Elevated-temperature vacuum-assisted resin transfer molding process for high performance aerospace composites

2013 ◽  
Vol 62 (10) ◽  
pp. 1465-1476 ◽  
Author(s):  
Venkatagireesh Menta ◽  
Ramabhadraraju Vuppalapati ◽  
K Chandrashekhara ◽  
Thomas Schuman ◽  
Jilun Sha
Keyword(s):  
Elevated Temperature ◽  
High Performance ◽  
Resin Transfer Molding ◽  
Molding Process ◽  
Transfer Molding

High-performance bismaleimide resins with low cure temperature for resin transfer molding process

2016 ◽  
Vol 29 (3) ◽  
pp. 298-304 ◽  
Author(s):  
Ping Liu ◽  
Chunyan Qu ◽  
Dezhi Wang ◽  
Ming Zhao ◽  
Changwei Liu
Keyword(s):  
High Performance ◽  
Resin Transfer Molding ◽  
Molding Process ◽  
Transfer Molding ◽  
Bismaleimide Resins ◽  
Cure Temperature

scholarly journals A Review of Thermoplastic Resin Transfer Molding: Process Modeling and Simulation

Polymers ◽  
2019 ◽  
Vol 11 (10) ◽  
pp. 1555 ◽  
Author(s):  
Ageyeva ◽  
Sibikin ◽  
Kovács
Keyword(s):  
Polymer Composites ◽  
High Performance ◽  
Resin Transfer Molding ◽  
High Viscosity ◽  
Commercial Application ◽  
Future Research ◽  
Thermoplastic Resin ◽  
Molding Process ◽  
Transfer Molding ◽  
The Matrix

The production and consumption of polymer composites has grown continuously through recent decades and has topped 10 Mt/year. Until very recently, polymer composites almost exclusively had non-recyclable thermoset matrices. The growing amount of plastic, however, inevitably raises the issue of recycling and reuse. Therefore, recyclability has become of paramount importance in the composites industry. As a result, thermoplastics are coming to the forefront. Despite all their advantages, thermoplastics are difficult to use as the matrix of high-performance composites because their high viscosity complicates the impregnation process. A solution could be reactive thermoplastics, such as PA-6, which is synthesized from the ε-caprolactam (ε-CL) monomer via anionic ring opening polymerization (AROP). One of the fastest techniques to process PA-6 into advanced composites is thermoplastic resin transfer molding (T-RTM). Although nowadays T-RTM is close to commercial application, its optimization and control need further research and development, mainly assisted by modeling. This review summarizes recent progress in the modeling of the different aspects of the AROP of ε-CL. It covers the mathematical modeling of reaction kinetics, pressure-volume-temperature behavior, as well as simulation tools and approaches. Based on the research results so far, this review presents the current trends and could even plot the course for future research.

Manufacturing Fiber-Reinforced Polymer Composite Using RTM Process: An Analytical Approach

2017 ◽  
Vol 380 ◽  
pp. 60-65 ◽  
Author(s):  
M.J. do Nascimento Santos ◽  
A.G. Barbosa de Lima
Keyword(s):  
High Performance ◽  
Separation Of Variables ◽  
Resin Transfer Molding ◽  
Surface Finishing ◽  
Constant Thickness ◽  
Molding Process ◽  
Transfer Molding ◽  
Dimensional Precision ◽  
Good Surface ◽  
Injection Process

The Resin Transfer Molding process (RTM) has been widely used for manufacturing of high performance components in aerospace and automotive industries. It is an economical and faster method when compared to open molding process because it allows the molding of complex parts with constant thickness, dimensional precision, good surface finishing and an excellent control of mechanical properties. In this sense, this work aims to study theoretically the manufacture process of polymeric composites reinforced with fibers via resin transfer molding. The governing equations of conservation of mass and momentum, and Darcy's law are presented, and the exact solution of the problems is obtained via method of separation of variables. Predicted results of the flow front and the pressure fields of the resin inside the model during the injection process are presented, compared with experimental data and analyzed. It was verified a good agreement between the results.

Cure Kinetics of High Performance Epoxy Molding Compounds

2014 ◽  
Vol 1024 ◽  
pp. 151-154
Author(s):  
Chean Cheng Su ◽  
Cheng Fu Yang ◽  
Chien Huan Wei
Keyword(s):  
Kinetic Model ◽  
High Performance ◽  
Resin Transfer Molding ◽  
Cure Kinetics ◽  
Molding Process ◽  
Transfer Molding ◽  
Molding Compounds ◽  
Higher Temperature ◽  
Kinetics Of ◽  
Rubber State

The reaction of EMCs with the triphenylphosphine-1,4-benzoquinone (TPP-BQ) latent catalyst also had a higher temperature sensitivity compared to the reaction of EMCs with triphenylphosphine (TPP) catalyst. In resin transfer molding, EMCs containing the TPP-BQ thermal latency accelerator are least active at a low temperature. Consequently, EMCs have a low melt viscosity before gelation, and the resins and filler are evenly mixed in the kneading process. Additionally, the rheological property, flowability, is increased before the EMC form a network structure in the molding process. The proposed kinetic model adequately describes curing behavior in EMCs cured with two different organophosphine catalysts up to the rubber state in the progress of curing.

