Pressure Effects on Lipidic Direct Phases:  The Dodecyl Trimethyl Ammonium Chloride−Water System

2006 ◽  
Vol 110 (25) ◽  
pp. 12410-12418 ◽  
Author(s):  
Lydia Paccamiccio ◽  
Michela Pisani ◽  
Francesco Spinozzi ◽  
Claudio Ferrero ◽  
Stephanie Finet ◽  
...  
1986 ◽  
Vol 90 (9) ◽  
pp. 1860-1863 ◽  
Author(s):  
John D. Gault ◽  
Edward Kavanagh ◽  
Lazaro A. Rodrigues ◽  
Hugo Gallardo

1991 ◽  
Vol 95 (4) ◽  
pp. 1703-1710 ◽  
Author(s):  
Haakan Hagslaett ◽  
Olle Soederman ◽  
Bengt Joensson ◽  
Lennart B. A. Johansson

Crystals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 449
Author(s):  
Shuai Yu ◽  
Hui Chen ◽  
Xujie Gao ◽  
Weichun Feng ◽  
Wenguo Xing ◽  
...  

Reaction crystallization to produce glycidyl trimethyl ammonium chloride (GTA) via epichlorohydrin with gas-state trimethylamine was investigated. The crystallization process of the GTA gas-liquid reaction was optimized by a seed method. The optimized technology can prepare GTA products with crystal form and purity greater than 97%. The crystallization process of GTA consists of four steps (i.e., addition of seed, dispersion of seed, growth of crystals on the seed surfaces, agglomeration and growth of crystal). Seed method and flow rate are the key factors affecting purity. The purity and particle size of GTA crystals were satisfactory as long as the operation was kept within the defined envelope. The experiments were conducted on a 1 L reactor and successfully scaled-up to 3000 L in industry.


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