Post‐processing technologies of copper – polylactic acid composites obtained by 3D printing fused deposition modelling

2021 ◽  
Author(s):  
Sebastian Ambruș ◽  
Roxana Muntean ◽  
Norbert Kazamer ◽  
Cosmin Codrean
Keyword(s):  
3D Printing ◽  
Polylactic Acid ◽  
Fused Deposition Modelling ◽  
Post Processing ◽  
Processing Technologies ◽  
Fused Deposition

scholarly journals Impact of Chemical Post-Processing in Fused Deposition Modelling (FDM) on Polylactic Acid (PLA) Surface Quality and Structure

Polymers ◽  
2019 ◽  
Vol 11 (3) ◽  
pp. 566 ◽  
Author(s):  
Ana Valerga ◽  
Moises Batista ◽  
Severo Fernandez-Vidal ◽  
Antonio Gamez
Keyword(s):  
Glass Transition ◽  
Thermal Resistance ◽  
Polylactic Acid ◽  
Surface Finish ◽  
Fused Deposition Modelling ◽  
Biodegradable Material ◽  
Post Processing ◽  
Fused Deposition ◽  
Functional Aspects ◽  
Property Changes

The application of techniques to improve the surface finish of pieces obtained by fused deposition modelling, as well as other functional aspects, is of great interest nowadays. Polylactic acid, a biodegradable material, has been considered a possible substitute for petroleum-based polymers. In this work, different chemical post-processing methods are applied to polylactic acid pieces obtained by fused deposition modelling and some characteristics are studied. Structural, thermal, and crystallinity property changes are analyzed according to the treatments applied. This can prevent degradation, eliminate the glass transition phase of the material, and thereby increase the thermal resistance by about 50 °C. An improvement in the roughness of the pieces of up to 97% was also found.

scholarly journals The use of statistical techniques to study the machine parameters affecting the properties of 3D printed cotton/polylactic acid fabrics

2020 ◽  
Vol 15 ◽  
pp. 155892502092853
Author(s):  
Nonsikelelo Sheron Mpofu ◽  
Josphat Igadwa Mwasiagi ◽  
Londiwe Cynthia Nkiwane ◽  
David Njuguna Githinji
Keyword(s):  
Tensile Strength ◽  
3D Printing ◽  
Polylactic Acid ◽  
Adhesion Force ◽  
Extrusion Temperature ◽  
Coefficient Of Determination ◽  
Fused Deposition Modelling ◽  
Fused Deposition ◽  
Before And After ◽  
Printing Speed

Textile materials have been combined with polymers using 3D printing technology, thus producing structures with novel properties. The aim of this study was to use statistical methods to determine the effect of 3D printing machine parameters on the mechanical properties of cotton fabrics combined with polylactic acid. Polylactic acid was printed on a cotton fabric using an Athena Fused Deposition Modelling 3D printer. The effect of extrusion temperature, printing speed, fill density and model height on adhesion force before and after washing was investigated. A study of the tensile strength was also undertaken using a central composite rotatable design and regression analysis. The experimental data were used to develop regression models to predict the properties of the cotton/ polylactic acid structures. The model for adhesion force before washing yielded a coefficient of determination (R2) value of 0.75 and an optimum adhesion force of 50.06 N/cm. The model for adhesion force had an R2 value of 0.84 and an optimum adhesion force of 42.91 N/cm and showed that adhesion force reduced after washing. Adhesion forces before and after washing were both positively correlated to extrusion temperature. However, they reduced with an increase in printing speed and model height. A positive correlation exists between tensile strength and temperature, while a negative correlation exists between tensile strength and printing speed and model height. From the results of this study, it was concluded that 3D printing parameters have an effect on the properties of the structures.

scholarly journals Polylactic acid as a suitable material for 3D printing of protective masks in times of COVID-19 pandemic

