Photoelectronic device for measuring glass tube diameters

1971 ◽  
Vol 14 (5) ◽  
pp. 688-690
Author(s):  
N. M. Protsenko ◽  
V. I. Skurikhin
Author(s):  
W. Liebrich

HeLa cells were grown for 2-3 days in EAGLE'S minimum essential medium with 10% calf serum (S-MEM; Seromed, München) and then incubated for 24 hours in serum free medium (MEM). After detaching the cells with a solution of 0. 14 % EDTA and 0. 07 % trypsin (Difco, 1 : 250) they were suspended in various solutions (S-MEM = control, MEM, buffered salt solutions with or without Me++ions, 0. 9 % NaCl solution) and allowed to settle on glass tube slips (Leighton-tubes). After 5, 10, 15, 20, 25, 30, 1 45, 60 minutes 2, 3, 4, 5 hours cells were prepared for scanning electron microscopy as described by Paweletz and Schroeter. The preparations were examined in a Jeol SEM (JSM-U3) at 25 KV without tilting.The suspended spherical HeLa cells are able to adhere to the glass support in all solutions. The rate of attachment, however, is faster in solutions without serum than in the control. The latter is in agreement with the findings of other authors.


Author(s):  
David C Joy

The electron source is the most important component of the Scanning electron microscope (SEM) since it is this which will determine the overall performance of the machine. The gun performance can be described in terms of quantities such as its brightness, its source size, its energy spread, and its stability and, depending on the chosen application, any of these factors may be the most significant one. The task of the electron gun in an SEM is, in fact, particularly difficult because of the very wide range of operational parameters that may be required e.g a variation in probe size of from a few angstroms to a few microns, and a probe current which may go from less than a pico-amp to more than a microamp. This wide range of operating parameters makes the choice of the optimum source for scanning microscopy a difficult decision.Historically, the first step up from the sealed glass tube ‘cathode ray generator’ was the simple, diode, tungsten thermionic emitter.


Author(s):  
Y.D. Yu ◽  
R. Guan ◽  
K.H. Kuo ◽  
H. Hashimoto

We have indicated that the lighter atoms such as oxygen in Cu2O can be observed at the specimen with optimal thicknesses based on the dynamic effect of electron diffraction(1). This rule in principle should hold good for the imaging of other lighter atoms such as sulphur atom in Cu2S. However, this point of view needs further experimentally confirm because up to now only oxygen atoms have been observed in Cu2O and a series of new suboxides of copper and nickel (2). In addition, the sulphur atom is much heavier than oxygen one though is still lighter than copper atom. In the present report we provide such a confirmation.The crystallites of Cu2S shown in Fig.l were obtained by sulfurizing at 300°C of the copper thin film which was sealed in a glass tube with mg sulphur left on the tube wall in a vacuum of about 10-2 Pa. The energy dispersive spectrocscopy analysis indicated that they are the sulfides and the electron diffraction analysis indicated they have anti-fluorite structure.


2018 ◽  
Vol 15 (2) ◽  
pp. 188-196 ◽  
Author(s):  
Chengpeng Xu ◽  
Shengying Ye ◽  
Xiaolei Cui ◽  
Quan Zhang ◽  
Yan Liang

Background: Improper storage and raw materials make peanut oil susceptible to Aflatoxin B1 (AFB1). The semiconductor TiO2 photocatalysis technology is an effective technology which is widely used in sewage treatment, environmental protection and so on. Moreover, the photocatalytic efficiency can be improved by doping I. Method: The experiment is divided into two parts. In the first part, supported TiO2 thin film (STF) was prepared on the quartz glass tube (QGT) by the sol-gel and calcination method and the supported iodine doped supported TiO2 thin film (I-STF) was synthesized using potassium iodate solution. In the second part, the photocatalytic degradation of AFB1 was performed in a self-made photocatalytic reactor. The AFB1 was detected by ELISA kit. Results: The photocatalytic degradation of AFB1 has been proven to follow pseudo first-order reaction kinetics well (R2 > 0.95). The maximum degradation rate of 81.96%, which was reached at the optimum iodine concentration of 0.1mol/L, was 11.38% higher than that with undoped STF. The doping of iodine reduces the band-gap of TiO2, thereby increasing the photocatalytic response range. The proportion of Ti4+ in I-STF has decreased, which means that Ti4+ are replaced by I. The I-STF prepared at iodine concentration of 0.1mol/L has good photocatalytic properties.


