scholarly journals Reference Materials for the Pyrolysis Gas-chromatographic Determination of Ammonia, Nitrogen, Nitrogen Monoxide, Carbon Monoxide, and Carbon Dioxide

1982 ◽  
Vol 55 (11) ◽  
pp. 3647-3648 ◽  
Author(s):  
Kikuo Miyokawa ◽  
Naoki Abe ◽  
Isao Masuda
Keyword(s):  
Carbon Dioxide ◽  
Carbon Monoxide ◽  
Reference Materials ◽  
Nitrogen Monoxide ◽  
Chromatographic Determination ◽  
Ammonia Nitrogen ◽  
Pyrolysis Gas

Gas-Solid Chromatographic Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke

1974 ◽  
Vol 57 (1) ◽  
pp. 1-7
Author(s):  
Arthur D Horton ◽  
Michael R Guerin
Keyword(s):  
Carbon Dioxide ◽  
Carbon Monoxide ◽  
Gas Phase ◽  
Confidence Intervals ◽  
Cigarette Smoke ◽  
Chromatographic Determination ◽  
Standard Errors ◽  
Sampling Techniques ◽  
Relative Standard

Abstract Gas-solid chromatographic methods are presented for the determination of carbon monoxide, carbon dioxide, or both simultaneously in the gas phase of cigarette smoke. The methods are optimized to allow quantitative determinations on the entire gas phase delivery of the cigarettes rather than single puffs and to allow the use of small numbers of cigarettes. Shortcomings of several sampling techniques are defined, and evidence is presented supporting the utility of Saran bag sampling and containment. Carbon monoxide and carbon dioxide analyses may be performed with relative standard errors of 2—3% and relative confidence intervals (95%) of 6—9% for determinations involving 4—6 cigarettes.

RUMEN GAS ANALYSIS BY GAS-SOLID CHROMATOGRAPHY

1961 ◽  
Vol 41 (2) ◽  
pp. 187-196 ◽  
Author(s):  
J. M. McArthur ◽  
J. E. Miltimore
Keyword(s):  
Carbon Dioxide ◽  
Carbon Monoxide ◽  
Hydrogen Sulphide ◽  
Sample Volume ◽  
Gas Analysis ◽  
Complete Analysis ◽  
Thermal Detector ◽  
Thermal Detection ◽  
Methane Carbon

Methods are described for sampling and analysing rumen gases. The analysis requires less than 15 minutes for the determination of hydrogen, oxygen, nitrogen, methane, carbon monoxide, carbon dioxide, and hydrogen sulphide, i.e., for all gases occurring in the rumen. The method is sensitive and requires only a small quantity of sample, and the sample volume need not be known. The presence of water or other vapours in the sample does not influence the results. Relative thermal detector responses have been determined for gases which occur in the rumen. These eliminate the necessity for the calibration of gas chromatographs using thermal detection. The first complete analysis of rumen gas is presented.

scholarly journals The Use of Cryogenic Temperature Gas Chromatography for the Determination of Carbon Monoxide and Carbon Dioxide in Cigarette Smoke

1972 ◽  
Vol 6 (4) ◽  
Author(s):  
G.P. Morie ◽  
C.H. Sloan
Keyword(s):  
Carbon Dioxide ◽  
Gas Chromatography ◽  
Carbon Monoxide ◽  
Liquid Nitrogen ◽  
Cigarette Smoke ◽  
Cryogenic Temperature ◽  
Chromatographic Method ◽  
Porapak Q ◽  
Gas Chromatographic Method

AbstractA gas chromatographic method for the determination of carbon monoxide and carbon dioxide in cigarette smoke was developed. A column containing Porapak Q packing and a cryogenic temperature programmer which employed liquid nitrogen to cool the column to subambient temperatures was used. The separation of N

Gas-Solid Chromatographic Determination of Oxygen, Nitrogen, Carbon Dioxide, Ethylene, and Nitrous Oxide at Ambient Temperature

1973 ◽  
Vol 56 (1) ◽  
pp. 119-123
Author(s):  
Martin J Finkelson
Keyword(s):  
Carbon Dioxide ◽  
Nitrous Oxide ◽  
Ambient Temperature ◽  
Molecular Sieve ◽  
Internal Standard ◽  
Chromatographic Determination ◽  
Digital Integrator ◽  
In Series ◽  
Peak Areas

Abstract A gas-solid chromatographic method is described for the separation and determination of 5 medicinal gases at ambient temperature, using 2 gas chromatographic columns, Porapak Q and Molecular Sieve 13X, operated in series with a 6-port thermal conductivity detector and I recorder. An electronic digital integrator is used for calculating peak areas. Data on retention time, linearity, reproducibility of injection, and comparison with absorption methods are presented. Analytical results for oxygen, nitrogen, carbon dioxide, ethylene, and nitrous oxide are attainable within 1.0% without the use of an internal standard.

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