scholarly journals Effect of Removal of Enamel on Rebonding Strength of Resin Composite to Enamel

2016 ◽  
Vol 2016 ◽  
pp. 1-7 ◽  
Author(s):  
L. Kilponen ◽  
L. Lassila ◽  
M. Tolvanen ◽  
J. Varrela ◽  
P. K. Vallittu
Keyword(s):  
Surface Layer ◽  
Bond Strength ◽  
Resin Composite ◽  
Optical Profilometer ◽  
Bond Strengths

Objective. To examine the effect of removing the surface layer of enamel on the rebonding strength of resin composite.Methods. Teeth in four groups (n=10) were etched, a small amount of resin composite was bonded and debonded, then specimens in three groups were ground for different lengths of time (10 s, 20 s, 30 s) to remove an increasing amount of enamel, one group was left untouched. The teeth were bonded again and the bond strengths of 1st and 2nd bonding were compared and analysed against the amount of enamel loss in different groups (7 µm (±2); 12 µm (±1); 16 µm (±3)). Specimens were examined with SEM and by noncontacting optical profilometer.Results. Although results indicated higher rebonding strength with increasing enamel removal ANOVA showed low statistical differences between the groups (p>0.05). However, values between first bonding and rebonding strengths differed significantly (p<0.05) in the group that was not ground. SEM revealed that enamel-surfaces that were ground after debonding etched well, compared to the surfaces that still contained adhesive remnants.Conclusions. Removal of small amount of enamel refreshed the surface for rebonding. Rebonding strengths without grinding the surface before bonding were lower than bond strength to intact enamel.

Adhesion of Resins to Ag-Pd Alloys by Means of the Silicoating Technique

1987 ◽  
Vol 66 (8) ◽  
pp. 1380-1385 ◽  
Author(s):  
H. Herø ◽  
I.E. Ruyter ◽  
M.L. Waarli ◽  
G. Hultquist
Keyword(s):  
Surface Layer ◽  
Bond Strength ◽  
Chemical Bonding ◽  
Silicon Oxide ◽  
Surface Defects ◽  
Water Storage ◽  
Flame Spraying ◽  
Four Point Bending ◽  
Bond Strengths ◽  
Oxide Particles

The purpose of the investigation was to study the effect of water storage on the bond strengths between silanized, silicoated Ag-Pd alloys and veneered composites, in comparison with the bond strengths of systems with conventional retention beads. Furthermore, the mechanism of the bonding was examined. The bond strength of silanized, silicoated dry specimens and similar specimens stored in water was measured by four-point bending. Water storage for 90 days at 37°C reduced the bond strength by approximately 30% to about 15-20 MPa. Mechanical retention beads caused bond strengths of approximately 16-18 MPa which were unaffected by water storage. SEM and microprobe investigations showed that sandblasting with Al2O3 prior to silanization caused substantial numbers of cracks and porosities in the surface layer of the alloy, partly filled with Al2O3. Some particles of silicon oxide in these surface defects were produced by the flame-spraying of the so-called silicoating technique. Further painting of the surface with a silane adhesion primer provided chemical bonding to the composite at the densely spaced Si-O-H-containing silica particles. Many cracks were observed in the interfaces between these particles; thus, water is likely to penetrate the interface with time. The bond strength is most likely reduced by reaction between water and the compositelSi-O structure. The silicon oxide particles are probably attached to the alloy substrate by mechanical retention. Without sandblasting, no bonding was obtained by means of the silicoating technique.

scholarly journals Shear Bond Strengths and Morphological Evaluation of Filled and Unfilled Adhesive Interfaces to Enamel and Dentine

2012 ◽  
Vol 2012 ◽  
pp. 1-9 ◽  
Author(s):  
Vajihesadat Mortazavi ◽  
Mohammadhosein Fathi ◽  
Ebrahim Ataei ◽  
Niloufar Khodaeian ◽  
Navid Askari
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Testing Machine ◽  
The Other ◽  
Adhesive Systems ◽  
Morphological Evaluation ◽  
Bond Strengths ◽  
Post Hoc ◽  
One Way Anova

