scholarly journals Comparison of mechanical properties for polyamide 12 composite-based biomaterials fabricated by fused filament fabrication and injection molding

Author(s):  
Tuan Noraihan Azila Tuan Rahim ◽  
Abdul Manaf Abdullah ◽  
Hazizan Md Akil ◽  
Dasmawati Mohamad
2015 ◽  
Vol 76 (7) ◽  
Author(s):  
Tuan Noraihan Azila Tuan Rahim ◽  
Hazizan Md Akil ◽  
Abdul Manaf Abdullah ◽  
Dasmawati Mohamad ◽  
Zainul Ahmad Rajion

Fused filament fabrication is a filament based rapid prototyping process, which offers the possibility of new polymer material for invention of biomedical implant. This study represents an investigation on a preparation and characterization of new polyamide 12 reinforced with 20 wt% of zirconium dioxide and hydroxyapatite by desktop 3D printer in comparison with conventional manufacturing method, injection molding. Polyamide 12 composite was compounded, pelletized and filament-extruded prior to apply to a 3D printer. Sample prototypes from the new polyamide composite have been successfully made and tested. Mechanical (flexural and impact) and morphological properties were evaluated and compared. From the results, the printed polyamide composite exhibited lower mechanical properties than injection molded due to the formation of porosity, laminate weakness and low pressure during printing. Although the mechanical properties of printed parts were lower than molded parts, but the capability of 3D printer to fabricate any customized 3D object could lead to the bright future and great contribution in this area, while at the same time many improvements can be made for the future works.


2021 ◽  
Vol 7 (2) ◽  
pp. 38
Author(s):  
Nectarios Vidakis ◽  
Markos Petousis ◽  
Lazaros Tzounis ◽  
Emmanuel Velidakis ◽  
Nikolaos Mountakis ◽  
...  

In this study, nanocomposites with polyamide 12 (PA12) as the polymer matrix and multiwalled carbon nanotubes (MWCNTs) and carbon black (CB) at different loadings (2.5, 5.0, and 10.0 wt.%) as fillers, were produced in 3D printing filament form by melt mixing extrusion process. The filament was then used to build specimens with the fused filament fabrication (FFF) three-dimensional (3D) printing process. The aim was to produce by FFF 3D printing, electrically conductive and thermoelectric functional specimens with enhanced mechanical properties. All nanocomposites’ samples were electrically conductive at filler loadings above the electrical percolation threshold. The highest thermoelectric performance was obtained for the PA12/CNT nanocomposite at 10.0 wt.%. The static tensile and flexural mechanical properties, as well as the Charpy’s impact and Vickers microhardness, were determined. The highest improvement in mechanical properties was observed for the PA12/CNT nanocomposites at 5.0 wt.% filler loading. The fracture mechanisms were identified by fractographic analyses of scanning electron microscopy (SEM) images acquired from fractured surfaces of tensile tested specimens. The nanocomposites produced could find a variety of applications such as; 3D-printed organic thermoelectric materials for plausible large-scale thermal energy harvesting applications, resistors for flexible circuitry, and piezoresistive sensors for strain sensing.


Polymers ◽  
2019 ◽  
Vol 11 (12) ◽  
pp. 2041 ◽  
Author(s):  
Hao Gu ◽  
Fayez AlFayez ◽  
Toseef Ahmed ◽  
Zahir Bashir

The 3D printing of articles by the effect of a directed laser beam on a plastic powder is a demanding process, and unlike injection molding, very few polymers work well enough with it. Recently, we reported that poly(ethylene terephthalate) (PET) powder has intrinsically good properties for 3D printing. Basic mechanical properties were shown earlier and it was demonstrated that unfused but heat-exposed PET powder does not degrade quickly allowing good re-use potential. In this work, we conducted a detailed comparison of the mechanical properties of PET and polyamide 12 from different build orientations. PET powders with two different molecular weights were used. With the high molecular weight powder, the processing parameters were optimized, and the printed bars showed little difference between the different orientations, which means there is low anisotropy in mechanical properties of built parts. Based on processing experience of the first powder, the second powder with a lower molecular weight was also very printable and complex parts were made with ease from the initial printing trials; since the process parameters were not optimized then, lower mechanical properties were obtained. While the intrinsic material properties of PET (melting and re-crystallization kinetics) are not the best for injection molding, PET is eminently suitable for powder bed fusion.


