Ferrocene-Containing Multifunctional Polyethers: Monomer Sequence Monitoring via Quantitative 13C NMR Spectroscopy in Bulk

2014 ◽  
Vol 47 (7) ◽  
pp. 2242-2249 ◽  
Author(s):  
Arda Alkan ◽  
Adrian Natalello ◽  
Manfred Wagner ◽  
Holger Frey ◽  
Frederik R. Wurm
Keyword(s):  
Nmr Spectroscopy ◽  
13C Nmr ◽  
13C Nmr Spectroscopy ◽  
Monomer Sequence ◽  
Quantitative 13C Nmr Spectroscopy

A study of species formation of aqueous tertiary and hindered amines using quantitative 13C NMR spectroscopy

2012 ◽  
Vol 18 (1) ◽  
pp. 568-573 ◽  
Author(s):  
Jeong Ho Choi ◽  
Seong Geun Oh ◽  
Yeo Il Yoon ◽  
Soon kwan Jeong ◽  
Kyung Ryong Jang ◽  
...  
Keyword(s):  
Nmr Spectroscopy ◽  
13C Nmr ◽  
13C Nmr Spectroscopy ◽  
Species Formation ◽  
Quantitative 13C Nmr Spectroscopy ◽  
Hindered Amines

Quantitative 13C-NMR spectroscopy of coals using 200 MHz-spectrometers

1993 ◽  
Vol 346 (6-9) ◽  
pp. 805-807 ◽  
Author(s):  
Sabine Wiggershaus-Eschert ◽  
Inge Wieschenk�mper ◽  
Wolfgang Riepe
Keyword(s):  
Nmr Spectroscopy ◽  
13C Nmr ◽  
13C Nmr Spectroscopy ◽  
Quantitative 13C Nmr Spectroscopy

Quantitative 13C NMR spectroscopy. Chemical structure of kraft and nitrosated lignins

2012 ◽  
Vol 38 (7) ◽  
pp. 720-725 ◽  
Author(s):  
L. V. Kanitskaya ◽  
A. F. Gogotov ◽  
Dam Thi Thanh Khai ◽  
A. V. Rokhin
Keyword(s):  
Nmr Spectroscopy ◽  
13C Nmr ◽  
Chemical Structure ◽  
13C Nmr Spectroscopy ◽  
Quantitative 13C Nmr Spectroscopy

scholarly journals (2S,3R,6R)-2-[(R)-1-Hydroxyallyl]-4,4-dimethoxy-6-methyltetrahydro-2H-pyran-3-ol

Molbank ◽  
10.3390/m1140 ◽  
2020 ◽  
Vol 2020 (2) ◽  
pp. M1140
Author(s):  
Jack Bennett ◽  
Paul Murphy
Keyword(s):  
Mass Spectrometry ◽  
Nmr Spectroscopy ◽  
Ir Spectroscopy ◽  
13C Nmr ◽  
Conjugate Addition ◽  
13C Nmr Spectroscopy ◽  
One Pot ◽  
1H And 13C Nmr ◽  
Esi Mass Spectrometry ◽  
The One

(2S,3R,6R)-2-[(R)-1-Hydroxyallyl]-4,4-dimethoxy-6-methyltetrahydro-2H-pyran-3-ol was isolated in 18% after treating the glucose derived (5R,6S,7R)-5,6,7-tris[(triethylsilyl)oxy]nona-1,8-dien-4-one with (1S)-(+)-10-camphorsulfonic acid (CSA). The one-pot formation of the title compound involved triethylsilyl (TES) removal, alkene isomerization, intramolecular conjugate addition and ketal formation. The compound was characterized by 1H and 13C NMR spectroscopy, ESI mass spectrometry and IR spectroscopy. NMR spectroscopy was used to establish the product structure, including the conformation of its tetrahydropyran ring.

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