Material Characterization of Pipeline Steels: Inspection Techniques Review and Potential Property Relationships

Author(s):  
Lucinda J. Smart ◽  
Brady J. Engle ◽  
Leonard J. Bond ◽  
John MacKenzie ◽  
Greg Morris

The oil and gas industry in North America operates an aging infrastructure of pipelines, 70% of which were installed prior to 1980 and almost half of which were installed during the 1950s and 1960s. There is growing interest in having knowledge of pipe properties so that a safe operating pressure can be determined, yet there are a significant number of cases where records are incomplete. Current in-line inspection (ILI) technologies focus on defect detection and characterization, such as corrosion, cracking, and the achieved probability of detection (POD). As a part of the process in assessing defect significance it is necessary to know the pipe properties, so as to determine potential failure limits. The mechanical properties (yield strength, tensile strength and fracture toughness) of steel pipe must be known or conservatively estimated in order to safely respond to the presence of detected defects in an appropriate manner and to set the operating pressure. Material property measurements such as hardness, chemical content, grain size, and microstructure can likely be used to estimate the mechanical properties of steel pipe without requiring cut-outs to be taken from pipes for destructive tests. There are in-ditch methods of inspection available or being developed that can potentially be used to determine many of the material characteristics and at least some mechanical properties. Furthermore, there is also potential ILI data to be used for obtaining some information. Advances in ILI technologies for this purpose are currently being explored by several interested parties. ILI companies are specifically focusing on relating magnetic measurements from eddy current and magnetic flux leakage measurements to mechanical properties. ILI also regularly uses ultrasound measurements for wall thickness determination. Potential application of advances in ultrasound measurements for grain size and other properties are being explored. However, nondestructive methods of inspection in common use today usually do not enable determination of either the material or mechanical properties, leaving the only alternative to be destructive testing. This is costly, time-consuming, and often not practical for pipe that is in-service. ILI and in-situ techniques are reviewed in this paper and provide an analysis of a sample set of data is presented. The paper explores the possibility of obtaining mechanical property data from data potentially measurable by ILI and in-situ measurements. Ideally, results would allow mechanical property measurements desired to assess pipelines so as to ensure that at a specific operating pressure there is the proper response to anomalies that might pose a significant threat. The use of a multivariate regression analysis showed better results than the traditional two-variable regression plots, and may be key to determining which properties are necessary to provide the best results for reliably estimating the mechanical properties of pipe. However, there is still much work to done in understand and account for the many sources of variability within the pipe material, and how that relates to the resultant relationships between the mechanical and material properties.

2021 ◽  
Author(s):  
Meng Meng ◽  
Luke Frash ◽  
James Carey ◽  
Wenfeng Li ◽  
Nathan Welch ◽  
...  

Abstract Accurate characterization of oilwell cement mechanical properties is a prerequisite for maintaining long-term wellbore integrity. The drawback of the most widely used technique is unable to measure the mechanical property under in situ curing environment. We developed a high pressure and high temperature vessel that can hydrate cement under downhole conditions and directly measure its elastic modulus and Poisson's ratio at any interested time point without cooling or depressurization. The equipment has been validated by using water and a reasonable bulk modulus of 2.37 GPa was captured. Neat Class G cement was hydrated in this equipment for seven days under axial stress of 40 MPa, and an in situ measurement in the elastic range shows elastic modulus of 37.3 GPa and Poisson's ratio of 0.15. After that, the specimen was taken out from the vessel, and setted up in the triaxial compression platform. Under a similar confining pressure condition, elastic modulus was 23.6 GPa and Possion's ratio was 0.26. We also measured the properties of cement with the same batch of the slurry but cured under ambient conditions. The elastic modulus was 1.63 GPa, and Poisson's ratio was 0.085. Therefore, we found that the curing condition is significant to cement mechanical property, and the traditional cooling or depressurization method could provide mechanical properties that were quite different (50% difference) from the in situ measurement.


2021 ◽  
Vol 1035 ◽  
pp. 102-107
Author(s):  
Shao Ming Ma ◽  
Chuan Liu Wang ◽  
Yun Lin Fan

Light-weight and high-strength aluminum alloy drill pipes are potential and promising to replace traditional steel drill pipes. In this study, the grain size and mechanical properties of aluminum alloy drilling pipe materials reinforced by in-situ TiB2 particles were studied. The results showed when reinforced by in-situ TiB2 particles the grain size of aluminum alloy materials was refined from 155 m to 57 m and ultimate tensile strength was increased from 590 MPa to 720 MPa. Besides, the results also indicated that the friction coefficient was reduced from 0.99 to 0.50 and thus the abrasion resistance of 7075 aluminum alloy was enhanced by 34 %. This study provided theoretical basis for the application of light-weight and high-strength aluminum alloy drill pipes in directional drilling and ultra-deep wells.


