium aluminate differing from MTA-P. BA mainly differed from MTA-P and MTA-A by the radiopacifier (tantalum oxide-TO) in its composition. Conclusions: The majority of constituents of the tested materials have shown similarity except for the presence of tricalcium aluminate in MTA-A and the inclusion of TO in BA. In addition, set MTA-P showed a strong peak of portlandite.

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