scholarly journals Novel synthesis of benzotriazolyl alkyl esters: an unprecedented CH2 insertion

RSC Advances ◽  
2021 ◽  
Vol 11 (13) ◽  
pp. 7564-7569
Author(s):  
Mohamed Elagawany ◽  
Lingaiah Maram ◽  
Bahaa Elgendy
Keyword(s):  
Building Block ◽  
Alkyl Esters ◽  
Novel Synthesis

Versatile synthesis of benzotriazolyl alkyl esters (BAEs) from N-acylbenzotriazoles using DCM as a methylene building block.

scholarly journals 1,1’-(3-Methyl-4-phenylthieno[2,3-b]thiophene-2,5-diyl)diethanone as a Building Block in Heterocyclic Synthesis. Novel Synthesis of Some Pyrazole and Pyrimidine Derivatives

Molecules ◽  
2011 ◽  
Vol 16 (8) ◽  
pp. 6502-6511 ◽  
Author(s):  
Yahia Nasser Mabkhot ◽  
Abdullah Mohammed Al-Majid ◽  
Assem Barakat ◽  
Saeed Alshahrani ◽  
Yamin Siddiqui
Keyword(s):  
Building Block ◽  
Heterocyclic Synthesis ◽  
Pyrimidine Derivatives ◽  
Novel Synthesis

Novel Synthesis of 2-Substituted 19-Norvitamin D A-Ring Phosphine Oxide from D-Glucose as a Building Block.

ChemInform ◽  
2003 ◽  
Vol 34 (30) ◽  
Author(s):  
Masato Shimizu ◽  
Yukiko Iwasaki ◽  
Yoshinori Shibamoto ◽  
Miki Sato ◽  
H. F. DeLuca ◽  
...  
Keyword(s):  
Phosphine Oxide ◽  
Building Block ◽  
Novel Synthesis

Novel Synthesis of 2-thienylcarbonyl-cyclohexane-1,3-dione as Building Block for Indazolones and Isoxazolones

2011 ◽  
Vol 64 (5) ◽  
pp. 638 ◽  
Author(s):  
Guillermo M. Chans ◽  
Elizabeth L. Moyano ◽  
Gloria I. Yranzo
Keyword(s):  
Nmr Spectroscopy ◽  
Ultrasonic Treatment ◽  
Building Block ◽  
Structural Elucidation ◽  
Synthetic Methodology ◽  
Novel Synthesis ◽  
Carbonyl Chloride

A new synthetic methodology using ultrasonic treatment was applied to the C-acylation of 1,3-cyclohexanedione with thiophene-2-carbonyl chloride to afford 3-hydroxy-2-(2-thienylcarbonyl)cyclohex-2-en-1-one (5). This compound was used as a building block to prepare different bicyclic systems: tetrahydro-4H-indazol-4-ones (7a–c and 9a,b,d), and 6,7-dihydrobenzisoxazole (11) by reaction with different hydrazines and hydroxylamine, respectively. Structural elucidation of all compounds was thoroughly achieved by NMR spectroscopy.

A Novel Synthesis of Esters via Substitution of the Benzotriazolyl Group in 1-(Benzotriazol-1-yl)alkyl Esters with Organozinc Reagents

Synthesis ◽  
1991 ◽  
Vol 1991 (01) ◽  
pp. 69-73 ◽  
Author(s):  
Alan R. Katritzky ◽  
Stanislaw Rachwal ◽  
Bogumila Rachwal
Keyword(s):  
Alkyl Esters ◽  
Novel Synthesis ◽  
Organozinc Reagents

ChemInform Abstract: Chemistry of Halonitroethenes. Part 2. Trichloronitroethenes as a Building Block for the Novel Synthesis of 5-Chloro(nitro)methyl-Substituted 1-Aryltetrazoles.

ChemInform ◽  
2012 ◽  
Vol 43 (28) ◽  
pp. no-no
Author(s):  
Viktor A. Zapol'skii ◽  
Xuena Yang ◽  
Jan C. Namyslo ◽  
Mimoza Gjikaj ◽  
Dieter E. Kaufmann
Keyword(s):  
Building Block ◽  
The Novel ◽  
Novel Synthesis ◽  
Substituted 1

Chemistry of Halonitroethenes, Part 2: Trichloronitroethene as a Building Block for the Novel Synthesis of 5-Chloro(nitro)methyl-Substituted 1-Aryltetrazoles

Synthesis ◽  
2012 ◽  
Vol 44 (06) ◽  
pp. 885-894 ◽  
Author(s):  
Dieter Kaufmann ◽  
Viktor Zapol'skii ◽  
Xuena Yang ◽  
Jan Namyslo ◽  
Mimoza Gjikaj
Keyword(s):  
Building Block ◽  
The Novel ◽  
Novel Synthesis ◽  
Substituted 1

Novel synthesis of 2-Substituted 19-norvitamin D A-ring phosphine oxide from d-glucose as a building block

2003 ◽  
Vol 13 (5) ◽  
pp. 809-812 ◽  
Author(s):  
Masato Shimizu ◽  
Yukiko Iwasaki ◽  
Yoshinori Shibamoto ◽  
Miki Sato ◽  
H.F DeLuca ◽  
...  
Keyword(s):  
Phosphine Oxide ◽  
Building Block ◽  
Novel Synthesis

scholarly journals Novel synthesis of pseudopeptides bearing a difluoromethyl group by Ugi reaction and desulfanylation

2011 ◽  
Vol 7 ◽  
pp. 1070-1074 ◽  
Author(s):  
Jingjing Wu ◽  
Hui Li ◽  
Song Cao
Keyword(s):  
Acetic Acid ◽  
Building Block ◽  
Ugi Reaction ◽  
The Novel ◽  
Protecting Group ◽  
Tributyltin Hydride ◽  
Novel Synthesis

Thirteen difluoromethyl-containing pseudopeptides were synthesized by Ugi reaction using the novel building block 2,2-difluoro-2-(phenylthio)acetic acid (2) as one component, followed by removal of the phenylsulfanyl protecting group in the presence of tributyltin hydride and azobisisobutyronitrile.

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