Determination of Internal Stresses During Pearlite Transformation of 0.8c–1.5Mn Steel Through In-Situ Neutron Diffraction

2020 ◽  
Author(s):  
Satoshi Morooka ◽  
Nobuo Nakada ◽  
Yuhki Tsukada ◽  
Wu Gong ◽  
Takuro Kawasaki ◽  
...  
2020 ◽  
Author(s):  
Satoshi Morooka ◽  
Nobuo Nakada ◽  
Yuhki Tsukada ◽  
Wu Gong ◽  
Takuro Kawasaki ◽  
...  

Crystals ◽  
2020 ◽  
Vol 10 (4) ◽  
pp. 306 ◽  
Author(s):  
Sanket Sarkar ◽  
Yan Gao ◽  
Shenyan Huang ◽  
Saswata Bhattacharya ◽  
Swapnil Patil ◽  
...  

According to Eshelby’s theory, inelastically inhomogeneous inclusions in a metallic matrix give rise to a distribution of internal stresses. In the case of particle strengthened materials, such as nickel base superalloys, the presence and evolution of this back-stress leads to various observable effects, such as primary creep, back-flow upon loading, and memory of prior deformation. This article presents the background of the concept of back-stress and how it applies to the scenario of creep. A derivation of an evolution equation for back-stress in the context of primary creep is also presented. The results from neutron diffraction with in-situ creep experiments on directionally solidified nickel superalloys are presented in order to demonstrate the validity of the proposed equation and the corollaries derived therefrom.


2010 ◽  
Vol 25 (2) ◽  
pp. 143-148 ◽  
Author(s):  
Mark A. Rodriguez ◽  
Mark H. Van Benthem ◽  
David Ingersoll ◽  
Sven C. Vogel ◽  
Helmut M. Reiche

The electrochemical reaction behavior of a commercial Li-ion battery (LiFePO4-based cathode, graphite-based anode) has been measured via in situ neutron diffraction. A multivariate analysis was successfully applied to the neutron diffraction data set facilitating in the determination of Li bearing phases participating in the electrochemical reaction in both the anode and cathode as a function of state-of-charge (SOC). The analysis resulted in quantified phase fraction values for LiFePO4 and FePO4 cathode compounds as well as the identification of staging behavior of Li6, Li12, Li24, and graphite phases in the anode. An additional Li-graphite phase has also been tentatively identified during electrochemical cycling as LiC48 at conditions of ∼5% to 15% SOC.


2008 ◽  
Vol 137 ◽  
pp. 163-168
Author(s):  
S.G. Sheverev ◽  
G.V. Markova ◽  
V.V. Sumin

Spinodal decomposition of solid solution in the 60 at.% Mn - 40 at.% Cu alloy was observed at the temperatures of decomposition (380 – 420 °C) using the neutron diffraction method in situ. The contribution of residual stresses of third type introduced by further cooling of alloy and, correspondingly, martensitic tranformation is estimated. The relatively small value of stresses of third type introduced by martensitic transformation is revealed. Appearance of magnetic superstructural reflexes typical for antiferromagnetic ordered structure is noted.


2017 ◽  
Vol 896 ◽  
pp. 012123
Author(s):  
S J Vitzthum ◽  
C Hartmann ◽  
H A Weiss ◽  
G Baumgartner ◽  
M Hofmann ◽  
...  

2005 ◽  
Vol 502 ◽  
pp. 339-344 ◽  
Author(s):  
Jozef Zrník ◽  
O. Muránsky ◽  
Petr Lukáš ◽  
Petr Šittner ◽  
Z. Nový

The precise characterization of the multiphase microstructure of low alloyed TRIP steels is of great importance for the interpretation and optimisation of their mechanical properties. In-situ neutron diffraction experiment was employed for monitoring of conditioned austenite transformation to ferrite, and also for retained austenite stability evaluation during subsequent mechanical loading. The progress in austenite decomposition to ferrite is monitored at different transformation temperatures. The relevant information on the course of transformation is extracted from neutron diffraction spectra. The integrated intensities of austenite and ferrite neutron diffraction profiles over the time of transformation are then assumed as a measure of the volume fractions of both phases in dependence on transformation temperature. Useful information was also obtained on retained austenite stability in TRIP steel during mechanical testing. The in-situ neutron diffraction experiments were conducted at two different diffractometers to assess the reliability of neutron diffraction technique in monitoring the transformation of retained austenite during room temperature tensile test. In both experiments the neutron investigation was focused on the volume fraction quantification of retained austenite as well as on internal stresses rising in structure phases due to retained austenite transformation.


JOM ◽  
2014 ◽  
Vol 66 (8) ◽  
pp. 1425-1430 ◽  
Author(s):  
Jean-Marie Drezet ◽  
Bastien Mireux ◽  
Zoltan Szaraz ◽  
Thilo Pirling

Materials ◽  
2014 ◽  
Vol 7 (2) ◽  
pp. 1165-1172 ◽  
Author(s):  
Jean-Marie Drezet ◽  
Bastien Mireux ◽  
Zoltan Szaraz ◽  
Thilo Pirling

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