scholarly journals A Conceptional Approach of Resin-Transfer-Molding to Rosin-Sourced Epoxy Matrix Green Composites

Aerospace ◽  
2020 ◽  
Vol 8 (1) ◽  
pp. 5
Author(s):  
Sicong Yu ◽  
Xufeng Zhang ◽  
Xiaoling Liu ◽  
Chris Rudd ◽  
Xiaosu Yi
Keyword(s):  
Composite Laminates ◽  
Resin Transfer Molding ◽  
High Viscosity ◽  
Ramie Fiber ◽  
Liquid Composite Molding ◽  
Curing Agent ◽  
Molding Process ◽  
Transfer Molding ◽  
Low Viscosity ◽  
Composite Molding

In this concept-proof study, a preform-based RTM (Resin Transfer Molding) process is presented that is characterized by first pre-loading the solid curing agent onto the preform, and then injecting the liquid nonreactive resin with an intrinsically low viscosity into the mold to infiltrate and wet the pre-loaded preform. The separation of resin and hardener helped to process inherently high viscosity resins in a convenient way. Rosin-sourced, anhydrite-cured epoxies that would normally be regarded as unsuited to liquid composite molding, were thus processed. Rheological tests revealed that by separating the anhydrite curing agent from a formulated RTM resin system, the remaining epoxy liquid had its flowtime extended. C-scan and glass transition temperature tests showed that the preform pre-loaded with anhydrite was fully infiltrated and wetted by the liquid epoxy, and the two components were diffused and dissolved with each other, and finally, well reacted and cured. Composite laminates made via this approach exhibited roughly comparable quality and mechanical properties with prepreg controls via autoclave or compression molding, respectively. These findings were verified for both carbon and ramie fiber composites.

Development of resin transfer molding process using scaling down strategy

2013 ◽  
Vol 35 (9) ◽  
pp. 1683-1689 ◽  
Author(s):  
Raghu Raja Pandiyan Kuppusamy ◽  
Swati Neogi
Keyword(s):  
Resin Transfer Molding ◽  
Molding Process ◽  
Transfer Molding ◽  
Scaling Down

scholarly journals Resin transfer molding process: a numerical and experimental investigation

2013 ◽  
Vol 7 (2) ◽  
pp. 125-136 ◽  
Author(s):  
Iran de Oliveira ◽  
Sandro Amico ◽  
Jeferson Souza ◽  
Antonio de Lima
Keyword(s):  
Experimental Investigation ◽  
Resin Transfer Molding ◽  
Molding Process ◽  
Transfer Molding

A Closed Form Solution for Flow During the Vacuum Assisted Resin Transfer Molding Process

1999 ◽  
Vol 122 (3) ◽  
pp. 463-475 ◽  
Author(s):  
K-T. Hsiao ◽  
R. Mathur ◽  
S. G. Advani ◽  
J. W. Gillespie, ◽  
B. K. Fink
Keyword(s):  
Closed Form ◽  
Scaling Laws ◽  
Resin Transfer Molding ◽  
Closed Form Solution ◽  
Form Solution ◽  
Flow Front ◽  
Molding Process ◽  
Transfer Molding ◽  
Front Region ◽  
Insight Into

A closed form solution to the flow of resin in vacuum assisted resin transfer molding process (VARTM) has been derived. VARTM is used extensively for affordable manufacturing of large composite structures. During the VARTM process, a highly permeable distribution medium is incorporated into the preform as a surface layer. During infusion, the resin flows preferentially across the surface and simultaneously through the preform giving rise to a complex flow front. The analytical solution presented here provides insight into the scaling laws governing fill times and resin inlet placement as a function of the properties of the preform, distribution media and resin. The formulation assumes that the flow is fully developed and is divided into two regimes: a saturated region with no crossflow and a flow front region where the resin is infiltrating into the preform from the distribution medium. The flow front region moves with a uniform velocity. The law of conservation of mass and Darcy’s Law for flow through porous media are applied in each region. The resulting equations are nondimensionalized and are solved to yield the flow front shape and the development of the saturated region. It is found that the flow front is parabolic in shape and the length of the saturated region is proportional to the square root of the time elapsed. The results thus obtained are compared to data from full scale simulations and an error analysis of the solution was carried out. It was found that the time to fill is determined with a high degree of accuracy while the error in estimating the flow front length, d, increases with a dimensionless parameter ε=K2xxh22/K2yyd2. The solution allows greater insight into the process physics, enables parametric and optimization studies and can reduce the computational cost of full-scale 3-dimensional simulations. A parametric study is conducted to establish the sensitivity of flow front velocity to the distribution media/preform thickness ratio and permeabilities and preform porosity. The results provide insight into the scaling laws for manufacturing of large scale structures by VARTM. [S1087-1357(00)02002-5]

Analysis of the resin transfer molding process using in-mold dielectric sensors

1993 ◽  
Vol 217 ◽  
pp. 251-262 ◽  
Author(s):  
D.J. Melotik ◽  
M. Czaplicki ◽  
T.J. Whalen ◽  
D.R. Day
Keyword(s):  
Resin Transfer Molding ◽  
Molding Process ◽  
Transfer Molding ◽  
Dielectric Sensors
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