Manufacturing of roughness standard samples based on ACF/PSD model programming

2018 ◽  
Author(s):  
Jérôme Reche ◽  
Maxime Besacier ◽  
Patrice Gergaud ◽  
Yoann Blancquaert
Keyword(s):  
Standard Samples

Reliability of MTurk Data From Masters and Workers

2020 ◽  
Vol 41 (1) ◽  
pp. 30-36
Author(s):  
Steven V. Rouse
Keyword(s):  
Cognitive Abilities ◽  
Online Survey ◽  
Quality Data ◽  
Standard Samples ◽  
Online Data ◽  
Approval Ratings ◽  
Cognitive Abilities Test ◽  
Elite Status ◽  
Master Status ◽  
Amazon's Mechanical Turk

Abstract. Previous research has supported the use of Amazon’s Mechanical Turk (MTurk) for online data collection in individual differences research. Although MTurk Masters have reached an elite status because of strong approval ratings on previous tasks (and therefore gain higher payment for their work) no research has empirically examined whether researchers actually obtain higher quality data when they require that their MTurk Workers have Master status. In two different online survey studies (one using a personality test and one using a cognitive abilities test), the psychometric reliability of MTurk data was compared between a sample that required a Master qualification type and a sample that placed no status-level qualification requirement. In both studies, the Master samples failed to outperform the standard samples.

Silicate analysis of carbonated rocks using ICP-AES with calibration by the concentration ratio

2020 ◽  
Vol 86 (5) ◽  
pp. 16-21
Author(s):  
T. A. Karimova ◽  
G. L. Buchbinder ◽  
S. V. Kachin
Keyword(s):  
Inductively Coupled Plasma ◽  
Concentration Ratio ◽  
Total Error ◽  
Atomic Emission ◽  
Emission Spectrometry ◽  
Calibration Error ◽  
Plasma Atomic Emission Spectrometry ◽  
Standard Samples ◽  
Inductively Coupled ◽  
Carbonate Materials

Calibration by the concentration ratio provides better metrological characteristics compared to other calibration modes when using the inductively coupled plasma atomic emission spectrometry (ICP-AES) for analysis of geological samples and technical materials on their base. The main reasons for the observed improvement are: i) elimination of the calibration error of measuring vessels and the error of weighing samples of the analyzed materials from the total error of the analysis; ii) high intensity of the lines of base element; and iii) higher accuracy of measuring the ratio of intensities compared to that of measuring the absolute intensities. Calcium oxide is better suited as a base when using calibration by the concentration ratio in analysis of carbonate rocks, technical materials, slags containing less than 20% SiO2 and more than 20% CaO. An equation is derived to calculate the content of components determined in carbonate materials when using calibration by the concentration ratio. A method of ICP-AES with calibration by the concentration ratio is developed for determination of CaO (in the range of contents 20 – 100%), SiO2 (2.0 – 35%), Al2O3 (0.1 – 30%), MgO (0.1 – 20%), Fe2O3 (0.5 – 40%), Na2O (0.1 – 15%), K2O (0.1 – 5%), P2O5 (0.001 – 2%), MnO (0.01 – 2%), TiO2 (0.01 – 2.0%) in various carbonate materials. Acid decomposition of the samples in closed vessels heated in a HotBlock 200 system is proposed. Correctness of the procedure is confirmed in analysis of standard samples of rocks. The developed procedure was used during the interlaboratory analysis of the standard sample of slag SH17 produced by ZAO ISO (Yekaterinburg, Russia).

Dc arc emission analysis of rare earth metals and their oxides with sorption preconcentration of impurities

2018 ◽  
Vol 84 (11) ◽  
pp. 9-14
Author(s):  
E. S. Koshel ◽  
V. B. Baranovskaya ◽  
M. S. Doronina
Keyword(s):  
Rare Earth ◽  
Rare Earth Metals ◽  
Analytical Signal ◽  
Graphite Powder ◽  
Atomic Emission ◽  
Standard Samples ◽  
Emission Analysis ◽  
Sorption Preconcentration ◽  
Sample Shape

The analytical capabilities of arc atomic emission determination of As, Bi, Sb, Cu, Te in rare earth metals (REM) and their oxides after preparatory group concentration using S,N-containing heterochain polymer sorbent are studied on a high-resolution spectrometer “Grand- Extra” (“WMC-Optoelectron-ics” company, Russia). Sorption kinetics and dependence of the degree of the impurity extraction on the solution acidity are analyzed to specify conditions of sorption concentration. To optimize the procedure of arc atomic emission determination of As, Bi, Sb, Cu, and Te various schemes of their sorption preconcentration and subsequent processing of the resulted concentrate with the addition of a collector at different stages of the sorption process have been considered. Graphite powder is used as a collector in analysis of rare earth oxides due to universality and relative simplicity of the emission spectrum. Conditions of analysis and parameters of the spectrometer that affect the analytical signal (mass and composition of the sample, shape and size of the electrodes, current intensity and generator operation mode, interelectrode spacing, wavelengths of the analytical lines) are chosen. The evaporation curves of the determinable impurities were studied and the exposure time of As, Bi, Sb, Cu, and Te in the resulted sorption concentrate was determined. Correctness of the obtained results was evaluated using standard samples of the composition and in comparisons between methods. The results of the study are used to develop a method of arc chemical-atomic emission analysis of yttrium, gadolinium, neodymium, europium, scandium and their oxides in a concentration range of n x (10-2 - 10-5) wt.%.

