Superstructures and Correlated Metal Ion Layers in Langmuir−Blodgett Films of Cadmium Soaps Observed with Grazing Incidence X-ray Diffraction

2000 ◽  
Vol 104 (23) ◽  
pp. 5553-5556 ◽  
Author(s):  
J. B. Peng ◽  
G. T. Barnes ◽  
I. R. Gentle ◽  
G. J. Foran
Langmuir ◽  
1998 ◽  
Vol 14 (20) ◽  
pp. 5896-5899 ◽  
Author(s):  
Deborah B. Hammond ◽  
Trevor Rayment ◽  
Damien Dunne ◽  
Philip Hodge ◽  
Ziad Ali-Adib ◽  
...  

Langmuir ◽  
2002 ◽  
Vol 18 (21) ◽  
pp. 8260-8262 ◽  
Author(s):  
Jeffrey T. Culp ◽  
Mark Davidson ◽  
Randolph S. Duran ◽  
Daniel R. Talham

2004 ◽  
Vol 19 (1) ◽  
pp. 45-48 ◽  
Author(s):  
B. K. Tanner ◽  
T. P. A. Hase ◽  
T. A. Lafford ◽  
M. S. Goorsky

The laboratory implementation of grazing incidence in-plane X-ray diffraction, using an unmodified commercial diffractometer, is described. Low resolution, high intensity measurements are illustrated in the study of the in-plane lattice parameters and texture of a thin polycrystalline ZnO film on glass, the in-plane order in Cd arachidate Langmuir–Blodgett films, and the depth dependence of the lattice parameter in graded Si–Ge epilayers. Use of an asymmetrically cut Ge crystal to compress and monochromate the beam provides a high resolution setting, appropriate to measurement of the in-plane mosaic of mismatched epilayers such as GaN on sapphire.


1991 ◽  
Vol 237 ◽  
Author(s):  
B. K. Tanner ◽  
D. K Bowen ◽  
M. C Petty ◽  
S. Swaminathan ◽  
F. Granfeld

ABSTRACTGrazing incidence X-ray reflectometry has been used to characterize Langmuir-Blodgett films of cadmium arachidate deposited on silicon substrates. The agreement between layer parameters deduced from the interference fringe period and low angle Bragg peak positions was excellent. Good agreement was found between experimental and simulated reflectivity profiles only when interface roughness and a varying molecular layer thickness was included. Inclusion of interface roughness alone results in a substantial enhancement in the intensity of the Bragg peaks. This effect is identified as being equivalent to the reduction in extinction found in classical X-ray diffraction due to crystal imperfections.


1992 ◽  
Vol 247 ◽  
Author(s):  
Yoshio Nogami ◽  
Kazuyoshi Ogasawara ◽  
Shigeki Takeuchi ◽  
Takehiko Ishiguro ◽  
Kazumasa Ohsumi ◽  
...  

ABSTRACTStacking of heterogeneous Langmuir-Blodgett films was studied by high resolution X-ray diffraction method using synchrotron radiation (SR) source. The diffraction patterns of the heterogeneous films formed with alternately deposited Cd salts of fatty acids with different length of alkyl chains exhibit anomalous oscillatory structure in diffraction vector.


1990 ◽  
Vol 208 ◽  
Author(s):  
Brian K Tanner ◽  
Simon J Miles ◽  
D Keith Bowen ◽  
Linda Hart ◽  
Neil Loxley

ABSTRACTX-ray reflectance measurements at grazing incidence provide non-destructively a measure of the thickness of thin layers, the electron density as a function of depth, and interface and surface roughness. We show that the effect of roughness at a buried interface is only to reduce the visibility of the interference fringes, whereas roughness at the top surface leads also to an overall increase in the rate of fall of intensity with angle (or energy). These two contributions can then be readily distinguished.Most work has been performed in monochromatic angular dispersive mode. We present here a preliminary study of the application of the high-energy, fixed-angle, energy dispersive mode for the study of thin epitaxial layers, Langmuir-Blodgett films, surface damage on silicon chemi-sol polished wafers and ion implanted silicon and aluminium. Data has been analysed using the theory of Parratt, which we have adapted for use in the energy dispersive method.


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