In this laboratory study shear bond strengths of three filled and one unfilled adhesive systems to enamel and dentine were compared. Forty-eight extracted intact noncarious human mandibular molars were randomly assigned to two groups of 24 one for bonding to enamel and the other for bonding to dentine. Buccal and lingual surfaces of each tooth were randomly assigned for application of each one of filled (Prime & Bond NT (PBNT), Optibond Solo Plus (OBSP), and Clearfil SE Bond (CSEB)) and unfilled (Single Bond (SB)) adhesive systems (n=12). A universal resin composite was placed into the translucent plastic cylinders (3 mm in diameter and 2 mm in length) and seated against the enamel and dentine surfaces and polymerized for 40 seconds. Shear bond strength was determined using a universal testing machine, and the results were statistically analyzed using two-way ANOVA, one-way ANOVA,t-test, and Tukey HSD post hoc test with a 5% level of significance.There were no statistically significant differences in bond strength between the adhesive systems in enamel, but CSEB and SB exhibited significantly higher and lower bond strength to dentine, respectively, than the other tested adhesive systems while there were no statistically significant differences between PBNT and OBSP.

Comparison of the Effect of Hydrogel and a Solution of Sodium Ascorbate on Dentincomposite Bond Strength After Bleaching

2008 ◽  
Vol 9 (2) ◽  
pp. 105-112 ◽  
Author(s):  
Soodabeh Kimyai ◽  
Hadi Valizadeh
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Sodium Ascorbate ◽  
Carbamide Peroxide ◽  
Treatment Groups ◽  
Bleaching Procedure ◽  
Bond Strengths ◽  
Composite Shear ◽  
Group 1

Abstract Aim The aim of this study was to compare the effects of solution and different sodium ascorbate hydrogels on dentin-resin composite shear bond strength subsequent to a bleaching procedure with 10% carbamide peroxide. Methods and Materials Sixty buccal dentin surfaces obtained from intact human third molars were randomly divided into five groups (n=12). Dentin surfaces received different treatments: (1) no treatment; (2) bleaching (10% carbamide peroxide gel); (3) bleaching + 10% sodium ascorbate solution; (4) bleaching + 10% sodium ascorbate hydrogel, and (5) bleaching + 20% sodium ascorbate hydrogel. Dentin surfaces were bonded with Single Bond™ and restored with a composite (Z100). The samples were tested for shear bond strengths. Data was analyzed using analysis of variance (ANOVA) and Tukey tests. Results Significantly higher bond strengths were observed subsequent to treatment with hydrogel and solution forms of sodium ascorbate (p<0.05). No significant differences were demonstrated between different forms of sodium ascorbate preparations. In addition, no significant differences were observed among groups with antioxidant treatment (Groups 3, 4, and 5) and Group 1 (no treatment). Conclusion Reduced bond strength to bleached dentin can be amended by the use of sodium ascorbate as an antioxidant. Clinical Significance Both hydrogel and solution forms of sodium ascorbate can significantly improve the reduced bond strength of resin composite to dentin subsequent to a bleaching procedure with 10% carbamide peroxide. Citation Kimyai S, Valizadeh H. Comparison of the Effect of Hydrogel and a Solution of Sodium Ascorbate on Dentin-composite Bond Strength After Bleaching. J Contemp Dent Pract 2008 February;(9)2:105-112.

scholarly journals Adhesion of Indirect MOD Resin Composite Inlays Luted With Self-adhesive and Self-etching Resin Cements

2012 ◽  
Vol 37 (5) ◽  
pp. 474-484 ◽  
Author(s):  
T Inukai ◽  
T Abe ◽  
Y Ito ◽  
P Pilecki ◽  
RF Wilson ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Resin Cement ◽  
Acid Etching ◽  
Resin Cements ◽  
Significant Difference ◽  
Before And After ◽  
Indirect Composite ◽  
Bond Strengths ◽  
Composite Inlays