Radiocarbon ◽  
2021 ◽  
pp. 1-10
Author(s):  
S Therre ◽  
L Proß ◽  
R Friedrich ◽  
M Trüssel ◽  
N Frank

ABSTRACT To achieve high-precision and reproducible results from radiocarbon (14C) dating of carbonate samples in paleoclimate research, a new CO2 extraction line was designed, constructed, and characterized at the Heidelberg Radiocarbon Lab of the Institute of Environmental Physics, Heidelberg. The setup includes a circular glass-tube design, which is operated at vacuum pressure levels of the order of 10–5 mbar. The efficiency of the extraction process was assessed, showing significantly favorable conditions for solid piece samples (99.58 ± 4.69)% over powdered samples (88.28 ± 10.03)%. Process blank values are below 0.2 pMC apparent 14C activity. Repeated measurements of IAEA C2 standards with an average value of (41.09 ± 0.23) pMC attest high accuracy and reproducibility of the instrument. Six consecutive samples of 6 to 12 mg carbonate mass can be processed in one run of roughly 2.5 hours. Thus, the new setup contributes to time-efficient and reproducible radiocarbon dating results for paleoclimate research at the Institute of Environmental Physics. In a first application, Dead Carbon Fraction (DCF) values of a Holocene alpine stalagmite from Schratten Cave are presented, revealing extraordinarily high offsets between atmospheric and stalagmite 14C with DCF values between (49.4 ± 0.4)% and (61.6 ± 0.4)%.


2015 ◽  
Vol 2015 ◽  
pp. 1-8
Author(s):  
Zhijun Zhang ◽  
Shiwei Zhang

The working principle of the refractive-type fiber optic liquid level sensor is analyzed in detail based on the light refraction principle. The optic path models are developed in consideration of common simplification and the residual liquid film on the glass tube wall. The calculating formulae for the model are derived, constraint conditions are obtained, influencing factors are discussed, and the scopes and skills of application are analyzed through instance simulations. The research results are useful in directing the correct usage of the fiber optic liquid level sensor, especially in special cases, such as those involving viscous liquid in the glass tube monitoring.


2001 ◽  
Vol 124 (1) ◽  
pp. 51-54 ◽  
Author(s):  
Eduardo A. Rinco´n ◽  
Fidel A. Osorio

A new two-dimensional concentrator for solar energy collection has been developed. The concentrator has the following advantages, when compared with the classic Compound Parabolic Concentrators invented by Roland Winston, W. T. Welford, A. Rabl, Baranov, and other researchers: 1) It allows the use of parabolic mirrors, which have a reflecting area much smaller for a given concentration ratio and acceptance angle. 2) Between the mirror and the absorber, there is a large gap so that conduction losses are reduced. Convection losses can be reduced, too, if the absorber is enclosed within a glass tube. 3) It can be easily manufactured. Instead of seeking the shape of the mirrors for a given shape of the absorber, we have made the inverse statement of the problem, and we have obtained the optimal shapes of the absorbers with a prescribed acceptance angle, for parabolic mirrors, assuming that the intercept factor is unity, the mirrors are perfect, and the absorber surfaces are convex. The concentrator should be east-west oriented, and could be seasonal or monthly tilt adjusted. This concentrator could have many practical applications, such as fluid heating, steam generation, etc.


1882 ◽  
Vol 33 (216-219) ◽  
pp. 257-258

The new cell consists of a flat copper case, of the same shape as a Grove’s cell; it has a lid of paraffined wood, from which hangs a plate of lead amalgamated with mercury, the lower part of the lead plate being held in a groove in a slip of paraffined wood resting on the bottom of the copper case: through the lid a hole is bored for the introduction of the solution, which consists of a solution of cupric sulphate, to which is added one-twelfth of hydric sulphate; the presence of this free sulphuric acid improves the cell at once. The following sectional sketch shows the arrangement:- AB. The outer flat copper case. C. Plate of amalgamated lead held in grooves in the cap D and the slip E. F shows the hole in the cap through which the solution is introduced, and by the introduction of a glass tube through this hole the state of the charge is seen by observing the colour; the interior surface of the case forms the negative, and the amalgamated lead the positive electrode.


2013 ◽  
Vol 28 (1) ◽  
pp. 13-17 ◽  
Author(s):  
F. Laufek ◽  
A. Vymazalová ◽  
D.A. Chareev ◽  
A.V. Kristavchuk ◽  
J. Drahokoupil ◽  
...  

The (Ag,Pd)22Se6 phase was synthesized from individual elements by silica glass tube technique and structurally characterized from powder X-ray diffraction data. The (Ag,Pd)22Se6 phase crystallizes in Fm$\overline3$m symmetry, unit-cell parameters: a = 12.3169(2) Å, V = 1862.55(5) Å3, Z = 4, and Dc = 10.01 g/cm3. The crystal structure of the (Ag,Pd)22Se6 phase represents a stuffed 3a.3a.3a superstructure of the Pd structure (fcc), where only 4 from 108 available octahedral holes are occupied. Its crystal structure is related to the Cr23C6 structure type.


Sign in / Sign up

Export Citation Format

Share Document