Quantitative 13C-NMR spectroscopy of coals using 200 MHz-spectrometers

1993 ◽  
Vol 346 (6-9) ◽  
pp. 805-807 ◽  
Author(s):  
Sabine Wiggershaus-Eschert ◽  
Inge Wieschenk�mper ◽  
Wolfgang Riepe
2012 ◽  
Vol 18 (1) ◽  
pp. 568-573 ◽  
Author(s):  
Jeong Ho Choi ◽  
Seong Geun Oh ◽  
Yeo Il Yoon ◽  
Soon kwan Jeong ◽  
Kyung Ryong Jang ◽  
...  

2012 ◽  
Vol 38 (7) ◽  
pp. 720-725 ◽  
Author(s):  
L. V. Kanitskaya ◽  
A. F. Gogotov ◽  
Dam Thi Thanh Khai ◽  
A. V. Rokhin

2014 ◽  
Vol 47 (7) ◽  
pp. 2242-2249 ◽  
Author(s):  
Arda Alkan ◽  
Adrian Natalello ◽  
Manfred Wagner ◽  
Holger Frey ◽  
Frederik R. Wurm

Molbank ◽  
10.3390/m1140 ◽  
2020 ◽  
Vol 2020 (2) ◽  
pp. M1140
Author(s):  
Jack Bennett ◽  
Paul Murphy

(2S,3R,6R)-2-[(R)-1-Hydroxyallyl]-4,4-dimethoxy-6-methyltetrahydro-2H-pyran-3-ol was isolated in 18% after treating the glucose derived (5R,6S,7R)-5,6,7-tris[(triethylsilyl)oxy]nona-1,8-dien-4-one with (1S)-(+)-10-camphorsulfonic acid (CSA). The one-pot formation of the title compound involved triethylsilyl (TES) removal, alkene isomerization, intramolecular conjugate addition and ketal formation. The compound was characterized by 1H and 13C NMR spectroscopy, ESI mass spectrometry and IR spectroscopy. NMR spectroscopy was used to establish the product structure, including the conformation of its tetrahydropyran ring.


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