Sorption of Se (IV) from aqueous solutions with subsequent determination by X-ray fluorescence analysis

2020 ◽  
Vol 86 (10) ◽  
pp. 5-9
Author(s):  
D. G. Filatova ◽  
A. A. Arkhipenko ◽  
M. A. Statkus ◽  
V. V. Es’kina ◽  
V. B. Baranovskaya ◽  
...  
Keyword(s):  
Inductively Coupled Plasma ◽  
Fluorescence Analysis ◽  
Standard Samples ◽  
Phase Contact Time ◽  
Sorbent Phase ◽  
X Ray ◽  
Fundamental Parameters ◽  
Inductively Coupled ◽  
Subsequent Determination

An approach to sorptive separation of Se (IV) from solutions on a novel S,N-containing sorbent with subsequent determination of the analyte in the sorbent phase by micro-x-ray fluorescence method is presented. The sorbent copolymethylenesulfide-N-alkyl-methylenamine (CMA) was synthesized using «snake in the cage» procedure and proven to be stable in acid solutions. Conditions for quantitative extraction of Se (IV) were determined: sorption in 5 M HCl or 0.05 M HNO3 solutions when heated to 60°C, phase contact time being 1 h. The residual selenium content in the solution was determined by inductively coupled plasma mass spectrometry (ICP-MS) using 82Se isotope. The absence of selenium losses is proved and the mechanism of sorption interaction under specified conditions is proposed. The method of micro-x-ray fluorescence analysis (micro-RFA) with mapping revealed a uniform distribution of selenium on the sorbent surface. The possibility of determining selenium in the sorbent phase by micro-RFA is shown. When comparing the obtained results with the results of calculations by the method of fundamental parameters, it is shown the necessity of using standard samples of sorbates to obtain correct results of RFA determination of selenium in the sorbent phase.

scholarly journals Apparatus for routine measurements of the thermal conductivity of ice cores

1999 ◽  
Vol 29 ◽  
pp. 151-154 ◽  
Author(s):  
Crescenzo Festa ◽  
Aristide Rossi
Keyword(s):  
Thermal Conductivity ◽  
Ice Cores ◽  
Maximum Temperature ◽  
Transient Hot Wire ◽  
Hot Wire ◽  
Standard Samples ◽  
Experimental Conditions ◽  
Heating Source ◽  
Central Segment ◽  
Wire Method

AbstractAn apparatus is described for measuring the thermal conductivity of ice by the transient hot-wire method. Thermal conductivity A, is determined by tracking the thermal pulse induced in the sample by a heating source consisting of a platinum resistor. A central segment of the same platinum heating resistor acts also as a thermal sensor. A heat pulse transferred to the ice for a period of 40s gives a maximum temperature increment of about 7-14°C. In good experimental conditions, the expected reproducibility of the measurements is within ±3%. The accuracy of the method depends on whether the instrument has been calibrated by reliable standard samples, certified by absolute methods.

Collaborative Study of a Titrimetric Method for the Assay of Amitrole Formulations

1967 ◽  
Vol 50 (3) ◽  
pp. 568-572
Author(s):  
J Russell Bishop
Keyword(s):  
Collaborative Study ◽  
Statistical Analyses ◽  
Standard Samples ◽  
Titrimetric Method ◽  
Inflection Points ◽  
Good Agreement

Abstract titrimetric method for the assay of dry and liquid amitrole formulations was studied by 10 collaborators. In the method, acid is added to the prepared amitrole sample, the solution is titrated potentiometrically with standard alkali, and the amitrole content is measured as the amount of alkali consumed between the first and second inflection points. Collaborative results on standard samples of a dry 90% formulation, a dry 50% formulation, and a liquid 2 lb/gallon formulation showed good agreement between samples and laboratories. Statistical analyses of the results were satisfactory, and the method for the assay of amitrole formulations is recommended for adoption as official, first action

Comparison of visual (MUNSELL) and instrumental measures (CIELAB) of coloured textile standard samples

