scholarly journals Visualizing the morphological and compositional evolution of the interface of InLi-anode|thio-LISION electrolyte in an all-solid-state Li–S cell by in operando synchrotron X-ray tomography and energy dispersive diffraction

2018 ◽  
Vol 6 (45) ◽  
pp. 22489-22496 ◽  
Author(s):  
Fu Sun ◽  
Kang Dong ◽  
Markus Osenberg ◽  
André Hilger ◽  
Sebastian Risse ◽  
...  

The interfacial evolution in ASSLSB is reported.

1977 ◽  
Vol 2 (4) ◽  
pp. 243-251 ◽  
Author(s):  
E. Laine ◽  
J. Kivilä ◽  
I. Lähteenmäki

The influence of preferred orientation on integrated x-ray intensities in powder specimen using energy-dispersive diffraction method is investigated. The theory used is based upon examination of the polar axis density distribution. The measurements were carried out using the Schulz technique added with defocusing correction. Experimental results are given for three aluminium powder specimens.


1985 ◽  
Vol 29 ◽  
pp. 243-250 ◽  
Author(s):  
W. Parrish ◽  
M. Hart ◽  
C. G. Erickson ◽  
N. Masciocchi ◽  
T. C. Huang

AbstractThe instrumentation developed for poly crystalline diffractometry using the storage ring at the Stanford Synchrotron Radiation Laboratory is described. A pair of automated vertical scan diffractometers was used for a Si (111) channel monochromator and the powder specimens. The parallel beam powder diffraction was defined by horizontal parallel slits which had several times higher intensity than a receiving slit at the same resolution. The patterns were obtained with 2:1 scanning with’ a selected monochromatic beam, and an energy dispersive diffraction method in which the monochromator is step-scanned, and the specimen and scintillation counter are fixed. Both methods use the same instrumentation.


2011 ◽  
Vol 18 (6) ◽  
pp. 938-941 ◽  
Author(s):  
Matthew R. Rowles

Equations for the calculation of the dimensions of a gauge volume, also known as the active volume or diffraction lozenge, in an energy-dispersive diffraction experiment where the detector is collimated by two ideal slits have been developed. Equations are given for equatorially divergent and parallel incident X-ray beams, assuming negligible axial divergence.


1983 ◽  
Vol 27 ◽  
pp. 331-337
Author(s):  
David R. Black ◽  
Carmen S. Menoni ◽  
Ian L. Spain

A wide range of structural studies have been carried out in high pressure diamond anvil cells using x-rays. The most common experimental geometry is shown in Fig. 1a. The incident x-ray beam passes axially through the first diamond and enters the sample, typically 100-300 μm in diameter and 20-100 μm thick; the diffracted x-rays exit via the second diamond. Energy-dispersive detection techniques (EDXRD) have been used. However the intensity of diffracted radiation from the sample is weak, so that typical exposure times with a conventional, fixed anode, x-ray source are typically one to several days.Accordingly, higher intensity radiation from synchrotron sources has been used for these experiments.


1995 ◽  
Vol 401 ◽  
Author(s):  
W. Dmowski ◽  
S. Fu ◽  
T. Egami ◽  
R. Gorte ◽  
J. Vhos

AbstractWe have utilized white x-ray beam and a Ge solid state detector, in energy dispersive mode, to study the diffraction from the surface layers of ceria deposited on (001) surface of Y stabilized cubic zirconia with grazing incident beam. We found that ceria forms islands, oriented epitaxially with respect to the zirconia substrate, with a lateral coherence of the order of 60 Å.


1978 ◽  
Vol 13 (1) ◽  
pp. 108-112 ◽  
Author(s):  
E. Laine ◽  
I. L�hteenm�ki ◽  
I. Lehtoranta

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