scholarly journals Shear Bond Strengths and Morphological Evaluation of Filled and Unfilled Adhesive Interfaces to Enamel and Dentine

2012 ◽  
Vol 2012 ◽  
pp. 1-9 ◽  
Author(s):  
Vajihesadat Mortazavi ◽  
Mohammadhosein Fathi ◽  
Ebrahim Ataei ◽  
Niloufar Khodaeian ◽  
Navid Askari

In this laboratory study shear bond strengths of three filled and one unfilled adhesive systems to enamel and dentine were compared. Forty-eight extracted intact noncarious human mandibular molars were randomly assigned to two groups of 24 one for bonding to enamel and the other for bonding to dentine. Buccal and lingual surfaces of each tooth were randomly assigned for application of each one of filled (Prime & Bond NT (PBNT), Optibond Solo Plus (OBSP), and Clearfil SE Bond (CSEB)) and unfilled (Single Bond (SB)) adhesive systems (n=12). A universal resin composite was placed into the translucent plastic cylinders (3 mm in diameter and 2 mm in length) and seated against the enamel and dentine surfaces and polymerized for 40 seconds. Shear bond strength was determined using a universal testing machine, and the results were statistically analyzed using two-way ANOVA, one-way ANOVA,t-test, and Tukey HSD post hoc test with a 5% level of significance.There were no statistically significant differences in bond strength between the adhesive systems in enamel, but CSEB and SB exhibited significantly higher and lower bond strength to dentine, respectively, than the other tested adhesive systems while there were no statistically significant differences between PBNT and OBSP.

Polymers ◽  
2021 ◽  
Vol 13 (6) ◽  
pp. 910
Author(s):  
Syed Rashid Habib ◽  
Salwa Bajunaid ◽  
Abdulrahman Almansour ◽  
Abdulkarim AbuHaimed ◽  
Muqrin Nasser Almuqrin ◽  
...  

The aim of the present study was to investigate the shear bond strength of five different repair methods and adhesive systems for zirconia (Zr) cores layered with feldspathic porcelain. Seventy-five Zr specimens (10 × 10 × 4 mm3) were prepared, sintered, layered with 2 × 10 × 10 mm3 of feldspathic porcelain, and fired. The ceramic was fractured, and the load recorded using a shear-bond test. Specimens were thermocycled and randomly divided into 5 groups (n = 15/group) based on the repair methods. Composite repair blocks with similar dimensions to the layered ceramic (2 × 10 × 10 mm3) were built according to each repair method. Shear bond strength testing of the specimens with composite built up was carried out using a universal testing machine (Instron®5960, Massachusetts, USA). The shear bond strengths of the adhesive interface between repaired composite and the Zr were recorded for all the test groups. The fractured specimens’ surfaces were examined under a scanning electron microscope (Jeol, Musashino, Akishima, Tokyo, Japan) for evaluation of the type of failure and surface characteristics. Shear bond strength of the veneered ceramic bonded to the Zr for all the test groups was non-significant (ANOVA, p = 0.062). Shear bond strength after the repair revealed significant differences (ANOVA, p = 0.002). Group-C (13.79 ± 1.32) and Group-D (9.77 ± 4.77) showed the highest and lowest shear bond strength values, respectively. Paired Sample T-tests showed significantly lower values (p = 0.000) for the repaired (composite) Zr compared to the layered (ceramic) Zr. Multiple comparisons revealed differences (significant) between the shear bond strength of Group-D with Groups A (p = 0.010) and C (p = 0.003, Post Hoc Tukey test). The repair methods tested showed variations in their respective shear bond strengths. Complete ceramic/zirconia repair systems showed better bonding between the repaired composite and Zr core. The mean shear bond strength for the repaired fractured layered Zr showed acceptable outcomes in terms of clinical perspective, but was, however, unpredictable.


2014 ◽  
Vol 2014 ◽  
pp. 1-7 ◽  
Author(s):  
Ahmed Mohammed Hassan ◽  
Ahmed Ali Goda ◽  
Kusai Baroudi

Objective. The aim of this study was to evaluate the effect of different disinfectant agents on bond strength of two types of resin composite materials.Methods. A total of 80 sound posterior teeth were used. They were divided into four groups(n=20)according to the dentin surface pretreatment (no treatment, chlorhexidine gluconate 2%, sodium hypochlorite 4%, and EDTA 19%). Each group was divided into two subgroups according to the type of adhesive (prime and bond 2.1 and Adper easy one). Each subgroup was further divided into two subgroups according to the type of resin composite (TPH spectrum and Tetric EvoCeram). Shear bond strength between dentin and resin composite was measured using Universal Testing Machine. Data collected were statistically analyzed byt-test and one-way ANOVA followed by Tukey’spost hoctest.Results. It was found that dentin treated with EDTA recorded the highest shear bond strength values followed by sodium hypochlorite and then chlorhexidine groups while the control group showed the lowest shear bond strength.Conclusions. The surface treatment of dentin before bonding application has a great effect on shear bond strength between resin composite and dentin surface.


