Baylis–Hillman acetates in organic synthesis: convenient one-pot synthesis of α-carboline framework – a concise synthesis of neocryptolepine

2012 ◽  
Vol 10 (44) ◽  
pp. 8774 ◽  
Author(s):  
Deevi Basavaiah ◽  
Daggula Mallikarjuna Reddy
2013 ◽  
Vol 11 (3) ◽  
pp. 659-664 ◽  
Author(s):  
M. Mamaghani ◽  
F. Shirini ◽  
N. O. Mahmoodi ◽  
A. Azimi-Roshan ◽  
A. Monfared

RSC Advances ◽  
2014 ◽  
Vol 4 (78) ◽  
pp. 41631-41635 ◽  
Author(s):  
Atul Kumar ◽  
Ajay Kumar Bishnoi

We have demonstrated the first ligand free CuI-nanoparticle catalyzed N-arylation of amides/cyclic amides in an ethylene glycol/2-propanol solvent system under mild conditions. This is further extended for one pot synthesis of benzimidazole, and quinazolinone via intermolecular amidation followed by cyclization.


1978 ◽  
Vol 19 (20) ◽  
pp. 1759-1762 ◽  
Author(s):  
Yuji Oikawa ◽  
Hitoshi Hirasawa ◽  
Osamu Yonemitsu

Synlett ◽  
2017 ◽  
Vol 28 (10) ◽  
pp. 1201-1208 ◽  
Author(s):  
Lanting Xu ◽  
Xianhua Pan ◽  
Yanyu Chen ◽  
Qiujun Peng ◽  
Rong Zhang ◽  
...  

A highly efficient and generally applicable protocol, starting from 2-bromobenzamides and 2-bromo(thio)phenols via twice copper-catalyzed couplings to afford dibenzothiazepines and dibenzoxazepinones has been developed. High levels of yield and chemoselectivity are achieved in a single-pot reaction by using an appropriate ligand. Moreover, this facile methodology allows rapid access to a variety of bio­active compounds and known psychotropic drug, which should broaden its application in organic synthesis.


Molecules ◽  
2021 ◽  
Vol 26 (21) ◽  
pp. 6599
Author(s):  
Hina Mehmood ◽  
Muhammad Asif Iqbal ◽  
Muhammad Naeem Ashiq ◽  
Ruimao Hua

In the presence of Cs2CO3, the first simple, efficient, and one-pot procedure for the synthesis of 3,5-diaryl pyridines via a variety of aromatic terminal alkynes with benzamides as the nitrogen source in sulfolane is described. The formation of pyridine derivatives accompanies the outcome of 1,3-diaryl propenes, which are also useful intermediates in organic synthesis. Thus, pyridine ring results from a formal [2+2+1+1] cyclocondensation of three alkynes with benzamides, and one of the alkynes provides one carbon, whilst benzamides provide a nitrogen source only. A new transformation of alkynes as well as new utility of benzamide are found in this work.


2006 ◽  
Vol 47 (13) ◽  
pp. 2219-2222 ◽  
Author(s):  
Biswajit K. Singh ◽  
Shyam S. Verma ◽  
Namrata Dwivedi ◽  
Rama P. Tripathi

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