SUMMARY This study investigated the effect of loading on the bond strength to dentin and microleakage of MOD indirect composite restorations bonded with self-adhesive and self-etching resin cements with or without acid etching of the proximal enamel margins. Class II MOD cavities were prepared in 48 molar teeth into dentin and divided into three groups of 16 teeth. Impressions were taken and indirect composite inlays fabricated (Estenia C & B). The enamel margins of the proximal boxes of half the specimens were phosphoric acid etched, and the inlays were cemented with one of three cements (Panavia F 2.0, SA Cement, or Rely X Unicem). After luting, eight teeth in each cement group were mechanically loaded at 2.5 cycles/s for 250,000 cycles. Unloaded teeth acted as controls. Teeth were stored in Rhodamine B solution for 24 hours, sectioned buccolingually at the proximal boxes to examine microleakage using confocal microscopy, and further sectioned for μTBS testing of the resin-dentin interface. Analysis of variance was performed to assess the effect of loading and acid etching on microleakage and bond strength. Acid etching had no effect on microleakage. No significant difference in the dentin bond strengths between the three cements existed after loading. Panavia F 2.0 exhibited a significant reduction in bond strength. With regard to microleakage at the proximal boxes, loading had no effect on dye penetration at the cavity floor. However, at the axial walls, loading had a significant deleterious effect on Panavia F 2.0. No difference in microleakage existed between the three cements at both sites before and after loading. In conclusion, the two tested self-adhesive cements exhibited similar bond strengths before and after loading to the self-etching resin cement. Loading reduced dentin bond strengths and increased microleakage at the resin-dentin interface. However, acid etching of the enamel margins had no significant effect on microleakage in the approximal regions of the bonded inlays.

scholarly journals The Durability of Zirconia/Resin Composite Shear Bond Strength using Different Functional Monomer of Universal Adhesives

2021 ◽  
Author(s):  
Awiruth Klaisiri ◽  
Nantawan Krajangta ◽  
Niyom Thamrongananskul
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Functional Monomers ◽  
Composite Interface ◽  
Before And After ◽  
Universal Adhesives ◽  
Bond Strengths ◽  
Composite Shear ◽  
One Way Anova

Abstract Objective This study examined the effectiveness of different functional monomers in universal adhesives on zirconia/resin composite bond strength both before and after thermocycling. Four universal adhesives (G-premio bond universal, GPU; Clearfil Tri-S bond universal, CTB; Optibond Universal, OBU; Tetric N-bond universal; TNU), one adhesive (single bond 2; SB2), and one ceramic primer (Clearfil ceramic primer plus, CCP) were used in this study. Materials and Methods Zirconia discs were prepared and embedded in acrylic. Specimens were polished and sandblasted with alumina. The specimens were randomly divided into two groups (24 hours and the thermocycled), and each group was divided into six subgroups (n = 10), according to zirconia surfaces treatments: no Tx, CCP + SB2, GPU, CTB, OBU, TNU. An Ultradent mold was located on top of the treated zirconia surface. The resin composite was filled into the mold and then light-cured. A universal testing device was used to determine the shear bond strength. Statistical Analysis The data were statistically analyzed using one-way ANOVA and Tukey's test. Results After water storage for 24 hours, the shear bond strengths were GPU > CCP + SB2 = CTB = OBU = TNU > no Tx (p < 0.05). After thermocycling, the shear bond strengths were CCP + SB2 = GPU = CTB = TNU > OBU > no Tx (p < 0.05). Conclusion The universal adhesives containing 10-MDP exhibited the best performance in the shear bond strength of the zirconia/resin composite interface both before and after thermocycling.

