RAPID DETERMINATION OF MOISTURE IN GRAIN: III. CALIBRATION AND COMPARISON OF ELECTRICAL MOISTURE METERS WITH VACUUM OVEN FOR AMBER DURUM WHEAT, BARLEY AND OATS
The previous study has been extended to include durum wheat, barley and oats. The hand-operated Tag-Heppenstall meter was found to be unsatisfactory with these grains, as they would not feed into the roller electrodes in a suitable manner. The Burton-Pitt gave erratic results with these grains and it was only possible to calibrate this meter over a limited moisture range, and even over this range it was more inaccurate than the other meters. Qualitatively the calibration curves for these three grains, in the Limbrick and motor Tag-Heppenstall, were similar to those previously obtained with hard red spring wheat. The actual resistance and the slope of the curves were, however, somewhat different for the different grains. The standard error of prediction shows that the motor-operated Tag-Heppenstall was the most accurate meter for use with durum wheat and barley, while the Limbrick was superior with oats. With the limited number of samples available it was impossible to detect any significant difference between the temperature coefficients, in any particular meter, of the different grains. When converted to a moisture basis the correction factors were practically the same as for hard red spring wheat.The results from the entire investigation show that the Brown-Duvel method is more accurate than the 130 °C. air oven method with all grains studied. The motor-operated Tag-Heppenstall meter is as accurate as the Brown-Duvel with hard red spring wheat, over the moisture range 11.0 to 17.0%, and is superior to the air oven method over this limited range. Otherwise the rapid analytical methods are more accurate than any of the moisture meters tested with any of the grains. The meters fall in the following order of decreasing accuracy over the moisture range 11.0 to 17.0%:–with hard red spring wheat; motor Tag-Heppenstall, Limbrick, hand Tag-Heppenstall, Burton-Pitt and Davies: with durum wheat and barley; motor Tag-Heppenstall, Limbrick and Burton-Pitt: and with oats; Limbrick, Burton-Pitt and motor Tag-Heppenstall. Where a meter is not mentioned no tests were made, the instrument having been omitted because it gave no promise of practical utility.