Prediction of the Effect of Mobile-Phase Salt Type on Protein Retention and Selectivity in Anion Exchange Systems

2003 ◽  
Vol 75 (14) ◽  
pp. 3563-3572 ◽  
Author(s):  
Nihal Tugcu ◽  
Minghu Song ◽  
Curt M. Breneman ◽  
N. Sukumar ◽  
Kristin P. Bennett ◽  
...  
1989 ◽  
Vol 28 (3-4) ◽  
pp. 170-178 ◽  
Author(s):  
P. R. Levison ◽  
D. W. Toome ◽  
S. E. Badger ◽  
B. N. Brook ◽  
D. Carcary

1988 ◽  
Vol 71 (5) ◽  
pp. 930-933 ◽  
Author(s):  
James F Lawrence ◽  
Rajinder K Chadha

Abstract Sulfite was determined in a variety of foods by liquid chromatography (LC) after the samples were mixed with a solution containing mannitol, FeS04, and Na2HP04, adjusted to pH 11, and left to stand for 15 min at room temperature. An aliquot of the mixture was placed in a headspace vial and mixed with 50% H3P04. After 15 min, a portion of the headspace was removed with a syringe containing LC mobile phase without acetonitrile. The syringe was shaken and an aliquot of the solution was analyzed on an anion exchange column with a mobile phase of 0.03M methane sulfonate (pH 10.8) containing 5% acetonitrile. Sulfite was detected amperometrically (glassy carbon electrode) at +0.7 V. The method was successfully compared to the FDA-modified Monier-Williams procedure for a variety of foods. Minimum detectable levels were about 1 ng/g, based on a 15 g sample


ChemInform ◽  
2003 ◽  
Vol 34 (4) ◽  
Author(s):  
Minghu Song ◽  
Curt M. Breneman ◽  
Jinbo Bi ◽  
N. Sukumar ◽  
Kristin P. Bennett ◽  
...  

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