Fast, easy, clean chemistry by using water as a solvent and microwave heating: the Suzuki coupling as an illustration

2005 ◽  
pp. 2881 ◽  
Author(s):  
Nicholas E. Leadbeater
2004 ◽  
Vol 346 (13-15) ◽  
pp. 1627-1630 ◽  
Author(s):  
Robin B. Bedford ◽  
Craig P. Butts ◽  
Timothy E. Hurst ◽  
Pelle Lidström

2011 ◽  
Vol 7 ◽  
pp. 1294-1298 ◽  
Author(s):  
Bruno Piqani ◽  
Wei Zhang

Dihydropyrimidinones and dihydropyrimidinethiones generated from the Biginelli reactions of perfluorooctanesulfonyl-attached benzaldehydes are used as common intermediates for post-condensation modifications such as cycloaddition, Liebeskind–Srogl reaction and Suzuki coupling to form biaryl-substituted dihydropyrimidinone, dihydropyrimidine, and thiazolopyrimidine compounds. The high efficiency of the diversity-oriented synthesis is achieved by conducting a multicomponent reaction for improved atom economy, under microwave heating for fast reaction, and with fluorous solid-phase extractions (F-SPE) for ease of purification.


2002 ◽  
Author(s):  
Kazuo Aoki ◽  
Phadungsak Ratanadecho ◽  
Takashi Mikawa ◽  
Masatoshi Akahori

2002 ◽  
Author(s):  
Arnaud Jacotin ◽  
Elodie Bachelier ◽  
Francois Liousse ◽  
Pierre Millan

2013 ◽  
Vol 58 (3) ◽  
pp. 919-922 ◽  
Author(s):  
K. Granat ◽  
B. Opyd ◽  
D. Nowak ◽  
M. Stachowicz ◽  
G. Jaworski

Abstract The paper describes preliminary examinations on establishing usefulness criteria of foundry tooling materials in the microwave heating technology. Presented are measurement results of permittivity and loss tangent that determine behaviour of the materials in electromagnetic field. The measurements were carried-out in a waveguide resonant cavity that permits precise determination the above-mentioned parameters by perturbation technique. Examined were five different materials designed for use in foundry tooling. Determined was the loss factor that permits evaluating usefulness of materials in microwave heating technology. It was demonstrated that the selected plastics meet the basic criterion that is transparency for electromagnetic radiation.


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