Materials ◽  
2021 ◽  
Vol 14 (2) ◽  
pp. 466
Author(s):  
Nectarios Vidakis ◽  
Markos Petousis ◽  
Lazaros Tzounis ◽  
Athena Maniadi ◽  
Emmanouil Velidakis ◽  
...  

Plastic waste reduction and recycling through circular use has been critical nowadays, since there is an increasing demand for the production of plastic components based on different polymeric matrices in various applications. The most commonly used recycling procedure, especially for thermoplastic materials, is based on thermomechanical process protocols that could significantly alter the polymers’ macromolecular structure and physicochemical properties. The study at hand focuses on recycling of polyamide 12 (PA12) filament, through extrusion melting over multiple recycling courses, giving insight for its effect on the mechanical and thermal properties of Fused Filament Fabrication (FFF) manufactured specimens throughout the recycling courses. Three-dimensional (3D) FFF printed specimens were produced from virgin as well as recycled PA12 filament, while they have been experimentally tested further for their tensile, flexural, impact and micro-hardness mechanical properties. A thorough thermal and morphological analysis was also performed on all the 3D printed samples. The results of this study demonstrate that PA12 can be successfully recycled for a certain number of courses and could be utilized in 3D printing, while exhibiting improved mechanical properties when compared to virgin material for a certain number of recycling repetitions. From this work, it can be deduced that PA12 can be a viable option for circular use and 3D printing, offering an overall positive impact on recycling, while realizing 3D printed components using recycled filaments with enhanced mechanical and thermal stability.


Author(s):  
A Miranda ◽  
M Leite ◽  
L Reis ◽  
E Copin ◽  
MF Vaz ◽  
...  

The aerospace, automotive, and marine industries are heavily reliant on sandwich panels with cellular material cores. Although honeycombs with hexagonal cells are the most commonly used geometries as cores, recently there have been new alternatives in the design of lightweight structures. The present work aims to evaluate the mechanical properties of metallic and polymeric honeycomb structures, with configurations recently proposed and different in-plane orientations, produced by additive and subtractive manufacturing processes. Structures with configurations such as regular hexagonal honeycomb (Hr), lotus (Lt), and hexagonal honeycomb with Plateau borders (Pt), with 0°, 45°, and 90° orientations were analyzed. To evaluate its properties, three-point bending tests were performed, both experimentally and by numerical modeling, by means of the finite element method. Honeycombs of two aluminum alloys and polylactic acid were fabricated. The structures produced in aluminum were obtained either by selective laser melting technology or by machining, while polylactic acid structures were obtained by material extrusion using fused filament fabrication. From the stress distribution analysis and the load–displacement curves, it was possible to evaluate the strength, stiffness, and absorbed energy of the structures. Failure modes were also analyzed for polylactic acid honeycombs. In general, a strong correlation was observed between numerical and experimental results. The results show that the stiffness and absorbed energy increase in the order, Hr, Pt, Lt, and with the orientation through the sequence, 45°, 90°, 0°. Thus, Lt structures with 0° orientation seem to be good alternatives to the traditional honeycombs used in sandwich composite panels for those industrial applications where low weight, high stiffness, and large energy-absorbing capacity are required.


2010 ◽  
Vol 39 (5) ◽  
pp. 775-780 ◽  
Author(s):  
Hu Youhua ◽  
Li Yimin ◽  
He Hao ◽  
Lou Jia ◽  
Tang Xiao

2012 ◽  
Vol 532-533 ◽  
pp. 234-237
Author(s):  
Wei Lai Chen ◽  
Ding Hong Yi ◽  
Jian Fu Zhang

The purpose of this paper is to study the effect of high temperature in injection molding process on mechanical properties of the warp-knitted and nonwoven composite fabrics (WNC)used in car interior. Tensile, tearing and peeling properties of WNC fabrics were tested after heat treatment under120, 140,160,180°C respectively. It was found that, after 140°C heat treatment, the breaking and tearing value of these WNC fabrics are lower than others. The results of this study show that this phenomenon is due to the material properties of fabrics. These high temperatures have no much effect on peeling properties of these WNC fabrics. It is concluded that in order to preserve the mechanical properties of these WNC fabrics, the temperature near 140°C should be avoided possibly during injection molding process.


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