Production of rotary jet spun ultrathin fibers of poly-butylene adipate-co-terephthalate (PBAT) filled with nanocomposites

Author(s):  
Ana Maria do Espirito Santo ◽  
Patricia Oliveira de Andrade ◽  
Maíra Maftoum Costa ◽  
Anderson de Oliveira Lobo
Keyword(s):  
2018 ◽  
Vol 29 (5) ◽  
pp. 1435-1446 ◽  
Author(s):  
Petronela Pascariu Dorneanu ◽  
Corneliu Cojocaru ◽  
Petrisor Samoila ◽  
Niculae Olaru ◽  
Anton Airinei ◽  
...  

2021 ◽  
Vol 04 ◽  
Author(s):  
Anna L.M.M. Toledo ◽  
Talita N. da Silva ◽  
Arianne C. dos S. Vaucher ◽  
Arthur H. V. Miranda ◽  
Gabriela C. C. Silva de Miranda ◽  
...  

Background: The demand for novel biomaterials has been exponentially rising in the last years as well as the searching for new technologies able to produce more efficient products in both drug delivery systems and regenerative medicine. Objective: The technique that can pretty well encompass the needs for novel and high-end materials with a relatively low-cost and easy operation is the electrospinning of polymer solutions. Methods: Electrospinning usually produces ultrathin fibers that can be applied in a myriad of biomedical devices including sustained delivery systems for drugs, proteins, biomolecules, hormones, etc that can be applied in a broad spectrum of applications, from transdermal patches to cancer-related drugs. Results: Electrospun fibers can be produced to mimic certain tissues of the human body, being an option to create new scaffolds for implants with several advantages. Conclusions: In this review, we aimed to encompass the use of electrospun fibers in the field of biomedical devices, more specifically in the use of electrospun nanofibers applications toward the production of drug delivery systems and scaffolds for tissue regeneration.


Nanomaterials ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 144 ◽  
Author(s):  
Kelly J. Figueroa-Lopez ◽  
António A. Vicente ◽  
Maria A.M. Reis ◽  
Sergio Torres-Giner ◽  
Jose M. Lagaron

In this research, the antibacterial and antioxidant properties of oregano essential oil (OEO), rosemary extract (RE), and green tea extract (GTE) were evaluated. These active substances were encapsulated into ultrathin fibers of poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) derived from fruit waste using solution electrospinning, and the resultant electrospun mats were annealed to produce continuous films. The incorporation of the active substances resulted in PHBV films with a relatively high contact transparency, but it also induced a slightly yellow appearance and increased the films opacity. Whereas OEO significantly reduced the onset of thermal degradation of PHBV, both the RE and GTE-containing PHBV films showed a thermal stability profile that was similar to the neat PHBV film. In any case, all the active PHBV films were stable up to approximately 200 °C. The incorporation of the active substances also resulted in a significant decrease in hydrophobicity. The antimicrobial and antioxidant activity of the films were finally evaluated in both open and closed systems for up to 15 days in order to anticipate the real packaging conditions. The results showed that the electrospun OEO-containing PHBV films presented the highest antimicrobial activity against two strains of food-borne bacteria, as well as the most significant antioxidant performance, ascribed to the films high content in carvacrol and thymol. Therefore, the PHBV films developed in this study presented high antimicrobial and antioxidant properties, and they can be applied as active layers to prolong the shelf life of the foods in biopackaging applications.


2009 ◽  
Vol 113 (17) ◽  
pp. 5837-5842 ◽  
Author(s):  
Youliang Hong ◽  
Hongsong Fan ◽  
Xingdong Zhang

2017 ◽  
Vol 59 (3) ◽  
pp. 342-351 ◽  
Author(s):  
S. G. Karpova ◽  
A. A. Ol’khov ◽  
N. G. Shilkina ◽  
P. M. Tyubaeva ◽  
A. A. Popov ◽  
...  

2019 ◽  
Vol 9 (23) ◽  
pp. 5136 ◽  
Author(s):  
Busra Akinalan Balik ◽  
Sanem Argin ◽  
Jose M. Lagaron ◽  
Sergio Torres-Giner

Pectin was first dissolved in distilled water and blended with low contents of polyethylene oxide 2000 (PEO2000) as the carrier polymer to produce electrospun fibers. The electrospinning of the water solution of pectin at 9.5 wt% containing 0.5 wt% PEO2000 was selected as it successfully resulted in continuous and non-defected ultrathin fibers with the highest pectin content. However, annealing of the resultant pectin-based fibers, tested at different conditions, developed films with low mechanical integrity, high porosity, and also dark color due to their poor thermal stability. Then, to improve the film-forming process of the electrospun mats, two plasticizers, namely glycerol and polyethylene glycol 900 (PEG900), were added to the selected pectin solution in the 2–3 wt% range. The optimal annealing conditions were found at 150 °C with a pressure of 12 kN load for 1 min when applied to the electrospun pectin mats containing 5 wt% PEO2000 and 30 wt% glycerol and washed previously with dichloromethane. This process led to completely homogenous films with low porosity and high transparency due to a phenomenon of fibers coalescence. Finally, the selected electrospun pectin-based film was applied as an interlayer between two external layers of poly(3-hydroxybutyrate-co-3-hydroxyvalerate) (PHBV) by the electrospinning coating technology and the whole structure was annealed to produce a fully bio-based and biodegradable multilayer film with enhanced barrier performance to water vapor and limonene.


Nanomaterials ◽  
2018 ◽  
Vol 8 (4) ◽  
pp. 199 ◽  
Author(s):  
Kelly Figueroa-Lopez ◽  
Jinneth Castro-Mayorga ◽  
Margarita Andrade-Mahecha ◽  
Luis Cabedo ◽  
Jose Lagaron

2019 ◽  
Vol 13 (2) ◽  
pp. 313-327
Author(s):  
S. G. Karpova ◽  
A. A. Ol’khov ◽  
P. M. Tyubaeva ◽  
N. G. Shilkina ◽  
A. A. Popov ◽  
...  

RSC Advances ◽  
2016 ◽  
Vol 6 (35) ◽  
pp. 29423-29427 ◽  
Author(s):  
Hong-Wei He ◽  
Le Wang ◽  
Xu Yan ◽  
Li-Hua Zhang ◽  
Miao Yu ◽  
...  

Solvent-free electrospinning UV curable materials into ultrathin fibers under UV light radiation and in atmosphere of N2or air.


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