2019 ◽  
Vol 23 (4) ◽  
pp. 340-354
Author(s):  
Asim Kumar Roy Choudhury ◽  
Biswajit Naskar
Keyword(s):  
Correlation Coefficient ◽  
Design Methodology ◽  
Correlation Coefficients ◽  
Standard Samples ◽  
Content Type ◽  
Psychophysical Data ◽  
Physical Data ◽  
Hue Angle ◽  
Munsell Scale

Purpose This paper aims to compare visual (Munsell) and instrumental (CIELAB) attributes of SCOTDIC colour standards. Design/methodology/approach SCOTDIC cotton and polyester standards of defined hue, value and chroma were subjected to spectrophotometric assessment for finding the corresponding instrumental parameters. The visual and instrumental parameters were compared. Findings The correlation between SCOTDIC value and CIELAB lightness is quite high. Correlation coefficient between SCOTDIC hue and CIELAB hue angle and the correlation between SCOTDIC chroma and CIELAB chroma were only moderate because the CIELAB chroma varied widely at higher chroma. When the standards of SCOTDIC hues having erratic hue angles at two extremes are excluded, the Correlation coefficients between SCOTDIC hue and CIELAB hue angle become high. Research limitations/implications The psychophysical data (visual) are difficult to match with physical data (instrumental). Originality/value The object of the present research is to study and compare visual (Munsell) and instrumental (CIELAB) colorimetric parameters. Munsell scale is physically exemplified by SCOTDIC fabric samples available in two sets, namely, cotton and polyester sets.

Mechanical Behaviour of CoCrMo Alloy with Si Content

2015 ◽  
Vol 754-755 ◽  
pp. 1017-1022 ◽  
Author(s):  
Petrică Vizureanu ◽  
Mirabela Georgiana Minciună ◽  
Dragoş Cristian Achiţei ◽  
Andrei Victor Sandu ◽  
Kamarudin Hussin
Keyword(s):  
Tensile Strength ◽  
Chemical Composition ◽  
Testing Machine ◽  
Base Material ◽  
Optical Emission ◽  
Experimental Tests ◽  
Optical Emission Spectrometry ◽  
Emission Spectrometry ◽  
Standard Samples

.The paper present aspects about the obtaining of non-precious dental alloys (type CoCrMo and CoCrMoSi7), the determination of chemical composition by optical emission spectrometry and the experimental tests for determining the tensile strength, made on standard plate samples. The base material used in experiments was a commercial alloy, from CoCrMo system, which belongs to the class of dental non-precious alloys, intended to medical applications. The obtaining of studied alloy was made on arc re-melting installation, under vacuum, type MRF ABJ 900. The process followed to realize a rapid melting, with a maximum admissible current intensity. The samples for tests were obtained by casting in an electric arc furnace, under vacuum, in optimal conditions for melting and solidification and processing by electro-erosion, to eliminate all the disturbing factors which come by processing conditions for the samples. The determination of chemical composition for cobalt based alloys, by optical emission spectrometry, was made on SpectromaxX equipment with spark. The electrical discharge is made with the elimination of an energy quantity, fact which determine plasma forming and light issue. Tensile tests for standard samples, made from cobalt based alloy, was made on Instron 3382 testing machine, and assisted by computer. The obtained results are: elongation, elasticity modulus, tensile strength and offer complete information about the analyzed mechanical properties. For the certitude of obtained experimental results, the tests were made on samples with specific dimensions according ISO 6892-1:2009(E) standard, both for the tensile strength, and also machine operation.

Preparation and Mechanical Properties of Polyethylene-Portland Cement Composites

2009 ◽  
Vol 1242 ◽  
Author(s):  
Rivas-Vázquez L.P. ◽  
Suárez-Orduña R. ◽  
Valera-Zaragoza M. ◽  
Máas-Díaz A. De la L. ◽  
Ramírez-Vargas E.
Keyword(s):  
Mechanical Properties ◽  
Compressive Strength ◽  
Portland Cement ◽  
Plastic Waste ◽  
Cement Composites ◽  
Compression Tests ◽  
Standard Samples ◽  
Cement Ratio ◽  
Reinforcing Fibers ◽  
Waste Polyethylene

ABSTRACTThe effects of waste polyethylene aggregate as admixture agent in Portland cement at different addition polyethylene/cement ratios from 0.0156 to 0.3903 were investigated. The reinforced samples were prepared according the ASTM C 150 Standard (samples of 5 × 5 × 5 cm). The reinforcing fibers were milling at a size of 1/25 in diameter, form waste and used them to evaluate the effects in mechanical properties in cement-based composites. The evaluation of polyethylene as additive was based on results of density and compression tests. The 28-day compressive strength of cement reforced with plastic waste at a replacement polyethylene/cement ratio of 0.0468 was 23.5 MPa compared to the control concrete (7.5 MPa). The density of cement replaced with polyethylene varies from 2.114 (0% polyethylene) to 1.83 g/cm3 by the influence of polyethylene.

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