2021 ◽  
Author(s):  
Christian Kerschbaummayr ◽  
Martin Ryzy ◽  
Bernhard Reitinger ◽  
Mike Hettich ◽  
Jan Džugan ◽  
...  

Abstract The macroscopic mechanical properties like yield-strength, ductility or hardness play an important role during the steel production and the design of new steel grades. The austenite grain size is an important parameter, which influences the final microstructure and the properties of a material. When developing grain growth evolution models, typically many samples have to be treated thermally and micrographs have to be prepared ex-situ. To reduce the time expenditure of this procedure we carried out in-situ laser ultrasound measurements of austenitic grain growth in plain carbon steel (AISI 1045). A thermomechanical simulator of the type Linseis L78/RITA has been upgraded with a laser ultrasound measurement system, which enables the continuous and contactless determination of the austenite mean grain size during a thermal cycle. In this work we will show the calibration workflow and grain size results by a new attenuation model for plain carbon steel. In-situ laser ultrasound measurement data is compared with several micrographs defined at supporting points along a specified temperature program to corroborate the findings.


Metals ◽  
2020 ◽  
Vol 10 (5) ◽  
pp. 629
Author(s):  
Anagh Deshpande ◽  
Subrata Deb Nath ◽  
Sundar Atre ◽  
Keng Hsu

Selective laser melting (SLM) is one of the most widely used additive manufacturing technologies. Fabricating nickel-based superalloys with SLM has garnered significant interest from the industry and the research community alike due to the excellent high temperature properties and thermal stability exhibited by the alloys. Haynes-282 alloy, a γ′-phase strengthened Ni-based superalloy, has shown good high temperature mechanical properties comparable to alloys like R-41, Waspaloy, and 263 alloy but with better fabricability. A study and comparison of the effect of different heat-treatment routes on microstructure and mechanical property evolution of Haynes-282 fabricated with SLM is lacking in the literature. Hence, in this manuscript, a thorough investigation of microstructure and mechanical properties after a three-step heat treatment and hot isostatic pressing (HIP) has been conducted. In-situ heat-treatment experiments were conducted in a transmission electron microscopy (TEM) to study γ′ precipitate evolution. γ′ precipitation was found to start at 950 °C during in-situ heat-treatment. Insights from the in-situ heat-treatment were used to decide the aging heat-treatment for the alloy. The three-step heat-treatment was found to increase yield strength (YS) and ultimate tensile strength (UTS). HIP process enabled γ′ precipitation and recrystallization of grains of the as-printed samples in one single step.


Author(s):  
Zheng-Yang Hu ◽  
Hai-Chun Peng ◽  
Zhao-Hui Zhang ◽  
Peng Song ◽  
Ming Chen ◽  
...  

Abstract A hybrid of TiB whiskers and TiC particles reinforced TC4 matrix composites were in-situ synthesized by spark plasma sintering (SPS) using a TC4-0.6wt.% B4C powder mixture at temperatures range from 550°C to 1150°C. The effect of sintering temperature on microstructure, grain size, mechanical properties and densification process of the (TiB+TiC)/ TC4 matrix composites were investigated. The composite sintered at 1050℃ has the highest tensile strength (1129.0 MPa), yield strength (1077.8MPa) and plasticity (7.1%). The aspect ratio of TiB whiskers increases almost linearly below 1050°C and its highest value is 33.2. The grain size of TiC increases with the increase of sintering temperature, and rapid growth occurs in the range of 850°C to 950°C. The composite sintered body appears four shrinkage stages before applying sintering pressure. The corresponding peak temperatures are 663℃, 758℃, 840℃ and 994℃, respectively.