PeerJ ◽  
2020 ◽  
Vol 8 ◽  
pp. e10259
Author(s):  
Eva Vaňková ◽  
Petra Kašparová ◽  
Josef Khun ◽  
Anna Machková ◽  
Jaroslav Julák ◽  
...  
Keyword(s):  
3D Printing ◽  
Polylactic Acid ◽  
Sodium Hypochlorite ◽  
Mechanical Damage ◽  
Human Adenovirus ◽  
Test System ◽  
Fused Deposition Modelling ◽  
High Porosity ◽  
Suitable Material ◽  
Fused Deposition

A critical lack of personal protective equipment has occurred during the COVID-19 pandemic. Polylactic acid (PLA), a polyester made from renewable natural resources, can be exploited for 3D printing of protective face masks using the Fused Deposition Modelling technique. Since the possible high porosity of this material raised questions regarding its suitability for protection against viruses, we have investigated its microstructure using scanning electron microscopy and aerosol generator and photometer certified as the test system according to the standards EN 143 and EN 149. Moreover, the efficiency of decontaminating PLA surfaces by conventional chemical disinfectants including 96% ethanol, 70% isopropanol, and a commercial disinfectant containing 0.85% sodium hypochlorite has been determined. We confirmed that the structure of PLA protective masks is compact and can be considered a sufficient barrier protection against particles of a size corresponding to microorganisms including viruses. Complete decontamination of PLA surfaces from externally applied Staphylococcus epidermidis, Escherichia coli, Candida albicans and SARS-CoV-2 was achieved using all disinfectants tested, and human adenovirus was completely inactivated by sodium hypochlorite-containing disinfectant. Natural contamination of PLA masks worn by test persons was decontaminated easily and efficiently by ethanol. No disinfectant caused major changes to the PLA surface properties, and the pore size did not change despite severe mechanical damage of the surface. Therefore, PLA may be regarded as a suitable material for 3D printing of protective masks during the current or future pandemic crises.

scholarly journals The effect of nozzle hole diameter of 3D printing on porosity and tensile strength parts using polylactic acid material

2020 ◽  
Vol 10 (1) ◽  
pp. 762-768 ◽  
Author(s):  
Joko Triyono ◽  
Heru Sukanto ◽  
Rizki Mica Saputra ◽  
Dharu Feby Smaradhana
Keyword(s):  
Tensile Strength ◽  
3D Printing ◽  
Product Quality ◽  
Polylactic Acid ◽  
Hole Diameter ◽  
Fused Deposition Modelling ◽  
3D Printer ◽  
Fused Deposition ◽  
Nozzle Hole ◽  
Line Type

AbstractNozzle hole diameter of 3D printer (3DP) can be varied to obtain required product quality as well as to reduce manufacturing times. The use of larger diameter may accelerate manufacturing times of products, yet the product quality, including the mechanical properties, still needs to be investigated profoundly. The purpose of this work is to investigate experimentally the effect of nozzle hole diameter of 3DP to the surface quality, accuracy, and the strength of the product. The specimens were manufactured by fused deposition modelling (FDM) 3D printing using polylactic acid (PLA) as the filaments.Bed temperature, extruder temperature and printing speed were set to be 60∘C, 200∘C and 80 mm/s respectively. The thickness of each layer was set at the ratio of 20% to the nozzle hole diameter. Infill pattern was determined by using line type of 100%. Nozzle hole diameter of 0.3, 0.4, 0.5 and 0.6mmwas compared in thiswork. The results show that bigger nozzle hole diameter enhanced the density and tensile strength of the products thought it was not linearly correlation.

Effect of heat treatment on mechanical properties of 3D printed polylactic acid parts

2021 ◽  
Vol 63 (1) ◽  
pp. 73-78
Author(s):  
Pulkin Gupta ◽  
Sudha Kumari ◽  
Abhishek Gupta ◽  
Ankit Kumar Sinha ◽  
Prashant Jindal
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Polylactic Acid ◽  
Recrystallization Temperature ◽  
Fused Deposition Modelling ◽  
Fused Deposition ◽  
Dog Bone ◽  
Heat Treated ◽  
Maximum Decrease ◽  
3D Printed