2009 ◽  
Vol 79 (3) ◽  
pp. 564-570 ◽  
Author(s):  
Toshiya Endo ◽  
Rieko Ozoe ◽  
Koichi Shinkai ◽  
Makiko Aoyagi ◽  
Hiroomi Kurokawa ◽  
...  

Abstract Objective: To ascertain the effects of repeated bonding on the shear bond strength of orthodontic brackets bonded with a fluoride-releasing and -recharging adhesive system with a self-etching primer in comparison with two other types of adhesive system. Materials and Methods: A total of 48 premolars were collected and divided equally into three groups of 16. Each group was assigned one of three adhesive systems: Transbond XT, Transbond Plus, or a fluoride-releasing and -recharging adhesive system, Beauty Ortho Bond. Shear bond strength was measured 24 hours after bracket bonding, with the bonding/debonding procedures repeated twice after the first debonding. A universal testing machine was used to determine shear bond strengths, and bracket/adhesive failure modes were evaluated with the adhesive remnant index after each debonding. Results: At every debonding sequence, all of these three adhesive systems had a shear bond strength of 6 MPa, which is a minimum requirement for clinical use. Transbond XT and Transbond Plus had significantly higher mean shear bond strengths than did Beauty Ortho Bond at each debonding. No significant differences in mean bond strength were observed between the three debondings in each adhesive system. Bond failure at the enamel/adhesive interface occurred more frequently in Beauty Ortho Bond than in Transbond XT or Transbond Plus. Conclusions: The fluoride-releasing and -recharging adhesive system with the self-etching primer (Beauty Ortho Bond) had clinically sufficient shear bond strength in repeated bracket bonding; this finding can help orthodontists to decrease the risk of damage to enamel at debonding.


2014 ◽  
Vol 13 (1) ◽  
pp. 7
Author(s):  
Dewi Puspitasari ◽  
Andi Soufyan ◽  
Ellyza Herda

Composite resin is a widely used aesthetic restoration. The restoration can fail due to secondary caries. Chlorhexidinegluconate 2% is used as a cavity disinfectant to eliminate microorganisms on the prepared cavity and to prevent thesecondary caries. The purpose of this study was to analyze the effect of chlorhexidine gluconate 2% to the bondstrength of composite resin with self etch system adhesive on dentine. Sixteen specimens of buccal dentine of premolarscrown are divided into 2 different groups. Group I: Clearfil SE Bond self-etch primer was applied for 20 seconds,Clearfil SE Bond bonding was applied for 5 seconds and polymerized for 10 seconds. Composite resin was constructedincrementally and polymerized for 20 seconds. Group II: prior to self etch primer application as in group I,chlorhexidine gluconate 2% was applied for 15 seconds. Shear bond strength was tested using Testing machine andanalyzed with unpaired T test. The highest shear bond strength was obtained by applying chlorhexidine gluconate 2%.The study concludes that chlorhexidine gluconate 2% application to dentine did not affect significantly to the bondstrength composite resin using self etch adhesive systems.


2021 ◽  
Author(s):  
Ladan Ranjbar Omrani ◽  
Saba Tohidkhah ◽  
Elham Ahmadi ◽  
Mahdi Abbasi ◽  
Reza Morvaridi Farimani

Abstract Background: The aim of the current study was to evaluate and compare the influence of Dycal, Lime-lite, Theracal LC, Biodentine, Resin-modified glass ionomer cement (RMGIC), and Activa Bioactive as the pulp capping material on the shear bond strength of resin composite to dentin.Methods: A total of 70 extracted caries-free molars were randomly assigned to seven groups. Six test groups were covered with various protective liners: Dycal (GD), Theracal LC (GT), lime-lite (GL), Activa Bioactive (GA), Biodentine (GB), RMGIC (GR). The control group (GC)received no liner pretreatment. Each sample was bonded to resin composite using the total-etch tetric N bond adhesive. The samples were then tested for shear bond strength using the universal testing machine at a cross-head speed of 1 mm/min until bond failure occurred. The data were analyzed using the one-way ANOVA test followed by the Tamhane post-hoc test for pairwise comparisons of the groupsResults: Independent of the type of the applied liner, all groups exhibited inferior SBS to dentine compared to the control group. GT and GR showed significantly higher shear bond strength than GB and GD, which showed the lowest shear bond strength. GL and GA also had significantly lower SBS results than GT. The mode of fracture was predominantly cohesive in GD, GB, and GT and adhesive in GA.Conclusion: This present study concludes that the bond strength of resin-composite to dentine can be affected differently using various types of liners.