2021 ◽  
Vol 902 ◽  
pp. 81-86
Author(s):  
Shu Mao Zhao ◽  
Ling Ran Zhao

In this study, B4C-TiB2 ceramic composites were manufactured by hot pressing method. The raw materials for the in-situ synthesis of TiB2 were TiO2 and TiC. After being sintered at 1900°C for 60min under a pressure of 30MPa, compact composites samples with a TiB2 volume fraction range from 0 to 11.05% were prepared. The relative density, fracture toughness and flexural strength of different sample were tested. Microstructures on the fracture surface were studied by SEM. The result shows that B4C-TiB2 ceramic composites sintered from B4C-TiC had a better mechanical property than the one sintered from B4C-TiO2. When the content of TiB2 (reacted from TiC) was 11.05vol.%, the strength and toughness of B4C-TiB2 ceramics can reach 598MPa and 6.45MPa·m1/2. The toughening mechanisms of B4C-TiB2 composites include micro-crack toughening and energy consumption by the pulling out process of second phase.


2011 ◽  
Vol 233-235 ◽  
pp. 1830-1833 ◽  
Author(s):  
Yong Chen ◽  
Hui Xu ◽  
Tao Sun

The PMMA/TiO2 nanocomposites were prepared by in situ polymerization,the dissolution, thermal stability and the mechanical property of the nanocomposites were studied. The results indicated that nano-TiO2 may be crosslinking points in the matrix and the thermal stability of the nanocomposites became higher. As the content of nano-TiO2 increased, the mechanical properties of the nanocomposites had great changes.


2005 ◽  
Author(s):  
Bruce S. Kang ◽  
Chuanyu Feng

Since Tabor showed the application of spherical indentation approach to obtain material post-yielding true stress-strain curves, the indentation technique has been investigated to determine mechanical properties besides hardness measurement. Accurate measurement of indentation parameters is critical in the determination of surface mechanical properties using indentation method. In this research, an in-situ optical Transparent Indenter Measurement (TIM) method was developed for material inspection and mechanical property measurement. Using spherical indentation, residual surface deformation after spherical indentations was first investigated on IN783 superalloy samples using phase-shifting Twyman-Green and moire´ interferometry. The elastic-plastic boundary was identified based on the characteristic of the out-of-plane deformation fringe patterns. Then using the measured in-plane deformation, yield strength of the tested material was obtained. Using the TIM system, real-time in-situ measurement of indentation-induced out-of-plane deformation and contact radius were directly measured during an indentation process. Coupled with elastic recovery theories and 2D finite element analyses, a procedure was developed to determine the material stress-strain curve. It is also demonstrated that the TIM method is suitable for debonding inspection of thin film materials.


2018 ◽  
Vol 25 (3) ◽  
pp. 453-462 ◽  
Author(s):  
Hongying Li ◽  
Shouxin Zhao ◽  
Yangxun Ou ◽  
Yongqiu Lai

Abstract In situ TiB2/Al-4.5Cu composites with different TiB2 particle amounts were fabricated by the salt-metal reaction technique. The effects of in situ TiB2 on the microstructure and mechanical properties of Al-4.5Cu alloy were studied in this paper. The results showed that in situ TiB2 particles had significant effect on refining grain size and improving mechanical properties of as-cast Al-4.5Cu alloy. With the amounts of TiB2 particles increasing, the yield strength and ultimate tensile strength were improved, while the elongation reduced. The strengthening mechanisms of the in situ particle-reinforcing Al matrix composites were discussed, and the yield strength was predicted accurately by accounting for the three strengthening mechanisms and particle distribution.


2018 ◽  
Vol 2018 ◽  
pp. 1-7
Author(s):  
Jianchun Sun ◽  
Yilong Ma ◽  
Hongwei Miao ◽  
Kejian Li ◽  
Chunhong Li ◽  
...  

Quasicrystal-strengthened Mg-Zn-RE (RE = rare-earth element) alloys have been investigated extensively due to their excellent mechanical properties. Here, we prepare quasicrystal-strengthened Mg-7.2Zn-2.4Gd (wt.%) alloy with different concentrations of Ca addition (0, 0.16, 0.32, and 0.64 wt.%) by traditional gravity casting, followed by extrusion at 573 K with the extrusion ratio of 9 : 1. The microstructure and room temperature tensile properties of as-cast and as-extruded alloys are characterized. With the addition of the trace amount of Ca, the I-phase tends to transfer into W-phase due to the appearance of Mg2Ca and Mg6Zn3Ca2. As a consequence, the mechanical properties of the as-cast Ca containing alloys are downgraded. After extrusion, in comparison to the as-cast alloys, microstructure of the four types of alloys is refined and mechanical property is enhanced greatly. With the increasing of Ca concentration, the grain size is decreased gradually. However, the yield strength of the alloys is decreased to about 230 MPa and then up to 269 MPa, while the elongation increases first from 12.9% to 13.6% yet then decreases to 9.9%.


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