Abstract Fused deposition modelling (FDM) is a layer-by-layer manufacturing process type of 3D-printing (3DP). Significant variation in the mechanical properties of 3D printed specimens is observed because of varied process parameters and interfacial bonding between consecutive layers. This study investigates the influence of heat treatment on the mechanical strength of FDM 3D printed Polylactic acid (PLA) parts with constant 3DP parameters and ambient conditions. To meet the objectives, 7 sets, each containing 5 dog-bone shaped samples, were fabricated from commercially available PLA filament. Each set was subjected to heat treatment at a particular temperature for 1 h and cooled in the furnace itself, while one set was left un-treated. The temperature for heat treatment (Th) varied from 30 °C to 130 °C with increments of 10 °C. The heat-treated samples were characterized under tensile loading of 400 N and mechanical properties like Young’s modulus (E), Strain % ( ε ) and Stiffness (k) were evaluated. On comparing the mechanical properties of heat-treated samples to un-treated samples, significant improvements were observed. Heat treatment also altered the geometries of the samples. Mechanical properties improved by 4.88 % to 10.26 % with the maximum being at Th of 110 °C and below recrystallization temperature (Tr) of 65 °C. Deformations also decreased significantly at higher temperatures above 100 °C, by a maximum of 36.06 %. The dimensions of samples showed a maximum decrease of 1.08 % in Tr range and a maximum decrease of 0.31 % in weight at the same temperature. This study aims to benefit the society by establishing suitable Th to recover the lost strength in PLA based FDM 3D printed parts.

scholarly journals Advanced Pharmaceutical Applications of Hot-Melt Extrusion Coupled with Fused Deposition Modelling (FDM) 3D Printing for Personalised Drug Delivery

Pharmaceutics ◽  
2018 ◽  
Vol 10 (4) ◽  
pp. 203 ◽  
Author(s):  
Deck Tan ◽  
Mohammed Maniruzzaman ◽  
Ali Nokhodchi
Keyword(s):  
3D Printing ◽  
Hot Melt Extrusion ◽  
Pharmaceutical Products ◽  
Fused Deposition Modelling ◽  
Melt Extrusion ◽  
3D Object ◽  
3D Printing Technology ◽  
Fused Deposition ◽  
Pharmaceutical Applications ◽  
Hot Melt

Three-dimensional printing, also known as additive manufacturing, is a fabrication process whereby a 3D object is created layer-by-layer by depositing a feedstock material such as thermoplastic polymer. The 3D printing technology has been widely used for rapid prototyping and its interest as a fabrication method has grown significantly across many disciplines. The most common 3D printing technology is called the Fused Deposition Modelling (FDM) which utilises thermoplastic filaments as a starting material, then extrudes the material in sequential layers above its melting temperature to create a 3D object. These filaments can be fabricated using the Hot-Melt Extrusion (HME) technology. The advantage of using HME to manufacture polymer filaments for FDM printing is that a homogenous solid dispersion of two or more pharmaceutical excipients i.e., polymers can be made and a thermostable drug can even be introduced in the filament composition, which is otherwise impractical with any other techniques. By introducing HME techniques for 3D printing filament development can improve the bioavailability and solubility of drugs as well as sustain the drug release for a prolonged period of time. The latter is of particular interest when medical implants are considered via 3D printing. In recent years, there has been increasing interest in implementing a continuous manufacturing method on pharmaceutical products development and manufacture, in order to ensure high quality and efficacy with less batch-to-batch variations of the pharmaceutical products. The HME and FDM technology can be combined into one integrated continuous processing platform. This article reviews the working principle of Hot Melt Extrusion and Fused Deposition Modelling, and how these two technologies can be combined for the use of advanced pharmaceutical applications.

scholarly journals 3D Printing of Thermo-Sensitive Drugs

Pharmaceutics ◽  
2021 ◽  
Vol 13 (9) ◽  
pp. 1524
Author(s):  
Sadikalmahdi Abdella ◽  
Souha H. Youssef ◽  
Franklin Afinjuomo ◽  
Yunmei Song ◽  
Paris Fouladian ◽  
...  
Keyword(s):  
3D Printing ◽  
Three Dimensional ◽  
Fused Deposition Modelling ◽  
Future Directions ◽  
Digital Light Processing ◽  
Fused Deposition ◽  
Printing Technique ◽  
3D Printed ◽  
Semi Solid ◽  
Selection Of

