Electrochemiluminescence from successive electro- and chemo-oxidation of rifampicin and its application to the determination of rifampicin in pharmaceutical preparations and human urine

2007 ◽  
Vol 67 (2) ◽  
pp. 430-436 ◽  
Author(s):  
Yao-Dong Liang ◽  
Jun-Feng Song ◽  
Min Xu
Keyword(s):  
Human Urine ◽  
Pharmaceutical Preparations

scholarly journals Determination of phenobarbital in human urine and serum usingflow injection chemiluminescence

2012 ◽  
Vol 58 (1) ◽  
pp. 88-94
Author(s):  
K. Li ◽  
L.Z. Nu ◽  
K.L. Khe ◽  
K.H. Song
Keyword(s):  
Human Urine ◽  
Pharmaceutical Preparations ◽  
Injection System ◽  
Chemiluminescence Method ◽  
Chemiluminescence Intensity ◽  
Complete Determination ◽  
Flow Injection System ◽  
Human Urine And Serum ◽  
Urine And Serum

A sensitive chemiluminescence method, based on the enhancive effect of phenobarbital on the chemiluminescence reaction between luminol and dissolved oxygen in a flow injection system, was proposed for the determination of phenobarbital. The chemiluminescence intensity responded to the concentration of phenobarbital linearly ranging from 0.05 to 10 ng⋅ml-1 with the detection limit of 0.02 ng⋅ml-1 (3σ). At a flow rate of 2.0 ml⋅min-1, a complete determination of phenobarbital, including sampling and washing, could be accomplished in 0.5 min, offering the sampling efficiency of 120 h-1 accordingly. The method was applied successfully in an assay of PB for pharmaceutical preparations, human urine and serum without any pretreatment with recovery from 95.7 to 106.7% and RSDs of less than 3.0%.

Modified carbon paste and polymeric membrane electrodes for determination of hydroxychloroquine sulfate in pharmaceutical preparations and human urine

RSC Advances ◽  
2015 ◽  
Vol 5 (102) ◽  
pp. 83657-83667 ◽  
Author(s):  
M. M. Khalil ◽  
Y. M. Issa ◽  
G. A. El Sayed
Keyword(s):  
Human Urine ◽  
Pharmaceutical Preparations ◽  
Polymeric Membrane ◽  
Membrane Electrodes ◽  
Sodium Tetraphenylborate ◽  
Carbon Paste

This article describes characteristics, performance and application of hydroxychloroquine (HCQ) polymeric membrane (PMEs) and modified carbon paste (CPEs) electrodes which are based on sodium tetraphenylborate (NaTPB) or ammonium reineckate (Rt) as sensing materials.

Electroanalytical determination of lormetazepam in pharmaceutical preparations and human urine

1992 ◽  
Vol 4 (8) ◽  
pp. 811-817
Author(s):  
A. Zapardiel ◽  
E. Bermejo ◽  
J. A. Pérez López ◽  
P. Mateo ◽  
L. Hernández
Keyword(s):  
Human Urine ◽  
Pharmaceutical Preparations
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