Incremental and Bulk-fill Techniques With Bulk-fill Resin Composite in Different Cavity Configurations

2018 ◽  
Vol 43 (6) ◽  
pp. 631-641 ◽  
Author(s):  
S-H Han ◽  
S-H Park
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Weibull Analysis ◽  
Third Molars ◽  
Group Iii ◽  
Group I ◽  
Custom Made ◽  
Wall Compliance ◽  
Bond Strengths ◽  
Group Ii

SUMMARY Purpose: To compare the microtensile bond strengths of incremental and bulk-fill techniques under different C-factor and compliance conditions. Methods and Materials: Extracted human third molars were divided into three experimental groups. For group I, Class I cavities were prepared. For group II, MOD cavities of the same size were prepared. For group III, the cavities were prepared the same way as group II only with high compliance cavity walls. The cavity wall compliance of the specimens was evaluated. Each of these groups was divided into four subgroups. The teeth were restored using two different materials: TB (Tetric N-Ceram Bulk Fill; Ivoclar Vivadent, Hanau, Germany) and VB (Venus Bulk Fill; Heraeus Kulzer, Armonk, NY, USA), and two methods, either an incremental or bulk-fill technique. Then, the microtensile bond strengths (μ-TBSs) were measured and compared. The polymerization stresses of the composites were calculated using a custom-made device. The results were statistically analyzed using the Kruskal-Wallis test and Weibull analysis. Results: In group I, the μ-TBS obtained using the incremental technique was significantly higher than that obtained by the bulk-fill technique (p&lt;0.05). In contrast, no difference of the μ-TBS value was observed between the two techniques in groups II and III. The μ-TBS value of group I was significantly lower than those of groups II and III (p&lt;0.05). No statistical difference in the μ-TBS was observed when the cavities were filled with either TB or VB (p&gt;0.05). Conclusions: The incremental technique showed higher bond strength than did the bulk-fill technique in high C-factor cavities. However, no difference was found between the two techniques in the low C-factor cavities. The bond strength in the high C-factor cavities was significantly lower than that of the low C-factor cavities.

The Effect of Thermocycling on the Adhesion of Self-etching Adhesives on Dental Enamel and Dentin

2007 ◽  
Vol 8 (2) ◽  
pp. 17-24 ◽  
Author(s):  
Alaa Morsy El Araby ◽  
Yousef F. Talic
Keyword(s):  
Bond Strength ◽  
Null Hypothesis ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Dental Enamel ◽  
Single Step ◽  
The Self ◽  
Repeated Measure ◽  
List Type ◽  
Bond Strengths

Abstract Aim The aim of the present study was to investigate the effectiveness of one total-etch self-priming adhesive and two one-step self-etching adhesive systems on the adhesion of a resin composite to both dentin and enamel. The effect of thermocycling on the adhesion was also investigated. The null hypothesis tested was thermocycling would not affect bond strengths to enamel and dentin treated with self-etching adhesives or a total-etch adhesive. Methods and Materials Two single-step self-etching adhesives [Xeno III (XE3) and Prompt L-Pop (PP)] and one two-step total-etch adhesive system (Prime & Bond NT) (P&B NT) were used in this study. Thirty cariesfree unrestored human third molars were used to make specimens of enamel and dentin. Different adhesives were applied on enamel and dentin surfaces according to the manufacturer's instructions then hybrid composite restorative material was condensed on the surface using a mold. The bonded specimens were stored in distilled water at 37°C for 24 hours before being tested. Half of the bonded specimens were tested for shear bond strength without thermocycling. The other half of the test specimens were thermocycled using a thermocycling apparatus in water baths held at 5°C and 55°C with a dwell time of one minute each for 10,000 cycles prior to shear testing. The mean shear bond strength before and after thermocycling was calculated, and the results were subjected to two-way analysis of variance (ANOVA) and repeated measure design to show the interaction between different materials and different times. Results The results showed shear bond strength on both enamel and dentin of the total-etch adhesive and the self-etching adhesives decreased after the specimens were subjected to thermocycling. Conclusions The null hypothesis tested “thermocycling would not affect bond strengths treated with selfetching adhesives” was rejected. Furthermore, the study revealed the following: The shear bond strength to both enamel and dentin of the total-etch adhesive and the self-etching adhesives decreased after the specimens were subjected to thermocycling. XE3 achieved the highest bond strength to both enamel and dentin (26.994±1.17 and 25.22±1.26, respectively). XE3 showed even better bonding after thermocycling to enamel and dentin than the total-etching system or PP. Although PP bonded to enamel showed lower shear bond strength value than XE3, it has durable bond strength even after thermocycling. Citation El Araby AM, Talic YF. The Effect of Thermocycling on the Adhesion of Self-etching Adhesives on Dental Enamel and Dentin. J Contemp Dent Pract 2007 February;(8)2:017-024.

