Highly efficient synthesis of phosphorodithioates derived from 3′-thiothymidine by anhydro-ring opening of 2,3′-anhydro-5′-O-tritylthymidine with O,O-disubstituted phosphorodithioic acids

1998 ◽  
pp. 427-428 ◽  
Author(s):  
Wojciech Da¸bkowski ◽  
Izabela Tworowska ◽  
Wojciech Da¸bkowski ◽  
Maria Michalska
2018 ◽  
Vol 5 (16) ◽  
pp. 2458-2462 ◽  
Author(s):  
Giacomo Berton ◽  
Giuseppe Borsato ◽  
Roberta Zangrando ◽  
Andrea Gambaro ◽  
Fabrizio Fabris ◽  
...  

C3-Symmetric tris-benzyl-O-substituted hexahydroxytriphenylene (HHTP) was prepared through selective ring opening with DIBAL-H in 48% yield (38% from HHTP in a two-step synthesis).


2021 ◽  
Author(s):  
Xuejin Yang ◽  
Laura M. Murphy ◽  
Farihah M. Haque ◽  
Scott M. Grayson ◽  
Andrew J. Boydston

We have developed a highly efficient synthesis of linear polydicyclopentadiene (pDCPD) via photoredox mediated metal-free ring-opening metathesis polymerization (MF-ROMP) and investigated the Tg–Mn dependence of linear pDCPD.


2017 ◽  
Vol 19 (24) ◽  
pp. 5789-5793 ◽  
Author(s):  
Kai Qiao ◽  
Xin Yuan ◽  
Li Wan ◽  
Ming-Wei Zheng ◽  
Dong Zhang ◽  
...  

A novel method for the synthesis of β-nitrate ester carboxamides using non-corrosivetert-butyl nitrite (TBN) as the nitro source and easily available oxygen as the oxidant has been developed.


2013 ◽  
Vol 9 ◽  
pp. 2129-2136 ◽  
Author(s):  
Akula Raghunadh ◽  
Satish S More ◽  
T Krishna Chaitanya ◽  
Yadla Sateesh Kumar ◽  
Suresh Babu Meruva ◽  
...  

A highly efficient synthesis of enantiomerically pure (S) and (R)-isomers of N-(2,3-dihydroxypropyl)arylamides has been developed with good overall yields in a two step process. The key step involves the ring opening of the chiral epoxide with a nitrogen heterocyclic carbene (NHC) and further rearrangement to chiral N-(2,3-dihydroxypropyl)arylamides in high yields and enantioselectivity. During the reaction, no erosion in chiral purity was observed.


RSC Advances ◽  
2015 ◽  
Vol 5 (115) ◽  
pp. 94571-94581 ◽  
Author(s):  
Xiang Sun ◽  
Yunwei Chen ◽  
Ningjie Wu ◽  
Chi Soo Kang ◽  
Hyun A. Song ◽  
...  

Ring opening of aziridinium ions with nitrogen nucleophiles was applied to highly efficient synthesis of optically active vicinal diamines and diethylene triamine pentaacetic acid (DTPA) analogues.


2014 ◽  
Vol 34 (1) ◽  
pp. 243-250
Author(s):  
Jianghong DING ◽  
Le XU ◽  
Hao XU ◽  
Haihong WU ◽  
Yueming LIU ◽  
...  

2013 ◽  
Vol 17 (3) ◽  
pp. 283-295 ◽  
Author(s):  
Jadwiga Soloducho ◽  
Joanna Cabaj ◽  
Kamila Olech ◽  
Przemyslaw Data ◽  
Mieczyslaw Lapkowski

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