Thermal decomposition of sulfur-containing organotin molecular precursors to produce phase-pure SnS

2000 ◽  
Vol 2 (24) ◽  
pp. 5708-5711 ◽  
Author(s):  
George A. A. Costa ◽  
Mercês C. Silva ◽  
Ana C. B. Silva ◽  
Geraldo M. de Lima ◽  
Rochel M. Lago ◽  
...  
Keyword(s):  
Thermal Decomposition ◽  
Molecular Precursors ◽  
Phase Pure ◽  
Sulfur Containing

Synthesis, characterization and photovoltaic properties of phase pure Cu2SnSe3 nanostructures using molecular precursors

2018 ◽  
Vol 29 (11) ◽  
pp. 8937-8946 ◽  
Author(s):  
Adish Tyagi ◽  
Alpa Y. Shah ◽  
G. Kedarnath ◽  
Amey Wadawale ◽  
Vishal Singh ◽  
...  
Keyword(s):  
Photovoltaic Properties ◽  
Molecular Precursors ◽  
Phase Pure

Surfactant-controlled low-temperature thermal decomposition route to monodispersed phase pure tricobalt tetraoxide nanoparticles

2013 ◽  
Vol 90 ◽  
pp. 111-114 ◽  
Author(s):  
Chira R. Bhattacharjee ◽  
Debraj Dhar Purkayastha ◽  
Nirmalendu Das
Keyword(s):  
Thermal Decomposition ◽  
Low Temperature ◽  
Phase Pure

A modified citrate gel route for the synthesis of phase pure Bi2Sr2CaCu2O8 superconductor

1994 ◽  
Vol 9 (6) ◽  
pp. 1357-1362 ◽  
Author(s):  
Sujatha P. Devi ◽  
H.S. Maiti
Keyword(s):  
Thermal Decomposition ◽  
Transition Temperature ◽  
Combustion Process ◽  
Superconducting Phase ◽  
Mechanism Of Formation ◽  
Sharp Transition ◽  
Simple Method ◽  
Phase Pure ◽  
Plausible Mechanism

A simple method for the bulk synthesis of 80 K bismuth-based superconducting phase (2212) is described. It employs a modified citrate gel route giving rise to an auto-ignited combustion process. The precursor ash obtained after combustion is further calcined at 800 °C to produce the desired superconducting powder with excellent homogeneity and fineness, leading to good sinterability and fairly sharp transition temperature. For a particular citrate-nitrate ratio, the nature of combustion of the gels containing two different bases has been compared. The thermal decomposition characteristics of the gels and the plausible mechanism of formation of the superconducting phase are also described.

Synthesis of Phase-Pure Ferromagnetic Fe3P Films from Single-Source Molecular Precursors

2012 ◽  
Vol 22 (9) ◽  
pp. 1850-1855 ◽  
Author(s):  
Adam C. Colson ◽  
Chih-Wei Chen ◽  
Emilia Morosan ◽  
Kenton H. Whitmire
Keyword(s):  
Single Source ◽  
Molecular Precursors ◽  
Phase Pure

Effect of anions on the morphology of CdS nanoparticles prepared via thermal decomposition of different cadmium thiourea complexes in a solvent and in the solid state

2015 ◽  
Vol 39 (12) ◽  
pp. 9442-9453 ◽  
Author(s):  
Rama Gaur ◽  
Pethaiyan Jeevanandam
Keyword(s):  
Thermal Decomposition ◽  
Solid State ◽  
Cds Nanoparticles ◽  
Capping Agent ◽  
Molecular Precursors ◽  
Excellent Method

Use of single-molecular precursors with different anions has been demonstrated to be an excellent method to synthesize CdS nanoparticles with different morphologies without using any external capping agent.

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