Organic Analysis. XIV. Infrared Spectra of Phenylsulfonyl Derivatives. (3). The C-H Deformation Vibrations of Benzene Ring, the CH3 Rocking Frequencies of SO2CH3 Group, and the Characteristic Absorption Bands of SO2NH2 Group.

1959 ◽  
Vol 7 (6) ◽  
pp. 734-739 ◽  
Author(s):  
Tsutomu Momose ◽  
Yo Ueda ◽  
Tatsuo Shoji
Keyword(s):  
Benzene Ring ◽  
Infrared Spectra ◽  
Organic Analysis ◽  
Absorption Bands ◽  
Characteristic Absorption

Anomalies in the Infrared Spectra of Mixed Carbonate Precipitates

1968 ◽  
Vol 22 (5) ◽  
pp. 497-501 ◽  
Author(s):  
Gene E. Kalbus ◽  
Eugene A. Berg ◽  
Lee H. Kalbus
Keyword(s):  
Infrared Spectra ◽  
Anomalous Behavior ◽  
Absorption Bands ◽  
Characteristic Absorption ◽  
Quantitative Measurements ◽  
Mixed Carbonate

When a mixture of cations in solution is precipitated by the addition of carbonate, the resulting mixed carbonate precipitate, when subjected to infrared examination, does not usually exhibit the individually characteristic absorption bands due to each of the carbonates constituting the mixture. Instead, various interesting anomalies such as blending of bands, shifting of positions, and changing of intensities are observed. Such anomalous behavior may hamper any qualitative or quantitative measurements on such samples. Representative spectra and possible explanations for some of these anomalies are presented.

The Infrared Spectra of Some 1-(2-Thienyl)-3- and -4-Thiaalkanes

1979 ◽  
Vol 33 (6) ◽  
pp. 578-581
Author(s):  
Norman G. Foster ◽  
Bernice B. Bonner ◽  
Robert W. Higgins
Keyword(s):  
Absorption Band ◽  
Infrared Spectra ◽  
Thiophene Ring ◽  
Absorption Bands ◽  
Characteristic Absorption ◽  
Molecular Weights ◽  
Ring Compounds ◽  
Major Absorption Band

The infrared spectra of six 1-(2-thienyl)-3-thiaalkanes and seven 1-(2-thienyl)-4-thiaalkanes (molecular weights from 186 to 270) were obtained for the 4000 to 400 cm−1 range. These spectra are compared with spectra of other thiophene ring compounds substituted in the 2-position for their characteristic absorption bands. The spectra agree with other spectra as to the major absorption band around 680 cm−1 and the 2-substitution overtone pattern. A method of distinguishing between the two groups of compounds from moderate peaks in the 600 to 500 cm−1 (KBr) region is shown. Interference from the 2-alkylthiophenes and the 1-(2-thienyl)-1-thiaalkanes does not occur.

Infrared Spectra of Some α,ω-Dinitroxy Alkanes

1966 ◽  
Vol 20 (6) ◽  
pp. 380-383 ◽  
Author(s):  
R. D. Barefoot ◽  
A. R. Lawrence
Keyword(s):  
Infrared Spectra ◽  
Absorption Bands ◽  
Frequency Shifts ◽  
Characteristic Absorption

The infrared spectra of eight α, ω-dinitroxy alkanes are examined, and frequency shifts and related intensities of characteristic absorption bands are discussed.

An Infrared Study of Metal Isopropoxide Precursors for SrTiO3

1984 ◽  
Vol 32 ◽  
Author(s):  
R. E. Riman ◽  
D. M. Haaland ◽  
C.J.M. Northrup ◽  
H. K. Bowen ◽  
A. Bleier
Keyword(s):  
Ir Spectra ◽  
Detailed Analysis ◽  
Infrared Spectra ◽  
Spectral Features ◽  
Absorption Bands ◽  
Infrared Study ◽  
Characteristic Absorption ◽  
Local Environments ◽  
Insight Into ◽  
Hydrolysis Reactions