Author(s):  
Awiruth Klaisiri ◽  
Nantawan Krajangta ◽  
Niyom Thamrongananskul

Abstract Objective This study examined the effectiveness of different functional monomers in universal adhesives on zirconia/resin composite bond strength both before and after thermocycling. Four universal adhesives (G-premio bond universal, GPU; Clearfil Tri-S bond universal, CTB; Optibond Universal, OBU; Tetric N-bond universal; TNU), one adhesive (single bond 2; SB2), and one ceramic primer (Clearfil ceramic primer plus, CCP) were used in this study. Materials and Methods Zirconia discs were prepared and embedded in acrylic. Specimens were polished and sandblasted with alumina. The specimens were randomly divided into two groups (24 hours and the thermocycled), and each group was divided into six subgroups (n = 10), according to zirconia surfaces treatments: no Tx, CCP + SB2, GPU, CTB, OBU, TNU. An Ultradent mold was located on top of the treated zirconia surface. The resin composite was filled into the mold and then light-cured. A universal testing device was used to determine the shear bond strength. Statistical Analysis The data were statistically analyzed using one-way ANOVA and Tukey's test. Results After water storage for 24 hours, the shear bond strengths were GPU > CCP + SB2 = CTB = OBU = TNU > no Tx (p < 0.05). After thermocycling, the shear bond strengths were CCP + SB2 = GPU = CTB = TNU > OBU > no Tx (p < 0.05). Conclusion The universal adhesives containing 10-MDP exhibited the best performance in the shear bond strength of the zirconia/resin composite interface both before and after thermocycling.


Scanning ◽  
2019 ◽  
Vol 2019 ◽  
pp. 1-11
Author(s):  
Fatih Mehmet Korkmaz ◽  
Selin Aycan

Objectives. The aim of this study is to investigate the shear bond strength of an acrylic resin to titanium after different surface treatment methods. Material and Methods. A total of seventy-two disc-shaped specimens (10 mm×10 mm×2 mm) were prepared from titanium alloy. The specimens were randomly allocated to six equal groups: Group S (sandblasting), Group MP (metal primer), Group 10W (fiber laser 10 W), Group 20W (fiber laser 20 W), Group 10WMP (fiber laser 10 W+metal primer), and Group 20WMP (fiber laser 20 W+metal primer). All of the specimens were thermocycled up to 5000 cycles. After thermal cycling, a shear bond strength test was conducted. The shear bond strength data were analyzed with one-way ANOVA and Tukey’s post hoc pairwise comparisons (p<0.05). Results. While the highest values were determined in Group MP, the lowest values were observed in Group S. Additionally, Group MP exhibited significantly higher shear bond strength values than any of the other groups (p<0.05) except Group 10WMP. Similar results were observed between Group MP and Group 10WMP (p>0.05). The groups in which a metal primer was applied (Group MP, 10WMP, and 20WMP) showed significantly higher values than Group S. The shear bond strength values of Group 10W and Group 20W were similar. Conclusions. The application of a metal primer significantly improved the bond strength of acrylic resin to titanium. Fiber laser application may be an alternative method to sandblasting for improving the bond strength of acrylic resin to titanium.


2006 ◽  
Vol 17 (1) ◽  
pp. 39-43 ◽  
Author(s):  
Guilherme Carpena Lopes ◽  
Paula C. Cardoso ◽  
Luiz Clovis Cardoso Vieira ◽  
Luiz N. Baratieri ◽  
Karina Rampinelli ◽  
...  

