New Equation for Surface Tension near the Critical Point

1971 ◽  
Vol 54 (8) ◽  
pp. 3485-3487
Author(s):  
Jeff Pressing
Keyword(s):  
Surface Tension ◽  
Critical Point ◽  
New Equation

The Critical Point Drying Method Applied to Scanning Electron Microscopy of L-929 Cells

1970 ◽  
Vol 28 ◽  
pp. 278-279
Author(s):  
Charles TurnbiLL ◽  
Delbert E. Philpott
Keyword(s):  
Electron Microscopy ◽  
Carbon Dioxide ◽  
Surface Tension ◽  
Critical Point ◽  
Freeze Drying ◽  
Attractive Alternative ◽  
Crystal Formation ◽  
Critical Point Drying ◽  
Time Required ◽  
Scanning Electron

The advent of the scanning electron microscope (SCEM) has renewed interest in preparing specimens by avoiding the forces of surface tension. The present method of freeze drying by Boyde and Barger (1969) and Small and Marszalek (1969) does prevent surface tension but ice crystal formation and time required for pumping out the specimen to dryness has discouraged us. We believe an attractive alternative to freeze drying is the critical point method originated by Anderson (1951; for electron microscopy. He avoided surface tension effects during drying by first exchanging the specimen water with alcohol, amy L acetate and then with carbon dioxide. He then selected a specific temperature (36.5°C) and pressure (72 Atm.) at which carbon dioxide would pass from the liquid to the gaseous phase without the effect of surface tension This combination of temperature and, pressure is known as the "critical point" of the Liquid.

Amplitude of the surface tension near the critical point

1984 ◽  
Vol 29 (1) ◽  
pp. 472-475 ◽  
Author(s):  
Edouard Brézin ◽  
Shechao Feng
Keyword(s):  
Surface Tension ◽  
Critical Point

scholarly journals Network of Palladium-Based Nanorings Synthesized by Liquid-Phase Reduction Using DMSO-H2O: In Situ Monitoring of Structure Formation and Drying Deformation by ASEM

2020 ◽  
Vol 21 (9) ◽  
pp. 3271 ◽  
Author(s):  
Takuki Komenami ◽  
Akihiro Yoshimura ◽  
Yasunari Matsuno ◽  
Mari Sato ◽  
Chikara Sato
Keyword(s):  
Surface Tension ◽  
Liquid Phase ◽  
Aqueous Solutions ◽  
Critical Point ◽  
Synthesis Method ◽  
Three Dimensional ◽  
In Situ Monitoring ◽  
Critical Point Drying ◽  
Micrometer Size

We developed a liquid-phase synthesis method for Pd-based nanostructure, in which Pd dissolved in dimethyl sulfoxide (DMSO) solutions was precipitated using acid aqueous solution. In the development of the method, in situ monitoring using atmospheric scanning electron microscopy (ASEM) revealed that three-dimensional (3D) Pd-based nanonetworks were deformed to micrometer-size particles possibly by the surface tension of the solutions during the drying process. To avoid surface tension, critical point drying was employed to dry the Pd-based precipitates. By combining ASEM monitoring with critical point drying, the synthesis parameters were optimized, resulting in the formation of lacelike delicate nanonetworks using citric acid aqueous solutions. Precipitation using HCl acid aqueous solutions allowed formation of 500-nm diameter nanorings connected by nanowires. The 3D nanostructure formation was controllable and modifiable into various shapes using different concentrations of the Pd and Cl ions as the parameters.

scholarly journals Surface tension of 4He near the critical point

1986 ◽  
Vol 115 (9) ◽  
pp. 455-458
Author(s):  
S. Herminghaus ◽  
P. Leiderer
Keyword(s):  
Surface Tension ◽  
Critical Point

scholarly journals Stability of an electrified liquid jet approaching to critical point

2020 ◽  
Vol 12 (7) ◽  
pp. 168781402093637
Author(s):  
Zixuan Fang ◽  
Ping Wang
Keyword(s):  
Surface Tension ◽  
Critical Point ◽  
Weber Number ◽  
Maximum Growth ◽  
Maximum Growth Rate ◽  
Wave Number ◽  
Electrical Field ◽  
Electric Stress ◽  
Electrical Field Intensity ◽  
The Stability

This article reports the linear stability analysis of a thermodynamic-transcritical jet sprayed to a radial electrical field. An asymptotic approach was used to obtain the stability solution of a supercritical jet subjected to electrical field. In order to obtain the solutions for the electrified supercritical jet, the surface tension was decreased and consequently led the increase in Weber number in the linear governing equation of subcritical charged jet. To investigate the role of surface tension and electric stress playing in the destabilizing process when approaching the critical point, the energy budget is performed by tracing the energy sources. It was found that, when the Weber number is increased to a sufficiently large value, the solution will become an asymptotic value, which can be considered as a solution under the supercritical conditions. The electric stress can increase both the maximum growth rate and the dominant wave number of electrified supercritical jet, that is, higher electrical field intensity would enhance the instability of the electrified supercritical jet and decrease the wavelength of the disturbances.

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