ABSTRACTA Sr/Ti bimetallic isopropoxide complex was synthesized by two methods. The complex served as a precursor to the production of homogeneous SrTiO3 powders via alkoxide hydrolysis. Infrared spectra were obtained for Sr(OPri)2, Ti(OPri)4, and the product of the syntheses. In addition, the IR spectra of the solutions of each of the alkoxides were followed as hydrolysis reactions proceeded. Detailed analysis of the spectral features support the existence of a 1:1 Sr/Ti bimetallic alkoxide. The new Sr/Ti compound exhibits characteristic absorption bands at (1017, 993, 972, 961 cm−1), (844, 838, 827 cm−1) and (620, 596, and 572 −1). A band at 819−1 might also be associated with the new Sr/Ti bimetallic alkoxide. The infrared spectra suggest that the isopropoxide ligands in the bimetallic alkoxide are in at least three separate local environments. This information offers insight into possible structures for the complex.

Pyrrole Studies. I. The Infrared Spectra of 2-Monosubstituted Pyrroles

1963 ◽  
Vol 16 (1) ◽  
pp. 93 ◽  
Author(s):  
RA Jones
Keyword(s):  
Infrared Spectra ◽  
Infrared Absorption ◽  
Absorption Bands ◽  
Infrared Absorption Bands

The positions and intensities of the characteristic infrared absorption bands of the nucleus are recorded and discussed for thirty-five 2-monosubstituted pyrroles.

scholarly journals A surface confined yttrium(iii) bis-phthalocyaninato complex: a colourful switch controlled by electrons

2016 ◽  
Vol 7 (8) ◽  
pp. 4940-4944 ◽  
Author(s):  
I. Alcón ◽  
M. Gonidec ◽  
M. R. Ajayakumar ◽  
M. Mas-Torrent ◽  
J. Veciana
Keyword(s):  
Optical Properties ◽  
Absorption Bands ◽  
Electrical And Optical Properties ◽  
Redox States ◽  
Characteristic Absorption ◽  
Double Decker ◽  
Visible Spectra

SAMs of a Y(iii) double-decker complex on ITO have been prepared and their electrical and optical properties explored, exhibiting three accessible stable redox states with characteristic absorption bands in the visible spectra, corresponding to three complementary colors (i.e., green, blue and red).

scholarly journals Synthesis of ZnO and CuO nanoparticles via Sol gel method and Its Characterization by using XRD and FT-IR Analysis

2022 ◽  
Author(s):  
Monika Patel ◽  
Sunita Mishra ◽  
Ruchi Verma ◽  
Deep Shikha
Keyword(s):  
Particle Size ◽  
Zno Nanoparticles ◽  
Sol Gel ◽  
Broad Band ◽  
Zinc Nitrate ◽  
Zno Nanoparticle ◽  
Absorption Bands ◽  
Characteristic Absorption ◽  
Sol Gel Process ◽  
Ft Ir

Abstract Nanotechnology is a completely unique branch of technology that offers with substances in a very small size between (1-100 nm) with various crystal shapes which include spherical nanoparticles, flower shaped, Nano rods, Nano ribbons, and Nano platelets. Metals have ability to produce large number of oxides. These metal oxides play an major role in many areas of chemistry, physics, material science and food science. In this research, Zinc Oxide (ZnO) and Copper (II) oxide nanoparticles were synthesized via sol-gel process using zinc nitrate and copper (II) nitrate as precursor respectively. The characterization of CuO and ZnO nanoparticles was done by using various techniques. X-ray Diffraction (XRD) indicates the crystallinity and crystal size of CuO and ZnO nanoparticle. Fourier transform infrared spectroscopy (FT-IR) was used to get the infrared spectrum of the sample indicating composition of the sample which contains various functional groups. XRD result shows the particle size of CuO at highest peak 29.40140 was 61.25 nm and the particle size of ZnO at highest peak 36.24760 was 21.82 nm. FT-IR spectra peak at 594.56 cm-1 indicated characteristic absorption bands of ZnO nanoparticles and the broad band peak at 3506.9 cm-1 can be attributed to the characteristic absorption of O-H group. The analysis of FT-IR spectrum of CuO shows peaks at 602.09, 678.39, and 730.19cm−1 which refer to the formation of CuO. A broad absorption peak noticed at 3308.2 cm−1 attributed to O–H stretching of the moisture content.

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