scholarly journals In Vivo and In Vitro Effects of Chlorhexidine Pretreatment on Immediate and Aged Dentin Bond Strengths

2016 ◽  
Vol 41 (3) ◽  
pp. 258-267 ◽  
Author(s):  
Z Gunaydin ◽  
AR Yazici ◽  
ZC Cehreli
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Adhesive System ◽  
Etch And Rinse ◽  
Bonferroni Test ◽  
Bond Strengths ◽  
In Vitro Effects ◽  
Self Etch

SUMMARY This study evaluated the effect of 2% chlorhexidine (CHX) pretreatment of dentin on the immediate and aged microtensile bond strength (μTBS) of different adhesives to dentin in vivo and in vitro. Class I cavities were prepared in 80 caries-free human third molars of 40 patients in a split-mouth fashion. In each tooth pair, one tooth received 2% CHX pretreatment after which both teeth were randomly assigned to one of the following groups with respect to the type of adhesive system applied: Adper Single Bond 2 (etch-and-rinse), Clearfil SE Bond (two-step self-etch), Clearfil S3 Bond (one-step self-etch), and Adper Prompt-L-Pop (all-in-one self-etch). The teeth were restored with resin composite and extracted for μTBS testing either immediately or after six months in function. In vitro specimen pairs were prepared as with the clinical protocol in intact, freshly extracted human molars, and thereafter, subjected to testing immediately or after 5000× thermocycling. Data were analyzed with four-way analysis of variance (ANOVA). Bonferroni test was utilized for pair-wise comparisons. The immediate bond strength values were significantly higher than “aged” ones for all tested adhesives (p=0.00). The in vitro immediate bond strength values were statistically higher than in vivo bond strength values (p&lt;0.05). While the bond strength of in vitro aged, CHX-treated samples were higher than their in vivo counterparts (p&lt;0.05), no difference was observed in non-CHX treated groups (p&gt;0.05). In the absence of CHX pretreatment, all adhesives showed significantly higher immediate bond strength values than CHX-treated groups, while all “aged”, non-pretreated adhesives exhibited significantly lower bond strength values (both p&lt;0.05). By contrast, chlorhexidine pretreatment resulted in significantly higher aged bond strengths, regardless of the adhesive system and testing condition. Aging-associated decline in dentin bond strength of etch-and rinse and self-etch adhesives can be counteracted by chlorhexidine application.

scholarly journals The Bond of Different Post Materials to a Resin Composite Cement and a Resin Composite Core Material

2012 ◽  
Vol 37 (6) ◽  
pp. E38-E49 ◽  
Author(s):  
D Stewardson ◽  
A Shortall ◽  
P Marquis
Keyword(s):  
Bond Strength ◽  
Chemical Interaction ◽  
Resin Composite ◽  
Resin Cement ◽  
Core Material ◽  
Composite Cement ◽  
Grit Blasting ◽  
Bond Strengths ◽  
Push Out ◽  
Resin Composite Cement