The aim of this study was to assess the shear bond strength of four acetone-based one-bottle adhesive systems to enamel and dentin, and compare to that of an ethanol-based system used as control. Fifty human molars were bisected mesiodistally and the buccal and lingual surfaces were embedded in acrylic resin using PVC cylinders. The buccal surfaces were ground to obtain flat dentin surfaces, while the lingual surfaces were ground to obtain flat enamel surfaces. All specimens were polished up to 600-grit sandpapers and randomly assigned to 5 groups (n=20; 10 dentin specimens and 10 enamel specimens), according to the adhesive system used: One-Step (Bisco); Gluma One Bond (Heraeus Kulzer); Solobond M (Voco); TenureQuik w/F (Den-Mat) and OptiBond Solo Plus (Kerr) (control). Each adhesive system was applied according to the manufacturers' instructions. The respective proprietary hybrid composite was applied in a gelatin capsule (d=4.3mm) and light-cured for 40 s. The specimens were tested in shear strength with an Instron machine at a crosshead speed of 5 mm/min. Bond strengths means were analyzed statistically by one-way ANOVA and Duncan's post-hoc (p£0.05). Shear bond strength means (MPa) (±SD) to enamel and dentin were: Enamel: One-Step=11.3(±4.9); Gluma One Bond=16.3(±10.1); Solobond M=18.9(±4.5); TenureQuik w/F=18.7(±4.5) and OptiBond Solo Plus=16.4(±3.9); Dentin: One-Step=6.4(±2.8); Gluma One Bond=3.0(±3.4); Solobond M=10.6(±4.9); TenureQuik w/F=7.8(±3.9) and OptiBond Solo Plus=15.1(±8.9). In enamel, the adhesive systems had statistically similar bond strengths to each other (p>0.05). However, the ethanol-based system (OptiBond Solo Plus) showed significantly higher bond strength to dentin than the acetone-based systems (p£0.0001). In conclusion, the solvent type (acetone or ethanol) had no influence on enamel bond strength, but had great influence on dentin bonding, which should be taken into account when choosing the adhesive system.


2014 ◽  
Vol 2014 ◽  
pp. 1-6 ◽  
Author(s):  
Sezin Ozer ◽  
Emine Sen Tunc ◽  
Nihan Gonulol

Objective. To evaluate shear bond strength (SBS) values of a methacrylate (FZ 250) and a silorane-based (FS) resin composite to various underlying materials.Materials and Methods. A total of 80 samples were prepared with four different underlying materials; a flowable (FLC) and a bulk-fill flowable composite (BFC), and a conventional (CGIC) and resin modified glass-ionomer cement (RMGIC). These underlying materials were laminated plus to methacrylate or silorane-based resin composites(n=10). To evaluate the specimens SBS values were evaluated with a universal testing machine (cross-head speed; 1.0 mm/min). Statistical comparisons were carried out using two-way ANOVA and Tukey’s post hoc test with a significance level ofP<0.05.Results. SBS values for FZ250 were significantly higher than for FS for all of the underlying materials tested(P<0.05). SBS values of FZ250 to BFC were significantly higher than to all other materials(P<0.05), whereas SBS values of FS did not vary significantly according to underlying material(P>0.05).Conclusion. The use of FS in conjunction with any of the tested materials showed lower SBS than the FZ 250. Also, new low elastic modulus liner BFC presented slightly good interfacial adhesion so, the usage of BFC as an underlying material may be preferable for FZ 250.


2021 ◽  
Vol 24 (2) ◽  
Author(s):  
Fateme Vasei ◽  
Farahnaz Sharafeddin

Objective: To assess the shear bond strength (SBS) of resin composite to deep dentin, using 1 and 2.5% chitosan pretreatment as well as different adhesive systems. Material and Methods: 80 human maxillary molars were randomly divided to eight groups according to the type of adhesive system and dentin pretreatment (n = 10): I) two-step self-etch system (Clearfil SE bond); II) two-step etch-andrinse system (Adper single bond 2); III) 2.5% chitosan + Clearfil SE bond; IV) 2.5% chitosan +etch + Adper single bond 2; V) etch + 2.5% chitosan + Adper single bond 2; VI) 1% chitosan + Clearfil SE bond; VII) 1% chitosan + etch + Adper single bond 2; VIII) etch + 1% chitosan + Adper single bond 2 (chitosan solution (w/v): 2.5 g and 1 g of chitosan (Sigma Aldrich, USA) was dissolved in 100 ml of 1% acetic acid). Plastic molds were positioned on dentin and filled with composite (Z350, 3M ESPE, USA). SBS (MPa) was tested using a universal testing machine. ANOVA tests, Tukey’s test, and independent t test were used to analyze data (p < 0.05). Results: The highest SBS value among self-etch groups was observed with 1% chitosan (p = 0.001). In the etch-and-rinse group, the SBS of 1% chitosan was significantly lower than the other groups. Chitosan treatment following acid etching led to higher SBS in comparison to when chitosan was applied before etching, with the significant difference in 1% concentration (p = 0.030). A predominance of mix fractures was observed in dentin. Conclusion: Improved dentin bond strength can be achieved through immediate dentin pretreatment with 1% chitosan in self-etch adhesive systems. Chitosan Pretreatment may not be advantageous for etch-and-rinse adhesive systems. Keywords Adhesive system; Chitosan; Deep dentin; Shear strength.


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