In situ formed graphene/ZnO nanostructured composites for low temperature hydrogen sulfide removal from natural gas

RSC Advances ◽  
2016 ◽  
Vol 6 (84) ◽  
pp. 81142-81150 ◽  
Author(s):  
Sunil P. Lonkar ◽  
Vishnu Pillai ◽  
Ahmed Abdala ◽  
Vikas Mittal

Nanostructured composites of graphene and highly dispersed sub-20 nm sized ZnO nanoparticles (TRGZ) were prepared via a novel method combining freeze-drying and thermal annealing.

ChemCatChem ◽  
2019 ◽  
Vol 11 (4) ◽  
pp. 1286-1294 ◽  
Author(s):  
Xiaoyun Song ◽  
Qingxin Guan ◽  
Yu Shu ◽  
Xiaojing Zhang ◽  
Wei Li

1988 ◽  
Vol 134 ◽  
Author(s):  
C. Robin Hwang ◽  
Michael F. Malone ◽  
Richard J. Farris ◽  
David C. Martin ◽  
Edwin L. Thomas

ABSTRACTA novel method of preparing PBZT/nylon composite fibers by infiltrating nylon into pure PBZT fiber is described. The pure PBZT fiber formed a microfibrillar network structure during coagulation, which is effective in reinforcing the matrix in the “in-situ network” composite fibers (designated IC). These new composite fibers exhibit nearly indistinguishable mechanical properties as those of “molecular” composite fibers (MC) prepared from isotropic solutions before and after tension heat-treatment (E = 44 GPa, σ = 430 MPa, ε = 1.2 %, σc = 250 MPa, G = 1.75 GPa) for PBZT/nylon weight ratios equal to unity.The fine structure of pure PBZT and its composite fibers spun from isotropic solutions was characterized using techniques based on nitrogen adsorption, small-angle X-ray scattering, scanning and transmission electron microscopies. The structure of both type of composites was found to be a microfibrillar network of PBZT in a matrix of amorphous nylon. The average diameters of the PBZT microfibrils were in the range of 10 to 20 nm for the IC and 4 nm for the MC.


2016 ◽  
Vol 8 (4) ◽  
pp. 312-319 ◽  
Author(s):  
Sunil P. Lonkar ◽  
Vishnu V. Pillai ◽  
Samuel Stephen ◽  
Ahmed Abdala ◽  
Vikas Mittal

2018 ◽  
Vol 8 (24) ◽  
pp. 6396-6406 ◽  
Author(s):  
Yanran Yang ◽  
Minghong Wang ◽  
Zuliang Tao ◽  
Qing Liu ◽  
Zhaoyang Fei ◽  
...  

Mn–Ti amorphous oxides prepared by the combinedin situdeposition and freeze-drying strategy exhibited excellent activities and stability in low-temperature NH3-SCR.


1997 ◽  
Vol 12 (7) ◽  
pp. 1678-1680 ◽  
Author(s):  
Y. L. Li ◽  
Y. D. Yu ◽  
Y. Liang

We report a novel method for the synthesis of carbon nanotubes: low temperature solid pyrolysis. By pyrolysis of hexamethyldisilazane-derived silicon carbonitride powders in a graphite furnace, we synthesized carbon nanotubes at 1400 °C. This new method has advantages of in situ growth of the carbon nanotubes, is stable in the synthesis process, and is technically simpler than conventional arc-discharge methods.


2006 ◽  
Vol 510-511 ◽  
pp. 878-881 ◽  
Author(s):  
Yuan Hua Mu ◽  
Yu Bao Li ◽  
Ming Bo Wang ◽  
Feng Lan Xu ◽  
Xiang Zhang ◽  
...  

Porous n-HA/PVA hydrogel composite was prepared through in-situ hydrothermal treatment under normal pressure and emulsion foam freeze-drying method, which was used to fabricate porous hydrogel. The pores exhibited interconnection-pore structure owing to the injection of air bubbles and the removal of emulsifier (OP). The porous hydrogels were investigated by using IR, XRD, TEM and SEM. The results indicated that n-HA in the composite could disperse uniformly, and there were chemical bonding with PVA. In addition, nano-hydroxyapatite existed in the composite in the shape of short-rod. The pores were interconnection with narrowly pore size and highly porosity. And the pore size and size distribution were influenced by the weight of OP. The emulsion foam freeze-drying method can be used to prepare porous hydrogel scaffold for tissue engineering, or to contain proteins scaffold, because of operating at a low temperature. The method displayed a vast potential of applied foreground.


RSC Advances ◽  
2014 ◽  
Vol 4 (88) ◽  
pp. 47414-47420 ◽  
Author(s):  
Zi Ping Wu ◽  
Man Zhao ◽  
Jing Wei Hu ◽  
Wei Bo Zhang ◽  
Yan Hong Yin ◽  
...  

H2WO4 sheets approximately 50 nm long and 20 nm wide were prepared using a DWCNT template, and WC nanosheets with large surface areas were obtained when the H2WO4 was carbonized at a low temperature using a liquid carbon source.


2015 ◽  
Vol 107 ◽  
pp. 100-102 ◽  
Author(s):  
Ke Tao ◽  
Jin Wang ◽  
Rui Jia ◽  
Yun Sun ◽  
Zhi Jin ◽  
...  

1992 ◽  
Vol 283 ◽  
Author(s):  
Naoki Kono ◽  
Tatsuro Nagahara ◽  
Kenji Fujimoto ◽  
Yusaku Kashiwagi ◽  
Hisashi Kakinoki

ABSTRACTThin film transistors were fabricated using polycrystalline silicon (poly-Si) film which were directly deposited on Corning 7059 glass substrates by plasma chemical vapor deposition method at very low temperature of 450°C. No annealing procedure was carried out in the fabrication process. The dependences of the crystallinity and the electrical properties on the poly-Si film thickness were investigated for three kinds of films deposited under different conditions. These dependences on the film thickness were found to be strongly influenced by the deposition condition, especially the reaction gas pressure. By choosing optimum poly-Si deposition condition carefully, high performance TFTs have been fabricated by this novel method.


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