Determination of material properties and failure using in-situ thermo-mechanical probe

2014 ◽  
Author(s):  
B. Arrazat ◽  
S. Orellana ◽  
C. Rivero ◽  
P. Fornara ◽  
A. Di-Giacomo ◽  
...  
Keyword(s):  
Material Properties ◽  
Mechanical Probe

Identification and Determination of Material Properties for Porohyperelastic Analysis of Large Arteries

1998 ◽  
Vol 120 (2) ◽  
pp. 188-194 ◽  
Author(s):  
B. R. Simon ◽  
M. V. Kaufmann ◽  
M. A. McAfee ◽  
A. L. Baldwin ◽  
L. M. Wilson
Keyword(s):  
Experimental Data ◽  
Data Reduction ◽  
Material Properties ◽  
Effective Strain ◽  
Material Model ◽  
Radial Component ◽  
Constitutive Law ◽  
Hydraulic Permeability

A “porohyperelastic” (PHE) material model is described and the theoretical frame-work presented that allows identification of the necessary material properties functions for soft arterial tissues. A generalized Fung form is proposed for the PHE constitutive law in which the two fundamental Lagrangian material properties are the effective strain energy density function, We, and the hydraulic permeability, k˜ij. The PHE model is based on isotropic forms using We=Ue(φ)=1/2C0(eφ−1) and the radial component of permeability, k˜RR=k˜RR(φ), with φ=C′1(I¯1−3)+C′2(I¯2−3)+K′(J−1)2. The methods for determination of these material properties are illustrated using experimental data from in situ rabbit aortas. Three experiments are described to determine parameters in Ue and k˜RR for the intima and media of the aortas, i.e., (1) undrained tests to determine C0, C′1, and C′2 (2) drained tests to determine K′; and (3) steady-state pressurization tests of intact and de-endothelialized vessels to determine intimal and medial permeability (adventitia removed in these models). Data-reduction procedures are presented that allow determination of k˜RR for the intima and media and Ue for the media using experimental data. The effectiveness and accuracy of these procedures are studied using input “data” from finite element models generated with the ABAQUS program. The isotropic theory and data-reduction methods give good approximations for the PHE properties of in situ aortas. These methods can be extended to include arterial tissue remodeling and anisotropic behavior when appropriate experimental data are available.

Solid State Property - Bonding Electron Density – Volume Plasmon Energy Scaling Relationships: Novel AEM Technique for In Situ Diagnostics of Material Properties at the Nanoscale

2003 ◽  
Vol 791 ◽  
Author(s):  
Vladimir P. Oleshko ◽  
James M. Howe
Keyword(s):  
Solid State ◽  
Electron Density ◽  
Material Properties ◽  
Structure Property ◽  
Local Material ◽  
State Densities ◽  
Local Material Properties ◽  
Bonding Electron

ABSTRACTQuantized high-frequency (∼1016 Hz) correlated longitudinal electron excitations (plasmons) generated in the energy-loss range 0–50 eV by fast electrons passing through any solid enable one to probe various states of matter. Their energy, Ep, is directly related to the density of valence electrons, thus allowing determination of solid-state properties that are governed by ground-state densities. Universal features and scaling in relations between Ep and the cohesive energy per atomic volume, bonding electron density and elastic constants have been established. The resulting correlations follow the universal binding energy relationship, thus providing new insights into the fundamental nature of structure-property relationships. They allow direct in situ determination of local material properties in an analytical electron microscope, as illustrated by examples utilizing Al- and Ti-based structural alloys.

INDIREKTE PAPIERCHROMATOGRAPHISCHE METHODE ZUR BESTIMMUNG DER HARNOESTROGENE

1961 ◽  
Vol 38 (4) ◽  
pp. 545-562 ◽  
Author(s):  
L. Kecskés ◽  
F. Mutschler ◽  
I. Glós ◽  
E. Thán ◽  
I. Farkas ◽  
...  
Keyword(s):  
Pregnant Women ◽  
Granulosa Cell ◽  
Iron Content ◽  
List Type ◽  
Granulosa Cell Tumour ◽  
Hydrolysis Of ◽  
Phenol Fraction ◽  
Qualitative Determination

ABSTRACT 1. An indirect paperchromatographic method is described for separating urinary oestrogens; this consists of the following steps: acidic hydrolysis, extraction with ether, dissociation of phenol-fractions with partition between the solvents. Previous purification of phenol fraction with the aid of paperchromatography. The elution of oestrogen containing fractions is followed by acetylation. Oestrogen acetate is isolated by re-chromatography. The chromatogram was developed after hydrolysis of the oestrogens 'in situ' on the paper. The quantity of oestrogens was determined indirectly, by means of an iron-reaction, after the elution of the iron content of the oestrogen spot, which was developed by the Jellinek-reaction. 2. The method described above is satisfactory for determining urinary oestrogen, 17β-oestradiol and oestriol, but could include 16-epioestriol and other oestrogenic metabolites. 3. The sensitivity of the method is 1.3–1.6 μg/24 hours. 4. The quantitative and qualitative determination of urinary oestrogens with the above mentioned method was performed in 50 pregnant and 9 non pregnant women, and also in 2 patients with granulosa cell tumour.

Single Crystal Growth of High-Pressure Phases of Ice and Salt Hydrate Far Below the Original Melting Point by Mixing Alcohol: Crystal Structure Determination of Magnesium Chloride Heptahydrate

2020 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Hiroyuki Kagi
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
Crystal Growth ◽  
Single Crystal ◽  
Room Temperature ◽  
Growth Technique ◽  
Salt Hydrate ◽  
X Ray

An crystal-growth technique for single crystal x-ray structure analysis of high-pressure forms of hydrogen-bonded crystals is proposed. We used alcohol mixture (methanol: ethanol = 4:1 in volumetric ratio), which is a widely used pressure transmitting medium, inhibiting the nucleation and growth of unwanted crystals. In this paper, two kinds of single crystals which have not been obtained using a conventional experimental technique were obtained using this technique: ice VI at 1.99 GPa and MgCl<sub>2</sub>·7H<sub>2</sub>O at 2.50 GPa at room temperature. Here we first report the crystal structure of MgCl2·7H2O. This technique simultaneously meets the requirement of hydrostaticity for high-pressure experiments and has feasibility for further in-situ measurements.

Determination of Internal Stresses During Pearlite Transformation of 0.8c–1.5Mn Steel Through In-Situ Neutron Diffraction

2020 ◽  
Author(s):  
Satoshi Morooka ◽  
Nobuo Nakada ◽  
Yuhki Tsukada ◽  
Wu Gong ◽  
Takuro Kawasaki ◽  
...  
Keyword(s):  
Neutron Diffraction ◽  
Internal Stresses
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