SUMMARY Purpose To investigate the bond of endodontic post materials, with and without grit blasting, to a resin composite cement and a core material using push-out bond strength tests. Materials and Methods Fiber-reinforced composite (FRC) posts containing carbon (C) or glass (A) fiber and a steel (S) post were cemented into cylinders of polymerized restorative composite without surface treatment (as controls) and after grit blasting for 8, 16, and 32 seconds. Additional steel post samples were sputter-coated with gold before cementation to prevent chemical interaction with the cement. Cylindrical composite cores were bonded to other samples. After sectioning into discs, bond strengths were determined using push-out testing. Profilometry and electron microscopy were used to assess the effect of grit blasting on surface topography. Results Mean (standard deviation) bond strength values (MPa) for untreated posts to resin cement were 8.41 (2.80) for C, 9.61(1.88) for A, and 19.90 (3.61) for S. Prolonged grit blasting increased bond strength for FRC posts but produced only a minimal increase for S. After 32 seconds, mean values were 20.65 (4.91) for C, 20.41 (2.93) for A, and 22.97 (2.87) for S. Gold-coated steel samples produced the lowest bond strength value, 7.84 (1.40). Mean bond strengths for untreated posts bonded to composite cores were 6.19 (0.95) for C, 13.22 (1.61) for A, and 8.82 (1.18) for S, and after 32 seconds of grit blasting the values were 17.30 (2.02) for C, 26.47 (3.09) for A, and 20.61 (2.67) for S. FRC materials recorded higher roughness values before and after grit blasting than S. With prolonged grit blasting, roughness increased for A and C, but not for S. Conclusions There was no evidence of significant bonding to untreated FRC posts, but significant bonding occurred between untreated steel posts and the resin cement. Increases in the roughness of FRC samples were material dependent and roughening significantly increased bond strength values (p&lt;0.05). Surface roughening of the tested FRC posts is required for effective bonding.

Shear-Bond Strength of a New Self-Adhering Flowable Restorative Material to Dentin of Primary Molars

2013 ◽  
Vol 38 (2) ◽  
pp. 149-154 ◽  
Author(s):  
E Pacifici ◽  
M Chazine ◽  
A Vichi ◽  
S Grandini ◽  
C Goracci ◽  
...  
Keyword(s):  
Bond Strength ◽  
Shear Bond Strength ◽  
Resin Composite ◽  
Primary Molars ◽  
Restorative Material ◽  
Chi Square ◽  
Etch And Rinse ◽  
Bond Strengths ◽  
Vertise Flow ◽  
Wallis Anova

Objective: The aim of this study was to evaluate the shear bond strength to dentin of primary molars of a new self-adhering flowable resin composite with two ionomer-based cements and one flowable resin composite in combination with two different adhesive systems. Study design: Fifty primary molars were grinded on the occlusal surface to obtain flat dentin substrate and randomly divided into 5 groups (n=10): OFL:Phosphoric Acid/Optibond FL/Premise Flow; OAO:Optibond All-In-One/Premise Flowable; II:Polyacrylic Acid/Fuji II; IX:Polyacrylic Acid/Fuji IX; V:Vertise Flow. Cylinders (3mm diameter – 5mm height) of restorative material were built-up in three increments over the dentin surfaces. A shear load was applied until failure. Bond strength values were statistically analysed with Kruskall-Wallis ANOVA followed by Dunn's test (P&lt;.05). Differences in failure mode distribution were assessed with Chi-square (P&lt;.05). Results: OFL and OAO recorded significantly higher bond strengths than the other groups. Adhesive failures were evident in all groups except OFL and OAO, in which also cohesive failures in dentin were observed. Conclusions: Vertise Flow established on primary dentin bond strengths values similar to those of glass ionomer cements routinely used for restorations of primary teeth. The combination of flowable resin with etch-and-rinse or all-in-one adhesives obtained higher bond strength values, thus involving a more complex handling.

Sign in / Sign up

Export Citation Format

Share Document