Three-dimensional (3D) printing is among the rapidly evolving technologies with applications in many sectors. The pharmaceutical industry is no exception, and the approval of the first 3D-printed tablet (Spiratam®) marked a revolution in the field. Several studies reported the fabrication of different dosage forms using a range of 3D printing techniques. Thermosensitive drugs compose a considerable segment of available medications in the market requiring strict temperature control during processing to ensure their efficacy and safety. Heating involved in some of the 3D printing technologies raises concerns regarding the feasibility of the techniques for printing thermolabile drugs. Studies reported that semi-solid extrusion (SSE) is the commonly used printing technique to fabricate thermosensitive drugs. Digital light processing (DLP), binder jetting (BJ), and stereolithography (SLA) can also be used for the fabrication of thermosensitive drugs as they do not involve heating elements. Nonetheless, degradation of some drugs by light source used in the techniques was reported. Interestingly, fused deposition modelling (FDM) coupled with filling techniques offered protection against thermal degradation. Concepts such as selection of low melting point polymers, adjustment of printing parameters, and coupling of more than one printing technique were exploited in printing thermosensitive drugs. This systematic review presents challenges, 3DP procedures, and future directions of 3D printing of thermo-sensitive formulations.

scholarly journals 3D Printing of Solvent-Free Supramolecular Polymers

2021 ◽  
Vol 9 ◽  
Author(s):  
Harald Rupp ◽  
Wolfgang H. Binder
Keyword(s):  
3D Printing ◽  
Dynamic Properties ◽  
Polymeric Materials ◽  
Fundamental Principle ◽  
Supramolecular Polymers ◽  
Fused Deposition Modelling ◽  
Self Healing ◽  
Polymer Science ◽  
Fused Deposition ◽  
Molecular Ordering

Additive manufacturing has significantly changed polymer science and technology by engineering complex material shapes and compositions. With the advent of dynamic properties in polymeric materials as a fundamental principle to achieve, e.g., self-healing properties, the use of supramolecular chemistry as a tool for molecular ordering has become important. By adjusting molecular nanoscopic (supramolecular) bonds in polymers, rheological properties, immanent for 3D printing, can be adjusted, resulting in shape persistence and improved printing. We here review recent progress in the 3D printing of supramolecular polymers, with a focus on fused deposition modelling (FDM) to overcome some of its limitations still being present up to date and open perspectives for their application.

Vibration Characteristics of 3D Printed Viscoelastic Graded Polymeric Plates

2021 ◽  
Author(s):  
Justin Carter ◽  
Kumar Vikram Singh ◽  
Fazeel Khan
Keyword(s):  
3D Printing ◽  
Fused Deposition Modeling ◽  
Polymeric Materials ◽  
Vibration Characteristics ◽  
Thin Plates ◽  
Future Research ◽  
Structural Components ◽  
Processing Technologies ◽  
Fused Deposition ◽  
Multiple Materials

Abstract The exploration of structures made of multiple materials is a growing area of research as additive manufacturing processing technologies such as fused deposition modeling (FDM) 3D printing allows for their fabrication. Such a technology allows for rapid prototyping of structural components with complex geometries or spatially distributed materials with different properties and functionalities. By selecting suitable spatial distribution of materials, the performance of structural components can be manipulated and enhanced as per different engineering application needs. For a low-cost design of structural prototypes using 3D printing processes, viscoelastic polymeric materials are often used, having inherent damping properties. In this research, vibration characteristics of thin plates which are axially graded with multiple polymeric materials are investigated. The goal is to understand the influence of material grading on the frequency and damping characteristics of graded plates. Although in literature, material grading along the thickness in designing composite laminates and their vibration characteristics are available, the performance of plates having axially graded viscoelastic polymers have not been investigated yet. Through systematic modeling and experimental plans, vibration characteristics of axially graded viscoelastic plates are presented here. In particular, the damping performance for different grading schemes is evaluated. It is anticipated that such analysis will allow accurate modeling and testing of design prototypes of structural components for future research, such as design and testing of graded panels for enhanced flutter characteristics.

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